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Surface treatment, deactivation and coating in (GC)2 (glass capillary gas chromatography)

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Summary

The surface treatment, deactivation and coating of glass capillaries is discussed. Several techniques described in the literature are compared and for some critical points, new improved methods are advanced. Full details are given of optimised procedures yielding good results with every possible stationary phase. As an example, Table II mentions efficiencies of 3800 plates m−1 for OV-17 and of 1850 plates m−1 for OF-1, which hitherto was an “impossible” phase in (GC)2 (proposed abbreviation for glass capillary gas chromatography).

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Literature

  1. C. Watanabe andH. Tomita, J. Chromatogr. Science13, 123 (1975).

    Google Scholar 

  2. P. Sandra, M. Verstappe andM. Verzele; unpublished results.

  3. J. J. Franken, G. A. F. M. Rutten andJ. A. Ryks, J. Chromatogr.126, 117 (1976).

    Article  Google Scholar 

  4. G. Nota, G. C. Goretti, M. Armenante andG. Marino, J. Chromatogr.95, 229 (1974).

    Article  Google Scholar 

  5. G. C. Goretti, A. Liberti andG. Nota, Chromatographia8, 486 (1975).

    Google Scholar 

  6. J. G. Nikelly andM. Blumer, Amer. Lab.6, 12 (1974).

    Google Scholar 

  7. A. L. German, C. D. Pfaffenberger, J. P. Thenot, M. G. Hornig andE. C. Horning, Anal. Chem.45, 930 (1973).

    Article  Google Scholar 

  8. R. S. Deelder, J. J. M. Ramaekers, J. H. M. Van Den Berg andM. L. Wetzels, J. Chromatogr.119, 99 (1976).

    Article  PubMed  Google Scholar 

  9. L. S. Ettre andJ. E. Purcell, Adv. in Chromatogr.10, 1 (1974).

    Google Scholar 

  10. K. Grob andG. Grob, J. Chromatogr.125, 471 (1976).

    Article  Google Scholar 

  11. G. Alexander, G. Garzo andG. Palyi. J. Chromatogr.91, 25 (1974).

    Article  Google Scholar 

  12. J. Krupcik, M. Kristin, M. Valachovicova andS. Janiga, J. Chromatogr.126, 147 (1976).

    Article  Google Scholar 

  13. F. I. Onuska andM. E. Comba, J. Chromatogr.126, 133 (1976).

    Article  Google Scholar 

  14. K. Tesarik andM. Novotny inH. G. Struppe (Editor), Gas-Chromatographic 1968, Akademic-Verlag GmbH, Berlin, 1968, 575.

    Google Scholar 

  15. J. D. Schieke, N. R. Comins andV. Pretorius, J. Chromatogr.112, 97 (1975).

    Article  Google Scholar 

  16. J. D. Schieke, N. R. Comins andV. Pretorius, Chromatographia8, 354 (1975).

    Google Scholar 

  17. G. Alexander andG. A. M. F. Rutten, Chromatographia6, 231 (1973).

    Google Scholar 

  18. A. L. German andE. C. Horning, J. Chromatogr. Sci.11, 76 (1973).

    PubMed  Google Scholar 

  19. M. Novotny andK. Tesarik, Chromatographia1, 332 (1968).

    Article  Google Scholar 

  20. M. Novotny, K. D. Bartle andL. Biomberg, J. Chromatogr. Sci.8, 390 (1970).

    Google Scholar 

  21. G. A. F. M. Rutten andJ. A. Luyten, J. Chromatogr.74, 177 (1972).

    Article  PubMed  Google Scholar 

  22. H. T. Badings, J. J. G. Van Der Pol andJ. G. Wassink, Chromatographia8, 440 (1975).

    Google Scholar 

  23. R. E. Kaiser andR. Rieder, Chromatographia8, 491 (1975).

    Google Scholar 

  24. G. Schomburg, H. Husmann andF. Weeke, J. Chromatogr.99, 63 (1974).

    Article  Google Scholar 

  25. D. A. Cronin, J. Chromatogr.97, 263 (1974).

    Article  Google Scholar 

  26. L. Blomberg, J. Chromatogr.115, 365 (1975).

    Article  Google Scholar 

  27. C. Hista andJ. Bornstein, Adv. in Chromatogr.9, 215 (1970).

    Google Scholar 

  28. K. Grob, Helv. Chim. Acta51, 718 (1968).

    Article  Google Scholar 

  29. K. Grob andE. Grob, Chromatographia4, 422 (1971).

    Google Scholar 

  30. J. Bouche andM. Verzele, J. Gas. Chromatogr.6, 501 (1968).

    Google Scholar 

  31. G. Dykstra andJ. De Goey, inD. H. Desty (Editor), Gas Chromatography 1958, Butterworths, London (1958), 56.

    Google Scholar 

  32. T. Boogaerts, M. Verstappe andM. Verzele, J. Chromatogr. Sci.10, 217 (1972).

    Google Scholar 

  33. P. Sandra, M. Verzele andE. Vanluchene, Chromatographia8, 499 (1975).

    Google Scholar 

  34. G. Redant, P. Sandra andM. Verzele, in preparation.

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Authors and Affiliations

  1. Laboratory of Organic Chemistry, State University of Ghent, Krijgslaan, 271 (S4), 9000, Gent, Belgium

    P. Sandra & M. Verzele

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  1. P. Sandra
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  2. M. Verzele
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Sandra, P., Verzele, M. Surface treatment, deactivation and coating in (GC)2 (glass capillary gas chromatography). Chromatographia 10, 419–425 (1977). https://doi.org/10.1007/BF02257354

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  • DOI: https://doi.org/10.1007/BF02257354

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