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Determination of carbamate pesticides and some urea pesticides after derivatization with acetic anhydride by means of GC-MSD

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Summary

A simple method for the determination of several thermolabile carbamate and urea pesticides as acetyl derivatives by means of capillary gas chromatography is described. 10 carbamate and 6 urea pesticides yielded thermostable derivatives which can easily be analysed by GC-MSD at the relevant residue levels as demonstrated with food samples. The method was designed to be used in addition to a popular multimethod (S19 — DFG Pesticide Commission).

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Authors and Affiliations

  1. Institute of Food Chemistry, Technical University of Berlin, Gustav-Meyer-Allee 25, W-1000, Berlin 65, Federal Republic of Germany

    H. -J. Stan & P. Klaffenbach

Authors
  1. H. -J. Stan
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  2. P. Klaffenbach
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Stan, H.J., Klaffenbach, P. Determination of carbamate pesticides and some urea pesticides after derivatization with acetic anhydride by means of GC-MSD. Fresenius J Anal Chem 339, 151–157 (1991). https://doi.org/10.1007/BF00324402

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  • DOI: https://doi.org/10.1007/BF00324402

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