Abstract
The microsegregation in alloy 718 fusion zone during gas tungsten arc welding affected the aging response and the mechanical properties. The average weld cooling rate was enhanced in gas tungsten arc (GTA) welding process by employing liquid nitrogen during the process. The combination of in-process and external cooling methods reduced the microsegregation of Nb in alloy 718 fusion zone. Detailed characterization of the weld microstructures in the as-welded and the direct aged conditions was conducted. The dendritic structure have been refined to a level of 10-20 μm dendrite arm spacing and Laves particle sizes ranging from 0.04 to 1.43 μm due to the enhanced weld cooling rate. Similarly, the average Laves volume fraction was reduced from 45 to 0.1 % when compared to the conventionally cooled GTA welding process. The microsegregation was quantified through the computed solidification time through the DSC analysis and the volume fraction of the eutectic phases. It was found that the solidification time was reduced significantly from 2.499 s to as low as 0.36 s with the liquid nitrogen-cooled GTA welding process. The microhardness survey revealed an improved aging response of the fusion zone.
Similar content being viewed by others
Abbreviations
- CCAR:
-
Constant current argon
- CCPAR:
-
Compound current argon
- CCHE:
-
Constant current helium
- CCPHE:
-
Compound current helium
- EBW:
-
Electron beam welding
- AW:
-
As welded
- DA:
-
Direct aged
- STR:
-
Solidification temperature range
- t s :
-
Solidification time
- DTA:
-
Differential thermal analysis
- DSC:
-
Differential scanning calorimetry
- GTAW:
-
Gas tungsten arc welding
- Act:
-
Actual
- Nom:
-
Nominal
References
Böttger B, Grafe U, and MaD, (2000) Prediction and measurement of microsegregation and microstructural evolution in directionally solidified superalloys. In: Pollock CM, Kissinger RD, Bowman RR, Green KA, McLean M, Olson S, Schirra JJ (Eds.) Proceedings of Superalloys 2000, The Minerals, Metals & Materials Society, 2000, 313–322.
Radhakrishna C, Prasad Rao K, Srinivas S (1995) Laves phase in superalloy 718 weld metals. J Mater Sci Lett 14:1810–1812
Janaki Ram GD, Prasad RK, Madhusudhan Reddy G (2004) Control of Laves phase in Inconel 718 GTA welds with current pulsing. Sci Technol Weld Join 5(9):390–398
Janaki Ram GD, Venugopal Reddy A, Madhusudhan Reddy G, Prasad Rao K (2005) Improvement in stress rupture properties of Inconel 718 gas tungsten arc welds using current pulsing. J Mater Sci 40:1497–1500
Manikandan SGK, Sivakumar D, Prasad Rao K, Kamaraj M (2012) Control of Laves phase in Inconel 718 weldments. Mater Sci Forum 710:614–619
Manikandan SGK, Sivakumar D, Prasad Rao K, Kamaraj M (2014) Effect of weld cooling rate on Laves formation in Inconel 718 fusion zone. J Mater Process Technol 214(2):358–364. doi:10.016/j.jmatprotec.2013.09.006
Manikandan SGK, Sivakumar D, Karthikesan D, Prasad Rao K, Kamaraj M (2013) Frequency modulation effect on the solidification of alloy 718 fusion zone. Process Mater Sci Technol 1:1375–1361
Madhusudhana Reddy G, Srinivasa Murthy CV, Srinivasa Rao K, Prasad Rao K (2009) Improvement of mechanical properties of Inconel 718 electron beam welds—influence of welding techniques and post weld heat treatment. Int J Adv Manuf Technol 43:671–680
Amuda MOH, Mridha S (2013) Grain refinement and hardness distribution in cryogenically cooled ferritic stainless steel welds. Mater Des 47:365–371. doi:10.1016/j.matdes.2012.12.008
Gabzdyl J (2002) Cryogenic weld cooling. Ind Laser Solut 17(5):25–29
Needham JC (1972) Joining of metals by the pulsed TIG process—a solution to manage welding problems. Aus Weld J 16(5).
Boughton P (1971) High precision pulsed TIG welding. Paper no-10. Proc. Conf. on Adv. Welding Processes. Weld. Intl.
Manikandan SGK, Sivakumar D, Prasad Rao K, Kamaraj M (2015) Laves phase in alloy 718 fusion zone—microscopic and calorimetric studies. Mater Charact 100:192–206
Lee HT, Jeng SL, Kuo TY (2003) The microstructure and fracture behavior of dissimilar alloy 690-SUS304L joint with various Nb addition. Metall Mater Trans A 34A:1097–1105
Jeng SL, Lee HT, Kuo TY, Chung CL, Huang JY (2015) The effects of Mn and Nb on the microstructure and mechanical properties of alloy 152 welds. Mater Des 87:920–931
Kuo TY, Lee HT, Tu CC (2003) An evaluation of the effects of Nb and Mn addition on the nickel base weldments. Sci Technol Weld Join 8(1):39–48
Brandao WJ, Bueno VTL, Marques PV, Modenesi PJ (1992) Avoiding problems when welding AISI 430 ferritic stainless steel. Weld Int 6:713–716
Idowu OA, Ojo OA, Chaturvedi MC (2007) Effect of heat input on heat affected zone cracking in laser welded ATI Allvac 718Plus superalloy. Mater Sci Engg 454–455(25):389–397
Vishwakarma KR, Richards NL, Chaturvedi MC (2008) Microstructural analysis of fusion and heat affected zones in electron beam welded ALLVAC® 718PLUS™ superalloy. Mater Sci Engg A 480(1–2):517–528
Murata Y, Morinaga M, Yukawa N, Ogawa H and Kato M. (1994) Solidification structures of Inconel 718 with microalloying elements, In: E.A. Loria (Ed.) Superalloys 718,625,706 and Various Derivatives, The Minerals, Metals & Materials Society, 81–88.
Cieslak MJ, Headley TJ, Knorovsky GA, Romig AD Jr, Kollie T (1990) A comparison of the solidification of Incoloy 909 and Inconel 718. Metall Trans 21A:479–488
Beckers JL (1988) Study of solidification features of nickel base superalloys in relation with composition. Metall Trans A 19:2333–2340
Fusner E (2013) Elemental effects of Fe, Mo, C and Hf (or Nb) on solidification behavior, microstructure and weldability of high Cr nickel base filler metals. MS dissertation, Ohio State University.
Odabaşi A, Ünlü N, Göller G, Eruslu MN (2010) A study on laser beam welding (LBW) technique: effect of heat input on the microstructural evolution of superalloy Inconel 718. Metall Mater Trans A 41A:2357–2365
Manikandan SGK, Sivakumar D, Kamaraj M (2015) Phase transformation studies in alloy 718 fusion zone welded using high Mo filler metal. Symposium in the recent trends in the plasticity and phase transformations. Ruhr University, Bochum
Rocha OL, Siqueira CA, Garcia A (2003) Heat flow parameters affecting dendrite spacings during unsteady state solidification of Sn–Pb and Al–Cu alloys. Metall Mater Trans A 34(4):995–1006
Flemings MC (1974) Solidification processing. Mc-Graw Hill Inc., Ch. 10, 330.
Kurokawa S, Ruzzante E, Hey AM, Dyment F (1983) Diffusion of Nb in Fe and Fe alloys. Metal Sci 17:433–438
Chou TC, Nieh TG (1991) Explosive anisotropic grain growth of δ-NiMo by solid state diffusion. Appl Phys Lett 58(23):2642
Knorovsky GA, Cieslak MJ, Headley TJ, Romig AD Jr, Hammetter WF (1989) Inconel 718: a solidification diagram. Metall Mater Trans A 20(10):2149–2158
Sivaprasad K, Ganesh Sundararaman S (2008) Influence of weld cooling rate on microstructure and mechanical properties of alloy 718 weldments. Metall Mater Trans A 39(9):2115–2127
Mukherjee P, Sarkar A, Barat A, Jayakumar T, Mahadevan S, Sanjay RK (2008) Lattice misfit measurement in Inconel 625 by X-ray diffraction technique. Int J Mod Phy B 22(23):3977–3985. doi:10.1142/S0217979208048772
Harker D (1944) The crystal structure of Ni4Mo. J Chem Phy 12(7):315–317
Choi HS, Choi J (1972) Precipitation in Inconel 718 alloy. J Korean Nucl Soc 4(3):203–213
Saburi T, Komatsu K, Yamamoto M, Nenno S, Mizutani Y (1969) A new metastable phase Ni2Mo. Trans AIME 245:2348–2349
Arya A, Banerjee S, Das GP, Dasgupta I, Saha-Dasgupta, Mookerjee A (2001) A first principle thermodynamics approach to ordering in Ni-Mo alloys. Acta Mater 49:3575–3587
Arya A, Kulkarni UD, Dey GK, Banerjee (2008) Effect of ternary additions on the stability of ordered phases in Ni-Mo alloys—transmission electron microscopy results and first principles calculation. Metall Mater Trans A 39A:1623–1629
Kersker MM (1986) Precipitation in nickel-aluminum-molybdenum superalloys. University of Florida. http://ufdc.ufl.edu/UF00085802/00001
Okamoto H (1991) Molybdenum-nickel. J Phase Equilib 12(6):703
Author information
Authors and Affiliations
Corresponding author
Additional information
Highlights
• Interdendritic segregation has been controlled
• Laves phase formation have been studied with liquid nitrogen cooling
• Microfissure-free HAZ is demonstrated at higher cooling rates with LN2 cooling
• Aging response with solid solution filler metal have been demonstrated
Recommended for publication by Commission IX - Behaviour of Metals Subjected to Welding
Rights and permissions
About this article
Cite this article
Manikandan, S., Sivakumar, D., Rao, K.P. et al. Effect of enhanced cooling on microstructure evolution of alloy 718 using the gas tungsten arc welding process. Weld World 60, 899–914 (2016). https://doi.org/10.1007/s40194-016-0349-1
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s40194-016-0349-1