Summary
A new procedure for sampling, transfer, and analysis of volatile organic compounds by gas chromatography has been developed. An adsorbent trap ultimately becomes an insert for a modified injector port, and a valve system allows the sample to be transferred to a cooled precolumn and finally to the separating column. Several traps may be used for sampling (for multiple injections), and it has been established that such traps may be stored without loss of sample. The ease and reproducibility of this procedure is amenable for the investigation of volatile organic compounds involving air and water pollution, flavor, and aroma analyses, and body fluid metabolites.
Similar content being viewed by others
Literature
A. Zlatkis andH. M. Liebich, Clin. Chem.7, 592 (1971).
R. Teranishi, T. R. Mon, P. Cary, A. B. Robinson, andL. Pauling, Anal. Chem.44, 18 (1972).
E. C. Horning andM. G. Horning, in, Methods in Medical Research.R. E. Olson ed., Year Book Medical Publishers, Inc., Chicago (1970).
E. Jellum, O. Stokke, andL. Eldjarn, Scand. J. Clin. Lab. Invest.27, 273 (1971).
R. Teranishi, P. Issenberg, I. Hornstein, andE. L. Wick in Flavor Research, Principles and Techniques, O. R. Fennema, ed., Marcel Dekker, Inc., New York, 1971.
J. Novak, V. Vasak, andJ. Janak, Anal. Chem.,37, 660 (1965).
S. B. Dave, J. Chromatog. Sci.,7, 389 (1969).
V. J. Richter andJ. Tonzetich, Arch. Oral. Biol.9, 47 (1964).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Zlatkis, A., Lichtenstein, H.A. & Tishbee, A. Concentration and analysis of trace volatile organics in gases and biological fluids with a new solid adsorbent. Chromatographia 6, 67–70 (1973). https://doi.org/10.1007/BF02270540
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF02270540