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Past, present and future of the clathrate inclusion compounds built of cyanometallate hosts

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Abstract

One-, two- and three-dimensional CN-bridged metal complex structures made up of building blocks such as linear [Ag(CN)2]−, square planar [Ni(CN)4]2− or tetrahedral [Cd(CN)4]2−, and of the complementary ligands such as ammonia, water, unidentate amine, bidentate a,w- diaminoalkane, etc., are reviewed with an emphasis on their behaviour as hosts to afford clathrate inclusion compounds with guest molecules and as self-assemblies to form supramolecular structures with or without guests. The historical background is explained for Prussian blue and Hofmann's benzene clathrate based on their single crystal structure determinations. The strategies the author and coworkers have been applying to develop varieties of clathrate inclusion compounds from the Hofmann-type are demonstrated with the features observed for the developed structures determined by single crystal X-ray diffraction methods.

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Abbreviations

mma:

NMeH2

dma:

NMe2H

tma:

NMe3

mea:

NH2(CH2)2OH

en:

NH2(CH2)2NH2

pn:

NH2CHMeCH2NH2

tn:

NH2(CH2)3NH2

dabtn:

NH2(CH2)4NH2

daptn:

NH2(CH2)5NH2

dahxn:

NH2(CH2)6NH2

dahpn:

NH2(CH2)7NH2

daotn:

NH2(CH2)8NH2

danon:

NH2(CH2)9NH2

dadcn:

NH2(CH2)10NH2

mtn:

NMeH(CH2)3NH2

dmtn:

NMe2(CH2)3NH2

detn:

NEt2(CH2)3NH2

temtn:

NMe2(CH2)3NMe2

dien:

NH2(CH2)2NH(CH2)2NH2

pXdam:

p-C6H4(NH2CH2)2

rnXdam:

m-C6H4(NH2CH2)2

py:

C5H5N pyridine

ampy:

NH2C5H4N aminopyridine

Clpy:

CIC5H4N chloropyridine

Mepy:

MeC5H4N methylpyridine

dmpy:

Me2C5H3N dimethylpyridine

bpy:

NC5H4C5H4N bipyridine

quin:

C7H9N quinoline

iquin:

iso-C7H9N isoquinoline

qxln:

C8H6N2 quinoxaline

Pe:

C5H11-pentyl imH: C3N2H4 imidazole

pyrz:

N(CHCH)2N pyrazine

Mequin:

MeC7H8N methylquinoline

bppn:

C13H14N2 1,3-bis(4-pyridyl)propane

bpb:

C14H8N2 1,4-bis(4-pyridyl)butadiyne

N-Meim:

C3N2H3Me N-methylimidazole

2-MeimH:

C3N2H3Me 2-methylimidazole

dmf:

HOCNMe2 dimethylformamide

hmta:

C6H12N4 hexamethylenetetramine

o-phen:

C12H8N2 1,10-phenanthroline

den:

HN(CH2CH2)2NH piperazine

morph:

HN(CH2CH2)2O morpholine

ten:

N(CH2CH2)3N 1,4-diazabicyclo[2.2.2]octane

ameden:

NH2(CH2)2N(CH2CH2)2NH N-(2-aminoethyl)piperazine

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  1. Department of Chemistry, College of Arts and Sciences, The University of Tokyo, Komaba, Meguro, 153, Tokyo, Japan

    Toschitake Iwamoto

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Iwamoto, T. Past, present and future of the clathrate inclusion compounds built of cyanometallate hosts. J Incl Phenom Macrocycl Chem 24, 61–132 (1996). https://doi.org/10.1007/BF01053426

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