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Cure performance of multifunctional monomers to photo-initiators: a thermoanalytical study onbis-GMA-based resins

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Abstract

In order to assess cure performance in experimental monomer systems containingbis-GMA and 3G, differential scanning calorimetry was used to obtain heat for curing, and residual monomers present within the resin systems were measured by high-performance liquid chromatography. Visible light-activated polymerization of these monomer systems was studied using camphorquinone (CQ) and reducing agents of dimethylaminoethyl methacrylate (DMAEMA) and dimethyl-para-toluidine (DMPT). For unfilledbis-GMA-based resin (60 wt%bis-GMA and 40 wt% 3 G) containing CQ (0.5 wt%) and DMAEMA (0.5 wt%) indicating approximately 100% polymerization, less residual monomer and larger hardness than the other monomer systems were observed.

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Authors and Affiliations

  1. Department of Dental Materials, School of Dentistry, Hiroshima University, 1-2-3 Kasumi, Minami-ku, 734, Hiroshima, Japan

    H. Urabe, K. Wakasa & M. Yamaki

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  1. H. Urabe
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  2. K. Wakasa
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  3. M. Yamaki
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Urabe, H., Wakasa, K. & Yamaki, M. Cure performance of multifunctional monomers to photo-initiators: a thermoanalytical study onbis-GMA-based resins. J Mater Sci 26, 3185–3190 (1991). https://doi.org/10.1007/BF01124661

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