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Synthesis and characterization of micro-meso structure NaY zeolite in the presence of Nano-ZnO as a guest molecule

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Abstract

In this work, NaY zeolite/ZnO nanocomposites with different amounts of ZnO were prepared. The nanocomposites were characterized by different methods such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy, scanning electron microscope, Energy-Dispersive X-ray analysis, Diffuse reflectance spectroscopy (DRS) surface area (BET), NH3-TPD, Fluorescence microscopy and thermal gravimetric analysis. The results of BET confirmed the micro-meso structure of NaY zeolite in which low angle XRD shows that mesophase is not completely ordered in the composite. DRS result shows the decreasing band gap in the ZnO. In addition, Si/Al ratio decreasing to lower than two which increasing in the acidity confirmed by NH3-TPD. Therefore, can be said, a good zeolitic photocatalyst with high acidity and micro-meso structure was prepared in the mild condition, which was useful for degradation of the pollution in out coming works.

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Acknowledgement

Thanks to the Iranian Nanotechnology Innovation Council, the Research Council of Arak University, Center of Excellence in the Chemistry Department of Arak University and zeolite and porous materials committee of Iranian Chemical Society for supporting of this work.

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Authors and Affiliations

  1. Department of Natural Resources and Environment, Science and Research Branch, Islamic Azad University, Tehran, Iran

    Leili Meighani

  2. Department of Chemistry, Faculty of Science, Arak University, 38156-8-8349, Arak, Iran

    Mojgan Zendehdel

  3. Department of Physics and Earth Sciences, University of Ferrara, Via G. Saragat 1, 44122, Ferrara, Italy

    Giuseppe Cruciani

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  1. Leili Meighani
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  2. Mojgan Zendehdel
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  3. Giuseppe Cruciani
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Correspondence to Mojgan Zendehdel.

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Meighani, L., Zendehdel, M. & Cruciani, G. Synthesis and characterization of micro-meso structure NaY zeolite in the presence of Nano-ZnO as a guest molecule. J IRAN CHEM SOC 18, 2873–2881 (2021). https://doi.org/10.1007/s13738-021-02240-w

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  • DOI: https://doi.org/10.1007/s13738-021-02240-w

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