Abstract
Adducts of tellurium(IV) 3,6-di-tert-butyl catecholate (Te(Cat36)2) with 1,2-dimethoxyethane (Dme), bis(2-methoxy)ethyl ether (diglyme), and crown ether 18-crown-6 (18c6) ([Te(Cat36)2(Dme)]2 (I), [Te(Cat36)2(diglyme)] (II), and [Te2(Cat36)4(18c6)] (III), respectively) are synthesized and characterized by X-ray diffraction (XRD) (CIF files CCDC nos. 2208717 (I), 2208718 (II), and 2208719 (III)). The complexes are also characterized by NMR (1H, 125Te) and IR spectroscopy.
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ACKNOWLEDGMENTS
The author is grateful to the Center for Collective Use of the Nikolaev Institute of Inorganic Chemistry (Siberian Branch, Russian Academy of Sciences) and Dr. T.S. Sukhikh for the presented XRD data and to N.B. Kompan’kov for NMR spectra recording.
Funding
This work was supported by the Ministry of Science and Higher Education of the Russian Federation, project no. 121031700313-8.
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Translated by E. Yablonskaya
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This article is prepared for the memorial issue in tribute to the Corresponding Member of the Russian Academy of Sciences K.Yu. Zhizhin on his 50th birthday.
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Petrov, P.A. Adducts of Sterically Hindered Tellurium Catecholate with Ethers. Russ J Coord Chem 49, 357–362 (2023). https://doi.org/10.1134/S1070328423600262
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DOI: https://doi.org/10.1134/S1070328423600262