Skip to main content
Log in

Development of a modified test cell for AC impedance testing of coated Al fins

  • Published:
Journal of Coatings Technology and Research Aims and scope Submit manuscript

Abstract

An innovative test-cell arrangement is proposed and examined for electrochemical impedance spectroscopy (EIS) testing of coated thin sheet or foil samples. This arrangement uses a thin layer of medical cotton fabric as a medium containing and transporting 5% sodium chloride solution. This new EIS cell avoids the intervention of edge effect into EIS measurements of painted material. It also avoids the formation of crevice attack experienced at the edges of conventional sample holders or normally under the edge of the masking material. This arrangement is simple and flexible to suit different sizes and shapes of flat panel and foil samples. It can also be used effectively as specimen holders for other than thin sheets. The test cell is also suitable for any electrochemical tests other than impedance measurements. The accelerated results of the EIS present the viability of the EIS test cell to be used as an accelerated nondestructive, repetitive measurement of coated thin metal substrate.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

References

  1. G Bierwagen, D Tallman, J Li, L He, C Jeffcoate, EIS Studies of Coated Metals in Accelerated Exposure Prog. Org. Coat. 46, 2, 2003, 149–158

    Article  Google Scholar 

  2. JN Murray, LD Stephenson, A Kumar, Electrochemical and Physical Evaluations of Coil Coatings on Metal-Coated Steels for Roofing Applications Prog. Org. Coat. 47, 2, 2003, 136–146

    Article  CAS  Google Scholar 

  3. S Touzain, Q Le Thu, G Bonnet, Evaluation of Thick Organic Coatings Degradation in Seawater Using Cathodic Protection and Thermally Accelerated Tests Prog. Org. Coat. 52, 4, 2005, 311–319

    Article  CAS  Google Scholar 

  4. Q Le Thu, H Takenouti, S Touzain, EIS Characterization of Thick Flawed Organic Coatings Aged Under Cathodic Protection in Seawater Electrochim. Acta 51, 12, 2006, 2491–2502

    Article  CAS  Google Scholar 

  5. A Shi, S Koka, J Ullett, Performance Evaluation on the Weathering Resistance of Two USAF Coating Systems (Standard 85285 Topcoat Versus Fluorinated APC Topcoat) via Electrochemical Impedance Spectroscopy Prog. Org. Coat. 52, 3, 2005, 196–209

    Article  CAS  Google Scholar 

  6. JN Murray, Time Constraints in the Testing of Salt-Fogged Samples via Electrochemical Impedance Spectroscopy Prog. Org. Coat. 49, 4, 2004, 342–352

    Article  CAS  Google Scholar 

  7. V Lavaert, M De Cock, M Moors, E Wettinck, Influence of Pores on the Quality of a Silicon Polyester Coated Galvanised Steel System Prog. Org. Coat. 38, 3–4, 2000, 213–221

    Article  CAS  Google Scholar 

  8. Hegedus, CR, “A Holistic Perspective of Coatings Technology,” J. Coat. Technol. Res., 1 (1) 4–19 (2004)

  9. Nguyen, T, Bentz, D, Byrd, E, “A Method for Measuring Water Diffusion in a Coating Applied to a Substrate,” J. Coat. Technol., 67 (844) 37–46 (1995)

    Google Scholar 

  10. Granata, RD, MacQueen, RC, Miron, RR, “A Method for Corrosion Inhibitor Mechanism Studies in Epoxy Coated Aluminum,” J. Coat. Technol., 68 (857) 75–82 (1996)

  11. Wang, X, Chen, D, Lu, L, Wang, G, Yang, W, “A Novel Anti-Condensation Coating,” J. Coat. Technol., 70 (883) 55–59 (1998)

  12. Davis, GD, Krebs, LA, Dacres, CM, “Coating Evaluation and Validation of Accelerated Test Conditions Using an In-Situ Corrosion Sensor,” J. Coat. Technol., 74 (935) 69–74 (2002)

  13. Deflorian, F, Luigi Bonora, P, Fedrizzi, L, Rossi, S, “Advanced Testing Procedures for High Performance Coatings,” J. Coat. Technol., 72 (908) 81–87 (2000)

    Google Scholar 

  14. Mattos, O, Ferreira, J, Margarit, I, Quintela, J, “About Coatings and Cathodic Protection: Electrochemical Features of Coatings Used on Pipelines,” J. Coat. Technol., 73 (914) 61–65 (2001)

    Google Scholar 

  15. Kouloumbi, N, Tsangaris, GM, Molnar, F, Vourvahi, C, “Corrosion Resistance and Dielectric Properties of an Iron Oxide Filled Epoxy Coating,” J. Coat. Technol., 69 (870) 53–59 (1997)

    Google Scholar 

  16. Scantlebury JD, Galic K, The Application of AC Impedance to study the Performance of Lacqured Aluminum in Acetic Acid Solutions Prog. Org. Coat. 31 201–207, (1997)

    Article  CAS  Google Scholar 

  17. Huburn BJ, Gowers JD, Scantlebury JD, Interpretation of Low Frequency AC Impedance Data for Organic Coatings on Mild Steel Br. Corros. J. 21, 104–108 (1986)

    Google Scholar 

  18. Kendig M, Scully J, Basic Aspect of Electrochemical Impedance Application for Life Prediction of Organic Coatings on Metals Corros. Sci. 46, 1, 22–28, (1990)

    CAS  Google Scholar 

  19. DeFlorian, F, Fedrizzil, L, Bonora, PL, “Corrosion Behaviour of Epoxy Coated Galvanized Steel.” In: Costa, JM, Mercer, AD (eds) Progress in the Understanding and Prevention of Corrosion, Vol. 1 (1993)

  20. “Evaluation of Organic Coatings by Electrochemical Impedance Measurements”, Application Note: AC–2, Electrochemical Instruments Group EG&G Princeton Applied Research Princeton, New Jersey (1984)

  21. “Flex Cell Critical Pitting Test Cell Kit” Operator’s Manual Gamry Instrument Inc. PA, USA (1999)

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to A. Husain.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Husain, A., Brahme, P.S. & Al-Shamali, O. Development of a modified test cell for AC impedance testing of coated Al fins. J Coat Technol Res 4, 317–325 (2007). https://doi.org/10.1007/s11998-007-9043-y

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11998-007-9043-y

Keywords

Navigation