Abstract
29Si Nuclear Magnetic Resonance was used to analyse silicate polymerization in relation with the kinetic control of the curing process. Controlled Rate Thermal Analysis (CRTA) was applied to the monitoring of the thermal curing of a Reactive Powder Concrete. Heating could be adjusted so as to keep the rate of gas evolution constant and in dynamic equlibrium at a pre-established pressure or to be blunt and generating local hydrothermal vapor pressures inside of the sample. Different solid-state transformation states were detected and analysed by 29Si Nuclear Magnetic Resonance spectrometry, by X Ray Diffraction and by Fourier Transformed Infrared spectrometry. These results could be used to control hydrates crystallinity.
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Faugère, MP., Crespin, M., Dion, P., Bergaya, F., Feylessoufi, A., Van Damme, H. (1998). Influence of Heat Treatment Kinetics on Calcium Silicate Hydrates Phase Evolution. In: Colombet, P., Zanni, H., Grimmer, AR., Sozzani, P. (eds) Nuclear Magnetic Resonance Spectroscopy of Cement-Based Materials. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-80432-8_16
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DOI: https://doi.org/10.1007/978-3-642-80432-8_16
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