Abstract
The deformation behavior of monolithic modified 9Cr-1Mo (Grade 91) steel during uniaxial tensile loading was studied using the in situ neutron diffraction technique. The residual stress distribution across gas tungsten arc welds in the Grade 91 steel was measured by the time-of-flight neutron diffraction method using the SMARTS diffractometer at Lujan Neutron Scattering Center, Los Alamos National Laboratory. Grade 91 plates were welded using the gas tungsten arc welding (GTAW) technique. The load sharing by different grain orientations was observed during the tensile loading. The residual stresses along three orthogonal directions were determined at the mid-thickness, 4.35 and 2.35 mm below the surface of both the as-welded and post-weld heat-treated plates. The residual stresses of the as-welded plates were compared with those of the post-weld heat-treated plates. The post-weld heat treatment significantly reduced the residual stress level in the base metal, the heat-affected zone, and the weld zone. Vickers microhardness across the weld zone of the as-welded and post-weld heat-treated specimens was evaluated and correlated with the observed residual stress profile and microstructure.
Similar content being viewed by others
References
I. Charit and K.L. Murty, Structural Materials Issues for the Next Generation Fission Reactors, JOM, 2010, 62, p 67–74
E. Barker, Creep Fracture of 9Cr-1Mo Steel, Mater. Sci. Eng., 1986, 84, p 49–64
R.L. Klueh, Elevated Temperature Ferritic and Martensitic Steels and Their Application to Future Nuclear Reactors, Int. Mater. Rev., 2005, 50, p 287–310
S. Sathyanarayanan, A. Moitra, K.G. Samuel, G. Sasikala, S.K. Ray, and V. Singh, Evaluation of Dynamic Fracture Toughness Based Reference Temperature (\(T_{0}^{\text{dy}}\) of Modified 9Cr-1Mo Steel in Phosphorus Embrittled and Cold-worked Condition, Mater. Sci. Eng. A, 2008, 488, p. 519–528
K.L. Murty and I. Charit, Structural Materials for Gen-IV Nuclear Reactors: Challenges and Opportunities, J. Nucl. Mater., 2008, 383, p 189–195
K. Laha, K.S. Chandravathi, P. Parameswaran, and K. Bhanu, Sankara Rao, and S.L. Mannan, Characterization of Microstructures Across the Heat-Affected Zone of the Modified 9Cr-1Mo Weld Joint to Understand Its Role in Promoting Type IV Cracking, Metall. Mater. Trans. A, 2007, 38, p 58–68
S.-H. Kim, J.-B. Kim, and W.-J. Lee, Numerical Prediction and Neutron Diffraction Measurement of the Residual Stresses for a Modified 9Cr-1Mo Steel Weld, J. Mater. Process. Technol., 2009, 209, p 3905–3913
G.E. Dieter, Mechanical Metallurgy, McGraw-Hill Book Company, New York, 1961
P.J. Withers, Residual Stress and Its Role in Failure, Rep. Prog. Phys., 2007, 70, p 2211–2264
A.D. Krawitz, Introduction to Diffraction in Materials Science and Engineering, 1st ed., Wiley, New York, 2001
B. Clausen, D.W. Brown, and I.C. Noyan, Engineering Applications of Time-of-Flight Neutron Diffraction, JOM, 2012, 64(1), p 117–126
L. Pintschovius, Macrostresses, microstresses and stress tensors, Measurement of Residual and Applied Stress Using Neutron Diffraction, M.T. Hutchings and A.D. Krawitz, Ed., Kluwer Academics Publishers, Boston, 1992, p 115–130
H.M. Rietveld, A Profile Refinement Method for Nuclear and Magnetic Structures, J. Appl. Cryst., 1969, 2, p 65–71
E.L. Pavlina and C.J. Van Tune, Correlation of Yield Strength and Tensile Strength with Hardness for Steels, J. Mater. Eng. Perform., 2008, 17(6), p 888–893
T. Shrestha, M. Basirat, I. Charit, G.P. Potirniche, K.K. Rink, and U. Sahaym, Creep Deformation Mechanisms in Modified 9Cr-1Mo Steel, J. Nucl. Mater., 2012, 423, p 110–119
S. Alsagabi, T. Shrestha, and I. Charit, High Temperature Tensile Deformation Behavior of Grade 92 Steel, J. Nucl. Mater., 2014, 453, p 151–157
B. Clausen, D.W. Brown, M.A.M. Bourke, T.A. Saleh, and S.A. Maloy, In Situ Neutron Diffraction and Elastic-Plastic Self-Consistent Polycrystal Modeling of HT-9, J. Nucl. Mater., 2012, 425, p 228–232
M.R. Daymond and P.J. Bouchard, Elastoplastic Deformation of 316 Stainless Steel Under Tensile Loading at Elevated Temperature, Metall. Mater. Trans. A, 2006, 37, p 1863–1873
P.A. Turner and C.N. Tome, Study of Residual Stresses in Zircaloy-2 with Rod Texture, Acta Mater., 1994, 42, p 4143–4153
A.R. Pyzalla, Internal stresses in engineering materials, Neutrons and Synchrotron Radiation in Engineering Materials Science, W. Reimers, A.R. Pyazalla, A. Schreyer, and H. Clemens, Ed., Wiley, Weinheim, 2008, p 21–56
H. Dai, J.A. Francis, H.J. Stone, H.K.D.H. Bhadeshia, and P.J. Withers, Characterizing Phase Transformation and Their Effects on Ferritic Weld Residual Stresses with X-Rays and Neutrons, Metall. Mater. Trans. A, 2008, 39, p 3070–3078
N.S. Rossini, M. Dassisti, K.Y. Benyounis, and A.G. Olabi, Methods of Measuring Residual Stresses in Components, Mater. Des., 2012, 35, p 572–588
S. Paddea, J.A. Francis, A.M. Paradowska, P.J. Bouchard, and I.A. Shibi, Residual Stress Distributions in a P91 Steel-Pipe Girth Weld Before and After Post Weld Heat Treatment, Mater. Sci. Eng. A, 2012, 534, p 663–672
A.H. Yaghi, T.H. Hyde, A.A. Becker, and W. Sun, Finite Element Simulation of Welded P91 Steel Pipe Undergoing Post-Weld Heat Treatment, Sci. Technol. Weld. Join., 2011, 16(3), p 232–238
J.W.H. Price, A. Paradowska, S. Joshi, and T. Finlayson, Residual Stresses Measurement by Neutron Diffraction and Theoretical Estimation in a Single Weld Bead, Int. J. Press. Vessel. Pip., 2006, 83, p 381–387
R.J. Moat, D.J. Hughes, A. Steuwer, N. Iqbal, M. Preuss, S.E. Bray, and M. Rawson, Residual Stresses in Inertial-Friction-Welded Dissimilar High-Strength Steels, Metall. Mater. Trans. A, 2009, 40, p 2098–2108
D.J. Smith and S.J. Garwood, Influence of Post-Welded Heat Treatment on the Variation of Residual Stressed in 50 mm Thick Welded Ferritic Steel Plates, Int. J. Press. Vessel. Pip., 1992, 51, p 241–256
E.J. McDonald, L.F. Exworthy, P.E.J. Flewitt, K. Hallam, and W. Bell, Measurement of Residual Stresses in a Multi-Pass Low Alloy Ferritic Steel Weld Using x-ray Diffraction, Mater. Sci. Forum, 2000, 347–349, p 664–669
X. Ficquet, C.E. Truman, and D.J. Smith, Measurement of Residual Stress in an A533B Ferritic Steel Plate Containing a Repair Weld, Mater. Sci. Forum, 2006, 524–525, p 653–658
M. Turski, A.H. Sherry, P.J. Bouchard, and P.J. Withers, Residual Stress Driven Creep Cracking in Type 316 Stainless Steel, J. Neutron Res., 2004, 12(1–3), p 45–49
P.J. Bouchard, P.J. Withers, S.A. McDonald, and R.K. Heenan, Quantification of Creep Cavitation Damage Around a Crack in a Stainless Steel Pressure Vessel, Acta Mater., 2004, 52(1), p 23–34
S.K. Albert, M. Matsui, H. Hongo, T. Watanabe, K. Kubo, and M. Tabuchi, Creep Rupture Properties of HAZs of a High Cr Ferritic Steel Simulated by a Weld Simulator, Int. J. Press. Vessel. Pip., 2004, 81, p 221–234
D. Li and K. Shinozaki, Simulation of Role of Precipitation in Creep Void Occurrence in Heat Affected Zone of High Cr Ferritic Heat Resistant Steels, Sci. Technol. Weld. Join., 2005, 10(5), p 544–549
T. Watanabe, M. Yamazaki, H. Hongo, M. Tabuchi, and T. Tanabe, Effect of Stress on Microstructural Change Due to Aging at 823 K in Multi-layer Welded Joint of 2.25Cr-1Mo Steel, Int. J. Press. Vessel. Pip., 2004, p. 279–284.
Y. Tomota, H. Tokuda, Y. Adachi, M. Wakita, N. Minakawa, A. Moriai, and Y. Morii, Tensile Behavior of TRIP-Aided Multi-phase Steels Studied by In Situ Neutron Diffraction, Acta Mater., 2004, 52, p 5737–5745
S.A. David and T. Debroy, Current Issues and Problems in Welding Science, Science, 1992, 257, p 497–502
M. Regev, S. Berger, and B.Z. Weiss, Investigation of Microstructure Mechanical and Creep Properties of Weldments Between T91 and T22 Steels, Weld. J., 1996, 75, p 261s–268s
T. Sato, K. Tamura, Advances in Materials Technology for Fossil Power Plants, Proceedings of the 5th International Conference, Oct. 3-5, 2007, (Marco Island, FL, USA) ASM Int., 2008, p. 874–883.
D. Dean and M. Hidekazu, Prediction of Welding Residual Stress in Multi-pass Butt-Welded Modified 9Cr-1Mo Steel Pipe Considering Phase Transformation Effects, Comput. Mater. Sci., 2006, 37, p 209–219
M. Sireesha, S.K. Albert, and S. Sundaresan, Microstructure and Mechanical Properties of Weld Fusion Zones in Modified 9Cr-1Mo Steel, J. Mater. Eng. Perform., 2001, 10(3), p 320–330
Acknowledgments
This work has benefited from the use of the SMARTS facility at the Lujan Neutron Scattering Center at Los Alamos Neutron Science Center, funded by the DOE Office of Basic Energy Sciences. Los Alamos National Laboratory is operated by Los Alamos National Security LLC under DOE Contract DE-AC52-06NA25396. This research was performed using funding received from the DOE Office of Nuclear Energy’s Nuclear Energy University Programs (NEUP) through the US Department of Energy Grant no. 42246 release 59. The first author (TS) would like to acknowledge the assistance provided by Bjorn Clausen, Donald W. Brown, and Thomas A. Sisneros of the Lujan Scattering Center during the course of this study.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Shrestha, T., Charit, I. & Potirniche, G. In Situ Tensile Deformation and Residual Stress Measurement by Neutron Diffraction in Modified 9Cr-1Mo Steel. J. of Materi Eng and Perform 24, 4710–4720 (2015). https://doi.org/10.1007/s11665-015-1752-2
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-015-1752-2