Skip to main content
SpringerLink
Log in

The characterization and preparation of core–shell structure particles of carbon-sphere@NiFe2O4@PPy as microwave absorbing materials in X band

  • Published:
Journal of Materials Science: Materials in Electronics Aims and scope Submit manuscript

Abstract

An excellent PPy/NiFe2O4/CS microwave absorbing materials with a three-layer core–shell structure, was synthesized successfully by two reaction steps of solvothermal reaction and in situ polymerization. The surface morphology, phase structure and chemical components of the composite have been characterized by a scanning electron microscope, X-ray diffraction and X-ray photoelectron spectroscope. The results suggest that the surface of CS is covered by NiFe2O4 completely and PPy wraps the obtained NiFe2O4/CS successfully. The conductivity and the saturation magnetization (Ms) of the resulting PPy/NiFe2O4/CS composites are 0.38 S/cm and 46 emu/g, respectively. The vector network analysis shows the composite performs better microwave absorbing ability than that of CS and NiFe2O4/CS. The maximum reflection loss of the composite with 1.97 mm coating thickness is −53 dB at 10.5 GHz and the bandwidth of reflection loss less than −10 dB is 3.4 GHz (8.9–12.3 GHz). This ternary composite with light weight, thin thickness and strong absorbing capacity can be an attractive candidate in the field of microwave absorption.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7

Similar content being viewed by others

References

  1. Q. Liu, Q. Cao, H. Bi, C. Liang, K. Yuan, W. She, Y. Yang, R. Che, Adv. Mater. 28, 486–490 (2016)

    Article  Google Scholar 

  2. G. Wu, Y. Cheng, Z. Wang, K. Wang, A. Feng, J. Mater. Sci. 28, 576–581 (2017)

    Google Scholar 

  3. Y. Wang, W. Zhang, X. Wu, C. Luo, Q. Wang, J. Li, L. Hu, Synth. Met. 228, 18–24 (2017)

    Article  Google Scholar 

  4. H. Wu, G. Wu, L. Wang, Powder Technol. 269, 443–451 (2015)

    Article  Google Scholar 

  5. C. Pan, K. Kou, Q. Jia, Y. Zhang, G. Wu, T. Ji, Compos. Part B 111, 83–90 (2017)

    Article  Google Scholar 

  6. H. Wu, Y. Wang, C. Zheng, J. Zhu, G. Wu, X. Li, J. Alloys Compd. 685, 8–14 (2016)

    Article  Google Scholar 

  7. H. Lv, Y. Guo, G. Wu, G. Ji, Y. Zhao, Z.J. Xu, ACS Appl. Mater. Interfaces 9, 5660–5668 (2017)

    Article  Google Scholar 

  8. G. Wu, J. Li, K. Wang, Y. Wang, C. Pan, A. Feng, J. Mater. Sci. 28, 6544–6551 (2017)

    Google Scholar 

  9. Q. Liu, X. Xu, W. Xia, R. Che, C. Chen, Q. Cao, J. He, Nanoscale 7, 1736–1743 (2015)

    Article  Google Scholar 

  10. G. Wu, Y. Cheng, F. Xiang, Z. Jia, Q. Xie, G. Wu, H. Wu, Mater. Sci. Semicond. Process. 41, 6–11 (2016)

    Article  Google Scholar 

  11. H. Xu, X. Yin, M. Zhu, M. Han, Z. Hou, X. Li, L. Zhang, L. Cheng, ACS Appl. Mater. Interfaces 9, 6332–6341 (2017)

    Article  Google Scholar 

  12. G. Wu, Y. Cheng, Q. Xie, Z. Jia, F. Xiang, H. Wu, Mater. Lett. 144, 157–160 (2015)

    Article  Google Scholar 

  13. J. Liu, R. Che, H. Chen, F. Zhang, F. Xia, Q. Wu, M. Wang, Small 8, 1214–1221 (2012)

    Article  Google Scholar 

  14. J. Liu, J. Cheng, R. Che, J. Xu, M. Liu, Z. Liu, J. Phys. Chem. C 117, 489–495 (2013)

    Article  Google Scholar 

  15. G. Wu, Y. Cheng, Y. Ren, Y. Wang, Z. Wang, H. Wu, J. Alloys Compd. 652, 346–350 (2015)

    Article  Google Scholar 

  16. Z. Peng, W. Jiang, Y. Wang, S. Zhong, J. Mater. Sci. 27, 1304–1313 (2015)

    Google Scholar 

  17. X. Ding, Y. Huang, M. Zong, Mater. Lett. 157, 285–289 (2015)

    Article  Google Scholar 

  18. X.L. Dong, X.F. Zhang, H. Huang, F. Zuo, Appl. Phys. Lett. 92, 013127 (2008)

    Article  Google Scholar 

  19. H. Wu, G. Wu, Y. Ren, L. Yang, L. Wang, X. Li, J. Mater. Chem. C 3, 7677–7690 (2015)

    Article  Google Scholar 

  20. P. Liu, Y. Huang, J. Yan, Y. Yang, Y. Zhao, ACS Appl. Mater. Interfaces 8, 5536–5546 (2016)

    Article  Google Scholar 

  21. X. Huang, J. Zhang, Z. Liu, T. Sang, B. Song, H. Zhu, C. Wong, J. Alloys Compd. 648, 1072–1075 (2015)

    Article  Google Scholar 

  22. G. Wu, Y. Cheng, K. Wang, Y. Wang, A. Feng, J. Mater. Sci. 27, 5592–5599 (2016)

    Google Scholar 

  23. M. Qiao, X. Lei, Y. Ma, L. Tian, K. Su, Q. Zhang, Ind. Eng. Chem. Res. 55, 6263–6275 (2016)

    Article  Google Scholar 

  24. X. Sun, Y. Li, Angew. Chem. 116, 607–611 (2004)

    Article  Google Scholar 

  25. G. Wu, H. Wu, K. Wang, C. Zheng, Y. Wang, A. Feng, RSC Adv. 6, 58069–58076 (2016)

    Article  Google Scholar 

  26. J. Wang, F. Ren, B. Jia, X. Liu, Solid State Commun. 150, 1141–1144 (2010)

    Article  Google Scholar 

  27. J. Wang, F. Ren, R. Yi, A. Yan, G. Qiu, X. Liu, J. Alloys Compd. 479, 791–796 (2009)

    Article  Google Scholar 

  28. G. Wu, Y. Wang, K. Wang, A. Feng, RSC Adv. 6, 102542–102548 (2016)

    Article  Google Scholar 

  29. L. Chen, H. Dai, Y. Shen, J. Bai, J. Alloys Compd. 491, L33–L38 (2010)

    Article  Google Scholar 

  30. A. Poddar, R.N. Bhowmik, A. De, P. Sen, J. Magn. Magn. Mater. 321, 2015–2020 (2009)

    Article  Google Scholar 

  31. R. Rahimi, H. Kerdari, M. Rabbani, M. Shafiee, Desalination 280, 412–418 (2011)

    Article  Google Scholar 

  32. X. Wang, H. Yan, R. Xue, S. Qi, J. Mater. Sci. 28, 519–525 (2016)

    Google Scholar 

  33. M. Han, Y. Ou, L. Deng, J. Magn. Magn. Mater. 321, 1125–1129 (2009)

    Article  Google Scholar 

  34. X. Huang, J. Zhang, M. Lai, T. Sang, J. Alloys Compd. 627, 367–373 (2015)

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Applied Chemistry, School of Natural and Applied Sciences, Northwestern Polytechnical University, Xi’an, 710072, Shaanxi, China

    Xingwei Wang, Meiyu Yang, Hongxia Yan & Shuhua Qi

Authors
  1. Xingwei Wang
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Meiyu Yang
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Hongxia Yan
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Shuhua Qi
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Shuhua Qi.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Wang, X., Yang, M., Yan, H. et al. The characterization and preparation of core–shell structure particles of carbon-sphere@NiFe2O4@PPy as microwave absorbing materials in X band. J Mater Sci: Mater Electron 28, 14988–14995 (2017). https://doi.org/10.1007/s10854-017-7372-x

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10854-017-7372-x

Search

Navigation