Abstract
Using thermogravimetric analyses as well as isothermal gravimetric measurements, the thermal stability of the iron(III) nitrate nanohydrate has been determined. Several decomposition stages are the result of melting, evaporation and hydrolysis processes occurring in the salt—water system in the temperature range of 20–400°C. Some of the intermediates and the final product (α-Fe2O3) are characterized by means of chemical analyses, X-ray diffraction patterns and IR spectra.
Similar content being viewed by others
References
F. Paulik, Special Trends in Thermal Analysis, Wiley and Sons, Chichester 1995, p. 116.
F. A. Cotton and G. Wilkinson, Advanced Inorganic Chemistry, Wiley and Sons, New York 1980, p.757.
R. Ripan and I. Ceteanu, Neorganiczeskaja Chimija, t.2, Izd. Mir, Moskwa 1972, p. 479.
K. Wieczorek-Ciurowa and A. J. Kozak, Calorimetry, Experimental Thermodynamics and Thermal Analysis Conf. (CETTA.97) Sept. 8.13, 1997, Zakopane, Poland, Abstracts, S2/P12, p. 87.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Wieczorek-Ciurowa, K., Kozak, A.J. The Thermal Decomposition of Fe(NO3)3·9H2O. Journal of Thermal Analysis and Calorimetry 58, 647–651 (1999). https://doi.org/10.1023/A:1010112814013
Issue Date:
DOI: https://doi.org/10.1023/A:1010112814013