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Synthesis of 3,4,4'- and 2',3,4-Triaminodiphenyl Ethers

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Abstract

Procedures were developed for preparing 3,4,4'- and 2',3,4-triaminodiphenyl ethers by the reaction of 4-acetylaminophenol with, respectively, 4-nitro- or 2-nitrochlorobenzene, followed by nitration of the resulting 4-acetylamino-4'- or -2'-nitrodiphenyl ether, hydrolysis of the product, 4-acetylamino-3,4'- or -2',3-dinitrodiphenyl ether, and reduction of 4-amino-3,4'- or -2'-3-dinitrodiphenyl ether.

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Authors and Affiliations

  1. Research and Technological Institute of Herbicides and Plant Growth Regulators, Academy of Sciences of Bashkortostan, Ufa, Bashkortostan, Russia

    V. S. Pilyugin, A. N. Mikhailyuk, G. V. Kiseleva, S. L. Kuznetsova, G. E. Chikisheva & V. M. Kosareva

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  1. V. S. Pilyugin
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  2. A. N. Mikhailyuk
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  3. G. V. Kiseleva
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  4. S. L. Kuznetsova
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  5. G. E. Chikisheva
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  6. V. M. Kosareva
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Pilyugin, V.S., Mikhailyuk, A.N., Kiseleva, G.V. et al. Synthesis of 3,4,4'- and 2',3,4-Triaminodiphenyl Ethers. Russian Journal of General Chemistry 73, 1105–1109 (2003). https://doi.org/10.1023/B:RUGC.0000007620.98209.c6

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  • DOI: https://doi.org/10.1023/B:RUGC.0000007620.98209.c6

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