Skip to main content
Log in

Abrupt Casting Failures Due to Sub Entry Nozzle Clogging in Calcium Treated Aluminum Killed Steel

  • Technical Article---peer-reviewed
  • Published:
Journal of Failure Analysis and Prevention Aims and scope Submit manuscript

Abstract

Clogging of sub entry nozzle is a recurrent problem during continuous casting of low carbon aluminum deoxidized steel. Newly modernized SMS shop, producing mainly low carbon aluminum deoxidized steel through BOF-Twin LF-CC route was facing a major issue of nozzle clogging leading to abrupt abortion of sequence casting. The incidences of SEN clogging were very high leading to loss of shop productivity. Within a span of one month around 28 cases of casting abortion were reported due SEN clogging. Casting was getting stopped in 3–4 heat sequence even after calcium treatment practice was adopted in each heat. The process of steelmaking was studied in detail to find out the root cause of nozzle clogging. It was found that dendritic clusters of alumina originating as a result of deoxidation of steel and reoxidation of aluminum during secondary refining was probably causing SEN clogging. It was also found that optimization of Ca treatment practice was required for successful continuous casting of an aluminum-killed steel. The paper elaborates the technical issues faced related to clogging of SEN in a newly installed high speed single strand slab caster during continuous casting of low carbon steel deoxidized with aluminum. The paper covers the essential steps required to identify the root cause of nozzle clogging and various process interventions essential to eliminate the SEN clogging issues and streamline the production of low carbon aluminum-killed steel in higher sequence lengths.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17
Fig. 18
Fig. 19
Fig. 20

Similar content being viewed by others

References

  1. World Steel Association, “World Steel in Figures”, www.worldsteel.org, (2022); 10–11. https://worldsteel.org/wp-content/uploads/World-Steel-in-Figures2022.pdf

  2. Y. Vermeulen, B. Coletti, P. Wollants, B. Blanpain, F. Haers, Clogging in submerged entry nozzles. Steel research. 71(10), 391–395 (2000). https://doi.org/10.1002/srin.200001334

    Article  CAS  Google Scholar 

  3. A. Sen, B. Prasad, J. K. Sahu, and J. N. Tiwari. Designing of sub-entry nozzle for casting defect-free steel. in IOP Conference Series: Materials Science and Engineering, vol. 75, no. 1 (IOP Publishing, 2015), p. 012006. https://doi.org/10.1088/1757-899X/75/1/012006

  4. F. Tehovnik, J. Burja, B. Arh, M. Knap. Submerged entry nozzle clogging during continuous casting of Al-killed steel. Metalurgija 54(2), 371–374 (2015).https://hrcak.srce.hr/128965

  5. A. Kamaraj, R. Saravanakumar, M. Rajaguru. State of the art control measures for aluminium fade and SEN clogging during steelmaking operations. in IOP Conference Series: Materials Science and Engineering, vol. 314, no. 1, (IOP Publishing, 2018) p. 012022. https://doi.org/10.1088/1757-899X/314/1/012022

  6. E. B. Pretorius, H. G. Oltmann, B. T. Schart. An overview of steel cleanliness from an industry perspective. in AISTech proceedings, (2013), pp. 6–9. https://digital.library.aist.org/pages/PR-PM0315-7

  7. C. Liu, X. Gao, S. Ueda, M. Guo, S.-y. Kitamura, Composition changes of inclusions by reaction with slag and refractory: a review. in ISIJ International (2020): ISIJINT-2019. https://doi.org/10.2355/isijinternational.ISIJINT-2019-695

  8. S. Kumar, K.K. Keshari, A. Gupta, A. Prasad, V. Kumar, B. Mishra, K. Abhishek, Improvement in castability of Al-killed steel in billet casters by process optimization. Trans. Indian Inst. Metals. 73(1), 243–249 (2020). https://doi.org/10.1007/s12666-019-01828-4

    Article  CAS  Google Scholar 

  9. A.W. Cramb, High purity, low residual and clean steels. in Impurities in Engineering Materials, (Routledge, 2017) pp. 49–89. https://doi.org/10.1201/9780203751190-4

  10. L. Zhang, Q. Ren, H. Duan, Y. Ren, W. Chen, G. Cheng, W. Yang, S. Sridhar, Modelling of non-metallic inclusions in steel. Mineral Process. Extract. Metall. 129(2), 184–206 (2020). https://doi.org/10.1080/25726641.2020.1738087

    Article  CAS  Google Scholar 

  11. J. Nakashima, T.O.H. Takehiko, Improvement of continuously cast slabs by decreasing nonmetallic inclusions. Nippon Steel Tech. Rep. 104 (2013). https://www.nipponsteel.com/en/tech/report/nsc/pdf/104-08.pdf

  12. L. Zhang, B.G. Thomas, X. Wang, K. Cai. Evaluation and control of steel cleanliness-review. in Steelmaking Conference Proceedings, vol. 85, (2002), pp. 431–452. http://ccc.illinois.edu/PDF%20Files/Publications/02_Steel%20Cleanliness%20review%20ISS%202002%20pp431-452.pdf

  13. L.A. Moiseeva, B.P. Moiseev, Composition, structure, and sources of exogenous inclusions in steel. Steel Transl. 37(7), 607–613 (2007). https://doi.org/10.3103/S0967091207070133

    Article  Google Scholar 

  14. M. Burty, C. Louis, P. Dunand, P. Osmont, F. Ruby-Meyer, M. Nadif, F. Penet, T. Isono, E. Takeuchi, T. Toh, Methodology of steel cleanliness assessment. Revue de Métallurgie. 97(6), 775–782 (2000). https://doi.org/10.1051/metal/200097060775

    Article  CAS  Google Scholar 

  15. L. Zhang, B.G. Thomas, State of the art in evaluation and control of steel cleanliness. ISIJ Int. 43(3), 271–291 (2003). https://doi.org/10.2355/isijinternational.43.271

    Article  CAS  Google Scholar 

  16. S. Abraham, R. Bodnar, J. Raines, Y. Wang, Inclusion engineering and metallurgy of calcium treatment. J. Iron. Steel Res. Int. 25(2), 133–145 (2018). https://doi.org/10.1007/s42243-018-0017-3

    Article  Google Scholar 

  17. K. Ahlborg, Seven ways to shut down the caster manipulating inclusion composition to defeat the steel flow control mechanism on the tundish. in 6th Ironmaking Conference, pp. 1119–1127. 2001.

  18. L. Zhang, B. Rietow, B.G. Thomas, K. Eakin, Large inclusions in plain-carbon steel ingots cast by bottom teeming. ISIJ Int. 46(5), 670–679 (2006). https://doi.org/10.2355/isijinternational.46.670

    Article  CAS  Google Scholar 

  19. Y. Vermeulen, B. Coletti, B. Blanpain, P. Wollants, J. Vleugels, Material evaluation to prevent nozzle clogging during continuous casting of Al killed steels. ISIJ Int. 42(11), 1234–1240 (2002). https://doi.org/10.2355/isijinternational.42.1234

    Article  CAS  Google Scholar 

  20. K. Chen, D. Wang, D. Hou, Q. Tianpeng, J. Tian, H. Wang, Effect of interfacial properties on agglomeration of inclusions in molten steels. ISIJ Int. 59(10), 1735–1743 (2019). https://doi.org/10.2355/isijinternational.ISIJINT-2019-053

    Article  CAS  Google Scholar 

  21. Y. Jun, X.-H. Wang, M. Jiang, W.-J. Wang, Effect of calcium treatment on non-metallic inclusions in ultra-low oxygen steel refined by high basicity high Al2O3 slag. J. Iron. Steel Res. Int. 18(7), 8–14 (2011). https://doi.org/10.1016/S1006-706X(11)60083-6

    Article  Google Scholar 

  22. S.K. Choudhary, A. Ghosh, Thermodynamic evaluation of formation of oxide-sulfide duplex inclusions in steel. ISIJ Int. 48(11), 1552–1559 (2008). https://doi.org/10.2355/isijinternational.48.1552

    Article  CAS  Google Scholar 

  23. J.C.S. Pires, A. Garcia, Modification of oxide inclusions present in aluminum-killed low carbon steel by addition of calcium. Rem Revista Escola de Minas. 57(3), 183–189 (2004). https://doi.org/10.1590/S0370-44672004000300008

    Article  Google Scholar 

  24. S. Kumar, K. K. Keshari, A. K. Bandhyopadhyay, A. Prasad, V. Kumar, N. Sen, K. Choudhury, R. Kumar, An innovative slag engineering approach for improving de-sulphurisation efficiency in silicon killed steels. in Recent Advances in Manufacturing Processes, (Springer, Singapore, 2022), pp. 211–228.https://doi.org/10.1007/978-981-16-3686-8_17

  25. S. Dević, Identification of hibonite-5H in the characterization of inner SEN deposits. Steel Res. Int. 77(7), 524–527 (2006). https://doi.org/10.1002/srin.200606424

    Article  Google Scholar 

Download references

Acknowledgments

For the assistance and support given throughout the completion of this work, the authors of this paper would like to express their heartfelt gratitude to the management of Steel Authority of India Limited's R & D Centre for Iron & Steel. The writers also want to express their gratitude to everyone who provided direct or indirect assistance in accomplishing the assignment.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Somnath Kumar.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Kumar, S., Keshari, K.K., Deva, A. et al. Abrupt Casting Failures Due to Sub Entry Nozzle Clogging in Calcium Treated Aluminum Killed Steel. J Fail. Anal. and Preven. 23, 221–233 (2023). https://doi.org/10.1007/s11668-022-01569-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11668-022-01569-5

Keywords

Navigation