Abstract
A solidification benchmark experiment is simulated using a three-dimensional cellular automaton—finite element solidification model. The experiment consists of a rectangular cavity containing a Sn-3 wt pct Pb alloy. The alloy is first melted and then solidified in the cavity. A dense array of thermocouples permits monitoring of temperatures in the cavity and in the heat exchangers surrounding the cavity. After solidification, the grain structure is revealed by metallography. X-ray radiography and inductively coupled plasma spectrometry are also conducted to access a distribution map of Pb, or macrosegregation map. The solidification model consists of solutions for heat, solute mass, and momentum conservations using the finite element method. It is coupled with a description of the development of grain structure using the cellular automaton method. A careful and direct comparison with experimental results is possible thanks to boundary conditions deduced from the temperature measurements, as well as a careful choice of the values of the material properties for simulation. Results show that the temperature maps and the macrosegregation map can only be approached with a three-dimensional simulation that includes the description of the grain structure.
Similar content being viewed by others
References
Beckermann C (2002) International Materials Reviews 47: 243-261.
Flemings M C, Nereo G E 1967 Transactions of the Metallurgical Society of AIME 239 1449-1461.
Flemings M C, Mehrabian R, Nereo G E 1968 Transactions of the Metallurgical Society of AIME 242 41-49.
Flemings M C, Nereo G E 1968 Transactions of the Metallurgical Society of AIME 242 50-55.
Mehrabian R, Flemings M C 1969 Transactions of the Metallurgical Society of AIME 245 2347-2348.
Mehrabian R, Keane M, Flemings M C 1970 Metallurgical Transactions 1 1209-1220.
Flemings M C, Mehrabian R, Keane M 1970 Metallurgical Transactions 1 3238-3241.
Hebditch D J, Hunt J D 1974 Metallurgical Transactions 5 1557-1564.
Lesoult G, Gandin Ch.-A., Niane N T 2003 Acta Materialia 51 5263–5283.
D.J. Hebditch: Ph.D. Thesis, University of Oxford, Oxford, 1973.
Wang X D, Fautrelle Y 2009 International Journal of Heat and Mass Transfer 52: 5624-5633.
Hachani L, Saadi B, Wang X D, Nouri A, Zaidat K, Belgacem Bouzida A, Ayouni-Derouiche L, Raimondi G, Fautrelle Y 2012 International Journal of Heat and Mass Transfer 55 1986-1996.
Gandin Ch.-A., Blaizot J, Mosbah S, Bellet M, Zimmermann G, Sturz L, Browne D J, McFadden S, Jung H, Billia B, Mangelinck N, Nguyen Thi H, Fautrelle Y, Wang X 2010 Materials Science Forum 649 189-198.
Gandin Ch.-A., Rappaz M 1997 Acta materialia 45 2187-2195
Gandin Ch.-A., Desbiolles J L, Rappaz M, Thevoz Ph 1999 Metallurgical and Materials Transactions A 30 3153-3165.
Takatani H, Gandin Ch.-A., Rappaz M 2000 Acta materialia 48 675-688
Carter P, Cox D C, Gandin Ch.-A., Reed R C 2000 Materials science and engineering A280 233-246.
Guillemot G, Gandin Ch.-A., Combeau H, Heringer R 2004 Modelling and simulation in materials science and engineering 12 545-556.
Guillemot G, Gandin Ch.-A., Combeau H 2006 ISIJ International 46 880-895.
Guillemot G, Gandin Ch.-A., Bellet M 2007 Journal of crystal growth 303 58-68
Mosbah S, Bellet M, and Ch.-A. Gandin: 2010 Metallurgical and Materials Transactions A 41 651-69.
Gandin Ch.-A. 2010 Comptes rendus physique 11 216-225.
Carozzani T, Digonnet H, Gandin Ch.-A. 2012 Modelling and Simulation in Materials Science and Engineering 20 015010.
Ni J, Beckermann C 1991 Metallurgical Transactions B 22 349-361.
J.A. Dantzig and M. Rappaz: Solidification, EPFL Press, Lausanne, CH, 2009.
Felicelli S D, Heinrich J C, Poirier D R, 1991 Metallurgical Transactions B 22: 847-859.
Felicelli S D, Heinrich J C, Poirier D R 1998 Journal of Crystal Growth 191 879-888.
Ramirez J C, Beckermann C 2003 Metallurgical and Materials Transactions A 34 1525-1536.
B. Rivaux: Ph.D. Thesis, MINES ParisTech, Paris, FR, 2011.
Sabat Da Cruz K, Mangelinck-Noël N, Gandin Ch.-A., Billia B 2011 IOP Conf. Series: Materials Science and Engineering 27 012017.
Gandin Ch.-A., Guillemot G, Appolaire B, Niane N T 2003 Materials Science and Engineering A 342 44-50.
Trivedi R, Kurz W 1994 International Materials Reviews 39 49-74.
Ben Amar M, Brener E 1993 Phys. Rev. Lett. 71 589-592.
Tourret D, Gandin Ch.-A. 2009 Acta materialia 57 2066-2079.
Tourret D, Gandin Ch.-A., Volkmann T, Herlach D M 2011 Acta Materialia 59 4665-4677.
Tourret D, Reinhart G, Gandin Ch.-A., Iles G N, Dahlborg U, Calvo-Dahlborg M, Bao C M 2011 Acta materialia 59 6658-6669
Yin H, Koster J N 2003 J. Alloys Compounds 352 197-209.
Shevchenko N, Boden, Eckert S, Gerbeth G 2012 IOP Conference Series-Materials Science and Engineering 27 012085.
Bogno A, Nguyen-Thi H, Buffet A, Reinhart G, Billia B, Mangelinck-Noël N, Bergeon N, Baruchel J, Schenk T 2011 Acta Materialia 59 4356-4365.
Mathiesen R H, Arnberg L 2005 Acta Materialia 53 947-956.
Heringer R, Gandin Ch.-A., Lesoult G, Henein H 2006 Acta Materialia 54 4427-4440.
Gandin Ch.-A. 2000 ISIJ international 40 971-979.
Gandin Ch.-A. 2000 Acta Materialia 48 2483-2501.
Martorano M A, Beckermann C, Gandin Ch.-A. 2003 Metallurgical and Materials Transactions A 34 1657-1674.
Jackson K A, Hunt J D, Uhlmann D R, Seward T P 1966 Transaction AIME 236 149-158.
Thermo-Calc: Version S, Thermo-Calc Software AB, Stockholm, SE, 2010
PBIN: Public Binary Alloys Thermodynamic Database, version 1.2. Thermo-Calc Software AB, Stockholm, SE, 2008.
Acknowledgments
This study was funded by the French National Research Agency under projects SMACS (ANR-07-BLAN-0190) and Si-X (ANR-08-HABISOL-012-04), as well as by the European Space Agency under project CETSOL (ESA-4200014313).
Author information
Authors and Affiliations
Corresponding author
Additional information
Manuscript submitted May 20, 2012.
Rights and permissions
About this article
Cite this article
Carozzani, T., Gandin, CA., Digonnet, H. et al. Direct Simulation of a Solidification Benchmark Experiment. Metall Mater Trans A 44, 873–887 (2013). https://doi.org/10.1007/s11661-012-1465-1
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11661-012-1465-1