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Facile Preparation of ZIF-8 MOF Coated Mesoporous Magnetic Nanoarticles to Provide a Magnetic Solid Phase Extraction Platform

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Abstract

In this work, zeolitic imidazolate framework (ZIF-8) coated mesoporous magnetic nanoparticles (Fe3O4@PDA@mSiO2@ZIF-8) were prepared through a facile and efficient strategy and used as a magnetic solid phase extraction platform for phthalates detection. Polydopamine (PDA) not only provides a hydrophilic layer, but also possesses π electrons for aromatic compounds recognition; mSiO2 endows the nanoparticles with large surface area and regular channels, which facilitates the rapid transport of phthalates. The prepared Fe3O4@PDA@mSiO2@ZIF-8 with imposed properties showed ultrahigh efficiency and reusability for phthalates determination in human plasma samples. The linearity range was 50–8000 ng/mL, limits of detection were between 50–80 ng/mL, the intra-day RSDs were lower than 4.8%, inter-day RSDs were lower than 6.7%, the recoveries ranged from 90 to 107%. The new prepared nanoparticles displayed potential performance for aromatic compounds detection.

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Funding

This work is sponsored by Ningbo Natural Science Foundation (2018A610279), the Research Funds of NBU (XYL18025) and the K. C. Wong Magna Fund in Ningbo University.

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Authors and Affiliations

  1. School of Materials Science and Chemical Engineering, Institute of Mass Spectrometry, Ningbo University, 315211, Ningbo, China

    Baichun Wang, Bin Liu & Yinghua Yan

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  1. Baichun Wang
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  2. Bin Liu
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  3. Yinghua Yan
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Correspondence to Yinghua Yan.

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Wang, B., Liu, B. & Yan, Y. Facile Preparation of ZIF-8 MOF Coated Mesoporous Magnetic Nanoarticles to Provide a Magnetic Solid Phase Extraction Platform. J Anal Chem 76, 430–441 (2021). https://doi.org/10.1134/S1061934821040110

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