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The coupling of gas chromatography with methods of identification III. Infrared spectrophotometry

Die Kopplung der Gas-Chromatographie mit Erkennungsmethoden III. Infrarot-Spektrophotometrie

Le couplage de la chromatographie en phase gazeuse des méthodes d'identification III. Spectrophotométrie d'infrarouge

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Summary

This article reviews the combined technique in which vapors eluted from gas chromatographic columns are identified by their infra-red spectra. It describes the technology of the method, including both the simpler, established methods, and also the more recent techniques in which the spectroscopy and the chromatography are performed simultaneously. A brief table of some of the more significant published applications is given.

Zusammenfassung

Dieser Artikel referiert die Kopplungstechnik, in der die aus der gas-chromatographischen Säule eluierten Dämpfe durch ihre Infrarotspektren identifiziert werden. Es wird die Arbeitsweise der Methode beschrieben, einschließlich einfacher, eingeführter Verfahren und neuerer Techniken, wobei Spektroskopie und Chromatographie gleichzeitig betrieben werden. Eine kurze Tabelle über einige besondere, veröffentlichte Anwendungen wurde zusammengestellt.

Sommaire

Cet article traite des techniques de couplage permettant d'obtenir des spectres infra-rouges pour les vapeurs éluées des colonnes de chromatographie en phase gazeuse, ce qui facilite l'identification des composés correspondants. On décrit les différentes méthodes d'application de ce principe, depuis les dispositifs les plus simples jusqu'aux techniques les plus récentes permettant d'utiliser simultanément la chromatographie et la spectrophotométrie infra-rouge. Un tableau rassemble la bibliographie concernant les applications particulières de cette méthode de couplage.

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References

  1. Allen, R. R., Chem. and Ind. (London),1965, 1560.

  2. Anderson, D. M. W., Analyst84, 80 (1959).

    Article  Google Scholar 

  3. Anderson, D. M. W. andDuncan, J. L., Chem. and Ind.1958, 1662.

  4. Bartz, A. M. andRuhl, H. D., Anal. Chem.36, 1892 (1964).

    Google Scholar 

  5. Bellis, H. E., Slowinski, E. J., Jr., J. Chem. Phys.25, 795 (1956).

    Google Scholar 

  6. Beckman, H., Allen, P. T. andBerkenkotter, P., J. Gas Chromatog.1 (8), 21 (1963).

    Google Scholar 

  7. Beckman Instruments, Inc., Fullerton, California, Bulletin 7073.

  8. Behrendt, S., Nature201, 70 (1964).

    Google Scholar 

  9. Behrendt, S. andRichtering, H., J. Chromatog.24, 1 (1966).

    Article  Google Scholar 

  10. Bergomi, A., Burden, J., Hodgkins, T. M., Stephens, R. andTatlow, J. C., Tetrahedron22, 43 (1966).

    Article  Google Scholar 

  11. Blake, R. H., Erley, D. S., Beman, F. L., ibid.18, 114 (1964).

    Google Scholar 

  12. Blay, N. J., Danstan, I. andWilliams, R. L., J. Chem. Soc.1960, 430.

  13. Chang, S. S., Ireland, C. E., Tai, H., Anal. Chem.33, 479 (1961).

    Article  Google Scholar 

  14. Chang S. S., Brobst, K. M., Ireland, C. E., Tai, H., Appl. Spectry.16, 106 (1962).

    Article  Google Scholar 

  15. Chang, T. Cl. andKarr, C. Anal. Chim. Acta24, 343 (1961).

    Article  Google Scholar 

  16. Chen, J. T., J. Assoc. Offic. Agr. Chemists.48, 380 (1965).

    Google Scholar 

  17. Chrenko, R. M., Anal. Chem.36, 1883 (1964).

    Article  Google Scholar 

  18. Coffman, J. R., Smith, D. E. andAndrews, J. S., Food Res.25, 663 (1961).

    Google Scholar 

  19. Copier, H. andvan der Maas, J. H., Spectrochim. Act.23A, 2699 (1967).

    Article  Google Scholar 

  20. Datta, R. R. andSusi, H., Anal. Chem.34, 1028 (1962).

    Article  Google Scholar 

  21. Edwards, R. A., Fagerson, I. S., Anal. Chem.37, 1630 (1965).

    Article  Google Scholar 

  22. Ellis, C. F., Kendall, R. F. andEccleston, B. H., Anal. Chem.37, 511 (1965).

    Article  Google Scholar 

  23. Filipic, V. J. andUnderwood, J. C., J. Food Sci.29, 464 (1964).

    Google Scholar 

  24. Flett, M. St. C. andHughes, J., J. Chromatog.11 434 (1963).

    Article  Google Scholar 

  25. Fritz, G. andThelking, H., Z. anorg. u. allgem. chem.306, 39 (1960).

    Article  Google Scholar 

  26. Golay, M. J. E., “Gas Chromatography 1966”, Proceedings of the Sixth International Symposium, Ed. Littlewood, A. B., Institute of Petroleum, 1967, p. 333.

  27. Grasselli, J. G., Snavely, M. K., Appl. Spectry.16, 190 (1962).

    Article  Google Scholar 

  28. Gray, L. S., Metcalfe, L. D., Leslie, L. D., Fourth International Gas Chromatography Symposium, Michigan State University, June 1963.

  29. Haahti, E. A. andFales, H. M., Chem. and Ind.1961, 507.

  30. Hall, J. H., Hill, J. W. andTsai, H. C., Tetrahedron Letters, 1965, 2211.

  31. Hansen, R. P., Shorland, F. B. andMorrison, J. D., J. Dairy Res.32, 21 (1965).

    Google Scholar 

  32. Haslam, J., Jeffs, A. R., Willis, H. A., Analyst86, 44 (1961).

    Article  Google Scholar 

  33. Heinz, D. E. andJennings, W. G., J. Food Sci.31, 69 (1966).

    Google Scholar 

  34. Heinze, H. O., Angew. chem.72, 586 (1960).

    Google Scholar 

  35. Hoffman, G., J. Am. Oil Chemists Soc.38, 1, 31 (1961).

    Google Scholar 

  36. Hoffman, R. L., Silveira, A., Jr., J. Gas Chromatog.2, 107 (1964).

    Google Scholar 

  37. Howard, G. A. andStevens, R., Chem. and Ind.1959, 1518.

  38. Howlett, M. D. D. andWelti, D., Analyst91, 291 (1966).

    Article  Google Scholar 

  39. Hunter, G. L. K. andBrogden, W. B., J. Food Sci.30, 1 (1965).

    Google Scholar 

  40. Hunter, G. L. K. andMoshonas, M. G., J. Food Sci.31, 167 (1966).

    Google Scholar 

  41. Johns, T., “Gas Chromatography 1960”, Proceedings of the Third International Symposium, Ed. Scott, R. P. W., Butterworths, 1960, p. 251.

  42. Leggon, H. W., Anal. Chem.33, 1295 (1961).

    Article  Google Scholar 

  43. Low, M. J. D. andFreeman, S. K., Ana. Chem.39, 194 (1967).

    Article  Google Scholar 

  44. Mair, B. J. andMayer, T. J., Anal. Chem.36, 351 (1964).

    Article  Google Scholar 

  45. Matthews, J. S., Burow, F. H. andSnyder, R. E., Anal. Chem.32, 691 (1960).

    Article  Google Scholar 

  46. McGregor, D. R., Sugisawa, H. andMatthews, J. S., J. Food Sic.29, 448 (1964).

    Google Scholar 

  47. Nigam, I. C., J. Pharm. Sci.54, 1823 (1965).

    Google Scholar 

  48. Nozaki, H., Nisikawa, Y., Kamatani, Y. andNoyori, R., Tetrahedron Letters1965, 2161.

  49. Paulig, G., Deutsche Lebensmittel Rundschau57, 42 (1961).

    Google Scholar 

  50. Perry, S. G. andRitchie, R. K., Informal Symposium of the G. C. Discussion Group, Sept. 1967: see Littlewood, A. B., J. of Gas Chromatog.6, 65 (1968).

  51. Philpotts, A. R., Informal Symposium of the G. C. Discussion Group, Sept. 1967; see Littlewood, A. B., J. of Gas Chromatog.6, 65 (1968).

  52. Pyne, A. W. andWick, E. L., J. Food Sci.30, 193 (1965).

    Google Scholar 

  53. Rudloff, E. von Can. J. Chem.39, 1200 (1961).

    Google Scholar 

  54. Sato, S. andCvetanovic, R. J., Can. J. Chem.37, 953 (1959).

    Google Scholar 

  55. Scarpellino, R. andKosikowski, F. V., J. Dairy Sci.54, 343 (1962).

    Google Scholar 

  56. Schmeltz, I., Stills, C. D., Chamberlain, W. J. andStedman, R. L., Anal. Chem.,37, 1614 (1965).

    Article  PubMed  Google Scholar 

  57. Scott, R. P. W., Fowlis, I. A., Welti, D. andWilkins, T., “Gas Chromatography 1966”, Proceedings of the Sixth International Symposium, Ed. Littlewood, A. B., Institute of Petroleum, 1967, p. 318.

  58. Senn, W. L. andDrushel, H. V., Anal. Chim. Acta25, 328 (1961).

    Google Scholar 

  59. Sevenants, M. R. andJennings, W. G., J. Food Sci.31, 81 (1966).

    Google Scholar 

  60. Matthews, J. S., Burow, F. H., Snyder, R. E., ibid.,32, 691 (1960).

    Google Scholar 

  61. Schinohara, T., Ohkusa, T. andOkada, Y., Bunseki Kagaku 10, 241 (1961).

    Google Scholar 

  62. Shumaker, W., Chemist-Analyst50, 22 (1961).

    Google Scholar 

  63. Snelson, F. L. Chem. Ind. (London)14, 575 (1964).

    Google Scholar 

  64. Stevens, R. K., Mold, J. D. J. Chromatog.10, 398 (1963).

    Article  Google Scholar 

  65. Stewart, J. E., Brace, R. O., Johns, T. andUlrich, W. F., Nature,186, 628 (1960).

    Google Scholar 

  66. Szymanski, H. A., Povinelli, R., Stamires, D., Lynch, G., ibid.,31, 2110 (1959).

    Google Scholar 

  67. Tabuteau, J., Ind. chim. belge, Sullp1 135 (1959).

    Google Scholar 

  68. Tadayon, J., Informal Symposium of the G. C. Discussion Group, Sept. 1967; see Littlewood, A. B., J. of Gas Chromatog.6, 65 (1968).

  69. Thomas, P. J., Dwyer, J. L., J. Chromatog.13, 366 (1964).

    Article  Google Scholar 

  70. Thompson, C. J., Coleman, H. J., Hipkins, R. L. andRall, H. T., Anal. Chem. 38, 1562 (1966).

    Article  Google Scholar 

  71. Welti, D., Informal Symposium of the G. C. Discussion Group, Sept. 1967; see Littlewood, A. B., J. of Gas Chromatog.6, 65 (1968).

  72. Whittenbaugh, J. A., McCinness, J. D., andLucchesi, C. A., Tappi43, 1027 (1960).

    Google Scholar 

  73. Wilks, P. A. Jr., Informal Symposium of the G. C. Discussion Group, Sept. 1967; see Littlewood, A. B., J. of Gas Chromatog. 6, 65 (1968).

  74. Wilks, P. A. andBrown, R. A., Anal. Chem.36, 1896 (1964).

    Article  Google Scholar 

  75. Willis, H. A. andCudby, M. E. A., Informal Symposium of the G. C. Discussion Group, Sept. 1967; see Littlewood, A. B., J. of Gas Chromatog.6, 65 (1968).

  76. Zweig, G., Archer, T. E. andRubenstein, D., J. Agr. Food Chem.8, 403 (1960).

    Article  Google Scholar 

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Littlewood, B. The coupling of gas chromatography with methods of identification III. Infrared spectrophotometry. Chromatographia 1, 223–230 (1968). https://doi.org/10.1007/BF02255486

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