Abstract
The title structure, which belongs to the triclinicP¯1 space group witha=13.901(4),b=10.732(1),c=10.570(8)Åα=109.14(4),β=96.17(4), γ=90.34(2)°, is refined toR=0.052 for 2985I≥3σ(I) reflections. The structure consists of a non-interacting 1,2,4,6-tetraphenylpyridinium and tetrahedral tetrabromoferrate (III) ions.
Similar content being viewed by others
References
Adams, R., and Johnson, J. R. (1963)Laboratory experiments in organic chemistry. (The Macmillan Company, Collier-Macmillan Ltd., London) pp. 291–292.
Constant, G., Daran, J.-C., and Jeannin, Y. (1973)J. Inorg. Nucl. Chem. 35, 4093–4102.
Cotton, F. A., and Wilkinson, G. (1985)Advanced inorganic chemistry. (Wiley Eastern Limited, New Delhi), p. 864.
Delft Instruments (1990)MolEN structure determination system. (Delft Instruments, X-Ray Diffraction B. V., Röntgenweg 1, 2624 BD Delft, The Netherlands).
Farag, I. S. A., El-Shora, A. I., and Rybakov, V. G. (1990)Cryst. Res. Technol. 25, 591–524.
Gelb, S. J., Rheingold, A. L., Dong, T.-Y., and Hendrickson, D. N. (1986)J. Organomet. Chem. 312, 241–248.
Hackert, M. L., and Jacobson, R. A. (1971)Acta Crystallogr. B27, 1658–1662.
Jolly, W. L. (1985)Modern inorganic chemistry. (McGraw-Hill Book Co., Singapore), p. 334.
Katrizky, A. R., Zuriati, A., and Lunt, E. (1980)J. Chem. Soc. Perkins Trans. I, 1879–1887.
Killean, R. C. G., and Lawrence, J. L. (1969)Acta Crystallogr. 25, 1750–1752.
Lowe, C. B., Carlin, R. L., Shultz, A. J., and Loong, C. K. (1990)Inorg. Chem. 29, 3308–3315.
Mallah, T., Hollis, C., Bott, S., Kurmoo, M., Day, P., Allan, M., and Friend, R. H. (1990)J. Chem. Soc., Dalton Trans. 859–865.
Russo, U., Valle, G., Long, G. J., and Schlemper, E. O. (1987)Inorg. Chem. 26, 665–670.
Schmid, G., Barbenheim, G., and Boese, R. (1985)Z. Naturforsch., B: Anorg. Chem., Org., Chem. B 40, 787–793.
Sproul, G. D., and Stucky, G. D. (1972)Inorg. Chem. 11, 1647–1650.
Walker, N., and Stuart, D. (1983)Acta Crystallogr. A39, 158–166.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Hamid Othman, A., Zakaria, Z. & Weng Ng, S. Crystal structure of 1,2,4,6-tetraphenylpyridinium tetrabromoferrate(III). Journal of Crystallographic and Spectroscopic Research 23, 921–923 (1993). https://doi.org/10.1007/BF01185536
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF01185536