Abstract
The structure of the title compound has been solved by direct methods, and refined to anR value of 0.035 for 1613 reflections. Both methyl carbon atoms deviate from the plane of the pyridine ring by 1.505(3) Å in opposite directions. Both sulfur atoms S(1) and S(2) remain in short contact, at 3.247(1) Å. The two pyridine rings are inclined at 61.4(2)° to each other.
Similar content being viewed by others
References
Baranowska, I., Karmiński, W., Baranowski, R. (1973)Microchim. Acta, 815.
Boryczka, S., Wyszomirski, M., Maślankiewicz, A., Borowiak, T., and Kubicki, M. (1990)Recl. Trav. Chim., Pay-Bas 109, 509.
Maślankiewicz, A. (1985)Polish J. Chem. 59, 511.
Maślankiewicz, A., and Pluta, K. (1980)Polish J. Chem. 54, 33.
Maślankiewicz, A., Wyszomirski, M., and Gkl/owiak, T. (1990)J. Cryst. Spectr. Res. 20, 375.
Pauling, L. (1960)The Nature of the Chemical Bond (third edition) (Cornell, Ithaca).
Pluta, K. (1990) manuscript in preparation.
Syntex (1976)XTL Structure Determination System (Syntex Analytical Instruments, Cupertino, Calif.).
Sheldrick, G. (1986)Shelxs 86; Program for crystal solution (Univ. Gottingen, Germany).
Author information
Authors and Affiliations
Additional information
Part XIV in the series of Azinyl Sulfides.
Rights and permissions
About this article
Cite this article
Pluta, K., Maślankiewicz, A. & Głowiak, T. X-ray structure of 3,3′-bis(4-methylthioquinolinyl) sulfide. Journal of Crystallographic and Spectroscopic Research 21, 153–156 (1991). https://doi.org/10.1007/BF01161057
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF01161057