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Precision additive manufacturing of NiTi shape memory parts using micro-laser powder bed fusion

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Abstract

Nickel–titanium (NiTi) is a promising alloy for biomedical applications due to its unique combination of functional properties such as shape memory effect, superelasticity behavior and biocompatibility. In particular, additive manufacturing of complex NiTi parts containing micro features has received increased attention in bone tissue engineering. Micro-scale additive manufacturing using powder bed techniques such as laser powder bed fusion raises the need to develop new regimes of process parameters. In this research, micro-laser powder bed fusion (µLPBF) was served to fabricate single-phase austenitic nickel-titanium dense and porous materials. The focus of the first part of this study was on the phase transformation behaviour of µLPBF-built NiTi before and after various heat treatment cycles. Investigations revealed that post process age hardening heat treatment has a significant effect on phase transformation temperatures of µLPBF-built NiTi. In the second part of this study, a new strategy was employed to decrease the deviation of NiTi lattice structures with respect to the predesigned models. Results showed that precision additive manufacturing of single-phase NiTi is feasible through applying different µLPBF process parameters for border and hatching areas. With respect to nominal geometrical models, 13% and 24% deviations of pore diameter were calculated in NiTi lattice structures containing 580 µm and 380 µm pores, respectively.

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Notes

  1. Electrode Induction Gas Atomization.

Abbreviations

E :

Input energy density (J/mm3)

P :

Laser power (W)

V :

Scanning speed (mm/s)

dh :

Hatching distance (mm)

t :

Layer thickness (mm)

Ra :

Roughness (µm)

d :

Laser spot diameter (mm)

r 0 :

Beam radius (d/2)

r :

Radial position

E el :

Elastic modulus (GPa)

σ y :

Yield strength (MPa)

K :

Thermal conductivity (W/cm K)

S :

Standard error (µm)

D n :

Nominal pore diameter (µm)

D a :

As-built pore diameter (µm)

n :

Number of measurements

References

  1. Buehler WJ, Gilfrich JV, Wiley RC (1963) Effect of low-temperature phase changes on the mechanical properties of alloys near composition TiNi. J Appl Phys 34:1475

    Article  Google Scholar 

  2. Haberland C et al (2014) On the development of high quality NiTi shape memory and pseudoelastic parts by additive manufacturing. Smart Mater Struct 23:104002

    Article  Google Scholar 

  3. Elahinia M et al (2016) Fabrication of NiTi through additive manufacturing: a review. Prog Mater Sci 83:630–663

    Article  Google Scholar 

  4. Dadbakhsh S et al (2016) Laser additive manufacturing of bulk and porous shape-memory NiTi alloys: From processes to potential biomedical applications. MRS Bull 41:765

    Article  Google Scholar 

  5. Jani JM, Leary M, Subic A, Gibson MA (2014) A review of shape memory alloy research, applications and opportunities. Mater Des 56:1078–1113

    Article  Google Scholar 

  6. Elahinia MH et al (2012) Manufacturing and processing of NiTi implants: a review. Prog Mater Sci 57:911–946

    Article  Google Scholar 

  7. Haberland C et al (2013) Additive Manufacturing of Shape Memory Devices and Pseudoelastic Components. Proc ASME Conf Smart Mater Adapt Struct Intel Syst 1:V001T01A005

    Google Scholar 

  8. Khademzadeh S et al (2018) Precision additive manufacturing of NiTi parts using micro direct metal deposition. Int J Adv Man Tech 96:3729–3736

    Article  Google Scholar 

  9. Bormann T et al (2014) Microstructure of selective laser melted nickel–titanium. Mater Charact 94:189–202

    Article  Google Scholar 

  10. Khademzadeh S et al (2020) Quality enhancement of microstructure and surface topography of NiTi parts produced by laser powder bed fusion. CIRP J M Sci Tech 31:575

    Article  Google Scholar 

  11. Smith G (2012) Chapter 10—multiple regression. In: Smith G (ed) Essential statistics, regression, and econometrics. Academic Press, New York, p 297

    Chapter  Google Scholar 

  12. Bai S et al (2019) The effects of selective laser melting process parameters on relative density of the AlSi10Mg parts and suitable procedures of the Archimedes method. Appl Sci 9:583

    Article  Google Scholar 

  13. Steen W (2010) Laser material processing. Springer-Verlag, London

    Book  Google Scholar 

  14. Dadbakhsh S et al (2014) Texture and anisotropy in selective laser melting of NiTi alloy. Adv Eng Mater 16:1140

    Article  Google Scholar 

  15. Saedi S et al (2017) Texture, aging, and superelasticity of selective laser melting fabricated Ni-rich NiTi alloys. Mater Sci Eng A 686:1

    Article  Google Scholar 

  16. Shishkovsky I et al (2012) Direct Selective Laser Melting of Nitinol Powder. Phys Proc 39:447

  17. Morgan N (2004) Medical shape memory alloy applications—the market and its products. Mater Sci Eng A 2(378):16

    Article  Google Scholar 

  18. ShayestehMoghaddam N et al (2019) Achieving superelasticity in additively manufactured NiTi in compression without post-process heat treatment. Sci Rep 9:41

    Article  Google Scholar 

  19. Guan K et al (2013) Effects of processing parameters on tensile properties of selective laser melted 304 stainless steel. Mater Design 50:581

    Article  Google Scholar 

  20. Ma J et al (2017) Spatial control of functional response in 4D-printed active metallic structures. Sci Rep 7:46707

    Article  Google Scholar 

  21. Faulkner MG et al (2000) Experimental determination of thermal and electrical properties of Ni–Ti shape memory wires. Smart Mater Struct 9:632

    Article  Google Scholar 

  22. Tanzi MC et al (2019) Chapter 4—biomaterials and applications, foundations of biomaterials engineering. Academic Press, New York, p 199 (ISBN 9780081010341)

    Book  Google Scholar 

  23. Abbasi-Chianeh V et al (2011) Influence of applying external stress during aging on martensitic transformation and the superelastic behavior of a Ni-rich NiTi alloy. Mater Sci Eng A 528:5060

    Article  Google Scholar 

  24. Prokofiev EA et al (2010) Suppression of Ni4Ti3 precipitation by grain size refinement in Ni-rich NiTi shape memory alloys. Adv Eng Mater 12:747

  25. Abbasi-Chianeh V et al (2013) The effect of post-deformation aging on superelastic properties of Ni50.9Ti thin wires attaining micro and nano-substructure. J Alloys Comp 563:44

    Article  Google Scholar 

  26. Allafi JK et al (2002) The mechanism of multistage martensitic transformations in aged Ni-rich NiTi shape memory alloys. Acta Mater 50:793

    Article  Google Scholar 

  27. Eggeler G et al (2005) On the effect of aging on martensitic transformations in Ni-rich NiTi shape memory alloy. Smart Mater Struct 14(5):186

  28. Otsuka K (2005) Physical Metallurgy of Ti-Ni-Based Shape Memory Alloys. Prog Mater Sci 50(5):511

  29. Xue L et al (2021) Controlling martensitic transformation characteristics in defect-free NiTi shape memory alloys fabricated using laser powder bed fusion and a process optimization framework. Acta Mater 215:117017

    Article  Google Scholar 

  30. Khademzadeh S et al (2018) Textural Evolution During Micro Direct Metal Deposition of NiTi Alloy. Met Mater Int 24(4):869–876

    Article  Google Scholar 

  31. Saedi S et al (2016) The influence of heat treatment on the thermomechanical response of Ni-rich NiTi alloys manufactured by selective laser melting. J Alloys Comp 677:204

    Article  Google Scholar 

  32. Li G et al (2016) In vitro and in vivo study of additive manufactured porous Ti6Al4V scaffolds for repairing bone defects. Sci Rep 6:34072

    Article  Google Scholar 

  33. Hollander DA et al (2006) Structural, mechanical and in vitro characterization of individually structured Ti–6Al–4V produced by direct laser forming. Biomaterials 27:955

    Article  Google Scholar 

  34. Behera D et al (2021) Current Challenges and Potential Directions towards Precision Microscale Additive Manufacturing - Part IV: Future Perspectives. Precision Eng 68:197–205

    Article  Google Scholar 

  35. Vilardell AM et al (2021) Mechanical behavior of in-situ alloyed Ti6Al4V(ELI)-3 at.% Cu lattice structures manufactured by laser powder bed fusion and designed for implant applications. J Mech Behav Biomed Mater 113:104–130

    Article  Google Scholar 

  36. Guo Q et al (2019) In-situ characterization and quantification of melt pool variation under constant input energy density in laser powder bed fusion additive manufacturing process. Addit Manuf 28:600

    Google Scholar 

  37. Tan C et al (2019) Laser powder bed fusion of Ti-rich TiNi lattice structures: process optimisation, geometrical integrity, and phase transformations. Int J Mach Tool Manu 141:19–29

    Article  Google Scholar 

Download references

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Correspondence to Saeed Khademzadeh.

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Khademzadeh, S. Precision additive manufacturing of NiTi shape memory parts using micro-laser powder bed fusion. Prog Addit Manuf 7, 419–432 (2022). https://doi.org/10.1007/s40964-021-00239-6

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