Skip to main content
Log in

Effect of Electron Beam Treatment on the Structure, Properties and Fracture Behavior of High-Entropy Co – Cr – Fe – Mn – Ni Alloy

  • ADDITIVE TECHNOLOGIES, POWDER AND COMPOSITE MATERIALS
  • Published:
Metal Science and Heat Treatment Aims and scope

A high-entropy Co – Cr – Fe – Mn – Ni alloy with a non-equiatomic composition obtained by the method of wire arc additive manufacturing (WAAM) is studied. The stress-strain curves due to tension of the alloy are analyzed in the initial condition and after electron beam treatment. The strength and ductility parameters, the nano- and microhardness, and the tribological properties are determined as a function of the energy density of the electron beam. Analysis of the fracture surface after the electron beam treatment and of the regions of ductile fracture shows the presence of a region with a banded (lamellar) structure. The scalar dislocation density is shown to vary nonmonotonically and to attain a maximum value of about 5.5 × 1010 cm – 2 at a distance of 25 µm from the irradiated surface. The electron beam treatment lowers the strength and ductility properties of the high-entropy alloy. It is assumed that the defects produced in the surface layer under such a treatment may be responsible for lowering of the strength and ductility of the alloy.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.
Fig. 5.

Similar content being viewed by others

References

  1. E. P. George, W. A. Curtin, and C. C. Tasan, “High entropy alloys: A focused review of mechanical properties and deformation mechanisms,” Acta Mater., 188, 435 – 474 (2020).

    Article  CAS  Google Scholar 

  2. V. Shivam, J. Basu, V. K. Pandey, et al., “Alloying behaviour, thermal stability and phase evolution of quinary AlCoCrFeNi high entropy alloy,” Adv. Powder Technol., 29, 2221 – 2230 (2018).

    Article  CAS  Google Scholar 

  3. U. L. Ganesh and H. Raghavendra, “Review on the transition from conventional to muli-component-based nano-high-entropy alloys-NHEAs,” J. Therm. Anal. Calorim., 139, 207 – 216 (2020).

    Article  CAS  Google Scholar 

  4. K. A. Osintsev, V. E. Gromov, S. V. Konovalov, et al., “HEAs: structure, mechanical properties, deformation mechanisms and application,” Izv. Vysh. Uchebn. Zaved., Chern. Metall., No. 4, 1 – 8 (2021).

  5. V. E. Gromov, S. V. Konovalov, Yu. F. Ivanov, and K. A. Osintsev, “Structure and properties of high-entropy alloys,” Adv. Struct. Mater., 107, Springer (2021), 110 p.

  6. Yu. F. Ivanov, V. E. Gromov, S. V. Konovalov, and Yu. A. Shlyarov, “Evolution of structure of AlCoCrFeNi high-entropy alloy under irradiation with pulsed electron beam,” Zh. Tekh. Fiz., 91(12), 1971 – 1974 (2021).

    Google Scholar 

  7. K. Osintsev, S. Konovalov, and D. Zaguliaev, “Investigation of Co – Cr – Fe – Mn – Ni non-equiatomic high-entropy alloy fabricated by wire additive manufacturing,” Metals, 12(2), 197 (2022).

    Article  CAS  Google Scholar 

  8. K. A. Osintsev, S. V. Konovalov, V. E. Gromov, et al., “Microstructure and mechanical properties of non-equiatomic Co25.4 Cr15 Fe37.9 Mn3.5 Ni16.8 Si1.4 high-entropy alloy produced by wire-arc additive manufacturing,” Mater. Lett., 312, 131675 (2022).

    Article  CAS  Google Scholar 

  9. T. Zhang, L. Xin, F. Wu, et al., “Microstructure and mechanical properties of Fex CoCrNiMn high-entropy alloys,” J. Mater. Sci. Technol., 35(10), 2331 – 2335 (2019).

    Article  CAS  Google Scholar 

  10. B. A. Gludovats, A. Hohenwarter, D. Catoor, et al., “Fracture-resistant high-entropy alloy for cryogenic applications,” Science, 345(6201), 1153 – 1158 (2014).

    Article  Google Scholar 

  11. D. I. Proskyrovsky, V. P. Rotshtein, G. E. Ozur, et al., “Physical foundations for surface treatment of materials with low energy, high current electron beams,” Surf. Coat. Technol., 125(1 – 3), 49 – 56 (2000).

    Article  Google Scholar 

  12. S. Konovalov, Y. Ivanov, V. Gromov, and I. Panchenko, “Fatigue-induced evolution of AISI 310S steel microstructure after electron beam treatment,” Materials, 13(20), 4567 (2020).

    Article  CAS  Google Scholar 

  13. P. Lyu, T. Peng, Y. Miao, et al., “Microstructure and properties of CoCrFeNiMo0.2 high-entropy alloy enhanced by high-current pulsed electron beam,” Surf. Coat. Technol., 410, 126911 (2021).

    Article  Google Scholar 

  14. J. Cai, Y. Yao, C. Gao, et al., “Comparison of microstructure and oxidation behavior of NiCoCrAlYSi laser cladding coating before and after high-current pulsed electron beam modification,” J. Alloys Compd., 881, 160651 (2021).

    Article  CAS  Google Scholar 

  15. K. Osintsev, V. Gromov, Y. Ivanov, et al., “Evolution of structure in AlCoCrFeNi high-entropy alloy irradiated by a pulsed electron beam,” Metals, 11, 1228 (2021).

    Article  CAS  Google Scholar 

  16. N. N. Koval and Yu. F. Ivanov, “Surface nanostructuring of cermet and ceramic materials under pulsed electron beam treatment,” Izv. Vysh. Uchebn. Zaved., Fiz., No. 5, 60 – 70 (2008).

Download references

Author information

Authors and Affiliations

Authors

Additional information

Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 11, pp. 54 – 59, November, 2022.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Shlyarova, Y.A., Gromov, V.E., Konovalov, S.V. et al. Effect of Electron Beam Treatment on the Structure, Properties and Fracture Behavior of High-Entropy Co – Cr – Fe – Mn – Ni Alloy. Met Sci Heat Treat 64, 662–667 (2023). https://doi.org/10.1007/s11041-023-00868-4

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11041-023-00868-4

Keywords

Navigation