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Flow reactor for kinetic studies with simultaneous X-ray phase analysis of a catalyst

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Abstract

A flow reactor for kinetic studies of heterogeneous catalytic reactions with simultaneous X-ray phase analysis of the catalyst is described. As an example, the correlation between the selectivity of acetylene hydrogenation and the β-Pd hydride concentration in palladium catalysts is shown.

Abstract

Описан проточный реактор, позволяющий исследовать кинетику гетерогенных каталитических реакций с одновременным рентгенографическим фазовым анализом катализатора во время реакции. В качестве примера представлена полученная корреляция между селективностью гидрогенизации ацетилена и содержанием β-Pd гидрида в палладиевом катализаторе.

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References

  1. F. A. Lewis: The Palladium-Hydrogen System, Academic Press, New York 1967.

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Authors and Affiliations

  1. Department of Catalysis on Metals, Institute of Physical Chemistry, Polish Academy of Sciences, 01-224, Warszawa, Poland

    A. Borodziński & A. Janko

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  1. A. Borodziński
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  2. A. Janko
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Borodziński, A., Janko, A. Flow reactor for kinetic studies with simultaneous X-ray phase analysis of a catalyst. React Kinet Catal Lett 7, 163–169 (1977). https://doi.org/10.1007/BF02061833

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  • DOI: https://doi.org/10.1007/BF02061833

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