Skip to main content
Log in

High-resolution X-ray imaging and analysis of coatings on and in wood

  • Brief Communication
  • Published:
Journal of Coatings Technology and Research Aims and scope Submit manuscript

Abstract

Wood coatings are widely used for aesthetic and protective reasons. Assessment of coating performance during service life is crucial in order to establish a knowledge database for product optimization. A vast amount of techniques is available for analysis of a coating’s behavior of which microimaging is an important tool. In addition to standard microscopy techniques, high-resolution X-ray tomography is presented as a modality offering nondestructive visualization of a coating and the substrate on which it is applied. Combined with analysis of the 3D volumetric data, surface roughness, structure and thickness of the coating layer, penetration depth and related mechanical anchoring can be studied in relation with the underlying substrate. To provide a clear illustration of the possibilities and limitations of this technique, both an opaque solventborne and an opaque waterborne coating applied on two different wood types were scanned and analyzed. Clearly, three-dimensional X-ray imaging at high resolution produces valuable information merely by visualization. Moreover, by proper analysis, quantitative data are obtained taking into account the limitations of X-ray computed tomography and of automated image processing.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5

References

  1. Zabel, RA, Morell, JJ, Wood microbiology: decay and its prevention. Academic Press Inc., San Diego (1992).

    Google Scholar 

  2. de Meijer, M, Thurich, K, Militz, H, “Comparative study on penetration characteristics of modern wood coatings.” Wood Sci. Technol. 32 (5) 347-365 (1998) doi:10.1007/BF00702791.

    Article  Google Scholar 

  3. Yang, XF, Tallman, DE, Bierwagen, GP, Croll, SG, Rohlik, S, “Blistering and degradation of polyurethane coatings under different accelerated weathering tests.” Polym. Degrad. Stabil. 77 (1) 103-109 (2002) doi:10.1016/S0141-3910(02)00085-X.

    Article  CAS  Google Scholar 

  4. Yang, XF, Li, J, Croll, SG, Tallman, DE, Bierwagen, GP, “Degradation of low gloss polyurethane aircraft coatings under UV and prohesion alternating exposures.” Polym. Degrad. Stabil., 80 (1) 51-58 (2003) doi:10.1016/S0141-3910(02)00382-8.

    Article  CAS  Google Scholar 

  5. Singh, AP, Ratz, A, Dawson, BSW, “A novel method for high-resolution imaging of coating distribution within a rough-textured plywood surface.” J. Coat. Technol. Res., 4 (2) 207-210 (2007) doi:10.1007/s11998-007-9019-y.

    Article  CAS  Google Scholar 

  6. Singh, AP, Dawson, BSW, “Confocal microscope - A valuable tool for examining wood-coating interface.” J. Coat. Technol. Res., 1 (3) 235-237 (2004).

    CAS  Google Scholar 

  7. Leroux, O, Leroux, F, Bellefroid, E, Claeys, M, Couvreur, M, Borgonie, G, Van Hoorebeke, L, Masschaele, B, Viane, R, “A new preparation method to study fresh plant structures with X-ray computed tomography.” J. Microsc.-Oxf., 233 (1) 1-4 (2009).

    Article  CAS  Google Scholar 

  8. Sleutel, S, Cnudde, V, Masschaele, B, Vlassenbroek, J, Dierick, M, Van Hoorebeke, L, Jacobs, P, De Neve, S, “Comparison of different nano- and micro-focus X-ray computed tomography set-ups for the visualization of the soil microstructure and soil organic matter.” Comput. Geosci., 34 (8) 931-938 (2008) doi:10.1016/j.cageo.2007.10.006.

    Article  ADS  Google Scholar 

  9. Kulkarni, A, Goland, A, Herman, H, Allen, AJ, Dobbins, T, DeCarlo, F, Ilavsky, J, Long, GG, Fang, S, Lawton, P, “Advanced neutron and X-ray techniques for insights into the microstructure of EB-PVD thermal barrier coatings.” Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process., 426 (1-2) 43-52 (2006).

    Article  Google Scholar 

  10. Juuti, M, Prykari, T, Alarousu, E, Koivula, H, Myllys, M, Lahteela, A, Toivakka, M, Timonen, J, Myllyla, R, Peiponen, KE, “Detection of local specular gloss and surface roughness from black prints.” Colloid Surf. A-Physicochem. Eng. Asp., 299 (1-3) 101-108 (2007) doi:10.1016/j.colsurfa.2006.11.039.

    Article  CAS  Google Scholar 

  11. Chinga-Carrasco, G, Kauko, H, Myllys, M, Timonen, J, Wang, B, Zhou, M, Fossum, JO, “New advances in the 3D characterization of mineral coating layers on paper.” J. Microsc.-Oxf., 232 (2) 212-224 (2008).

    CAS  Google Scholar 

  12. Morigi, MP, Casali, F, Bettuzzi, M, Bianconi, D, Brancaccio, R, Cornacchia, S, Pasini, A, Rossi, A, Aldrovandi, A, Cauzzi, D, “CT investigation of two paintings on wood tables by Gentile da Fabriano.” Nucl. Instrum. Methods Phys. Res. Sect. A: Accel. Spectrom. Detect. Assoc. Equip., 580 (1) 735-738 (2007) doi:10.1016/j.nima.2007.05.140.

    Article  CAS  ADS  Google Scholar 

  13. Masschaele, BC, Cnudde, V, Dierick, M, Jacobs, P, Van Hoorebeke, L, Vlassenbroeck, J, “UGCT: new X-ray radiography and tomography facility.” Nucl. Instrum. Methods Phys. Res. Sect. A: Accel. Spectrom. Detect. Assoc. Equip., 580 (1) 266-269 (2007) doi:10.1016/j.nima.2007.05.099.

    Article  CAS  ADS  Google Scholar 

  14. Vlassenbroeck, J, Dierick, M, Masschaele, B, Cnudde, V, Van Hoorebeke, L, Jacobs, P, “Software tools for quantification of X-ray microtomography at the UGCT.” Nucl. Instrum. Methods Phys. Res. Sect. A: Accel. Spectrom. Detect. Assoc. Equip., 580 (1) 442-445 (2007) doi:10.1016/j.nima.2007.05.073.

    Article  CAS  ADS  Google Scholar 

  15. Tomasi, C, Manduchi, R, “Bilateral Filtering for Gray and Color Images.” Proc. of the 1998 IEEE International Conference on Computer Vision, Bombay, India, 1998

  16. Moell, M, Borgefors, G, “An image analysis method to measure cross-sectional tracheid dimensions on softwood increment cores.” Wood Fiber Sci., 33 (2) 200-212 (2001).

    CAS  Google Scholar 

  17. Chinga, G, Johnsen, PO, Dougherty, R, Berli, EL, Walter, J, “Quantification of the 3D microstructure of SC surfaces.” J. Microsc.-Oxf., 227 (3) 254-265 (2007).

    Article  Google Scholar 

  18. de Meijer, “Interactions Between Wood and Coatings with Low Organic Solvent Content.” Wageningen, the Netherlands, 1999

  19. Van den Bulcke, J, Rijckaert, V, Van Acker, J, Stevens, M, “Quantitative measurement of the penetration of water-borne coatings in wood with confocal lasermicroscopy and image analysis.” Holz Als Roh-und Werkst., 61 (4) 304-310 (2003) doi:10.1007/s00107-003-0394-5.

    Article  Google Scholar 

  20. Limaye, A, “Drishti - Volume Exploration and Presentation Tool”, Proc. of Vis, Baltimore, USA, 2006.

    Google Scholar 

  21. Vidal, FP, Letang, JM, Peix, G, Cloetens, P, “Investigation of artefact sources in synchrotron microtomography via virtual X-ray imaging.” Nucl. Instrum. Methods Phys. Res. Sect. B-Beam Interact. Mater. Atoms, 234 (3) 333-348 (2005).

    Article  CAS  ADS  Google Scholar 

Download references

Acknowledgments

The authors wish to thank the Fund for Scientific Research-Flanders (Belgium—FWO) for the postdoctoral funding granted to the first author.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Jan Van den Bulcke.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Van den Bulcke, J., Boone, M., Van Acker, J. et al. High-resolution X-ray imaging and analysis of coatings on and in wood. J Coat Technol Res 7, 271–277 (2010). https://doi.org/10.1007/s11998-009-9182-4

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11998-009-9182-4

Keywords

Navigation