Summary
A number of headspace techniques have been compared, using a standard solution containing 12 compounds and a wine sample, viz.: (1) purge and cold trap injection; (2) dynamic headspace combined with liquidliquid extraction; (3) static headspace with and without preconcentration; (4) direct liquid injection. The sensitivity, reproducibility and speed of analysis were determined. Considering the results obtained and dependent on the purpose of the experiments and the number of samples to be examined the appropriate technique can be selected.
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Etievant, P., Maarse, H. & van den Berg, F. Wine analysis: Study and comparison of techniques developed for the study of volatile constituents. Chromatographia 21, 379–386 (1986). https://doi.org/10.1007/BF02346136
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DOI: https://doi.org/10.1007/BF02346136