Abstract
Two samples of one litre each of mercury contaminated soil were analyzed by Big Sample INAA. Using this method, sample preparation procedures can be omitted and the number of sample size reduction steps are decreased. Therefore, the representativity of the sample is improved. Afterwards, Big Sample INAA is compared to standard INAA by analyzing ten subsamples taken from each one litre sample. It is concluded that multi-element analysis results of Big Sample INAA are valid even for inhomogeneous large samples. This paper presents the first concentrations measured with BSINAA.
Similar content being viewed by others
References
R. M. W. Overwater, J. E. Hoogenboom, Nucl. Sci. Eng., 117 (1994) 141.
R. M. W. Overwater, The Physics of Big Sample Instrumental Neutron Activation Analysis, Thesis, Delft University of Technology, Delft, 1994.
R. M. W. Overwater, Anal. Chem., submitted.
R. M. W. Overwater, P. Bode, J. J. M. De Goeu, Nucl. Instr. Meth., A324 (1993) 209.
P. Bode, R. M. W. Overwater, J. Radioanal. Nucl. Chem., 167 (1993) 169.
O. U. Anders, Nucl. Instr. Methods, 68 (1969) 205.
M. Blaauw, The Holistic Analysis of Gamma-Ray Spectra in Instrumental Neutron Activation Analysis, Thesis, Delft University of Technology, 1993.
A. Simonits, F. De Corte, J. Hoste, J. Radioanal. Nucl. Chem., 24 (1975) 31.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Lakmaker, O., Blaauw, M. The use of Big Sample INAA for inhomogeneous materials: Homogenizations no longer needed?. J Radioanal Nucl Chem 216, 69–74 (1997). https://doi.org/10.1007/BF02034498
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02034498