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Regeneration of used nickel catalyst

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Journal of the American Oil Chemists’ Society

ABSTRACT

Regeneration of used nickel catalyst from a hydrogenation plant has been achieved by converting the nickel content of slurry into NiO and Ni(OH)2, and the subsequent reduction of these compounds by hydrogen gas at temperatures of 450 C and 290 C respectively. A laboratory and plant apparatus for reduction are designed. Activity of regenerated catalyst was measured in comparison with reference catalyst (G15). Pretreatment of discarded catalyst prior to reduction is described.

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References

  1. Coenen, J.W.E., and B.G. Linsen, “Physical and Chemical Aspects of Adsorbents and Catalysis,” Academic Press, London, 1970, p. 496.

    Google Scholar 

  2. Mork, P.C. JAOCS 49:426 (1972).

    Article  Google Scholar 

  3. Drozdawski, B., and N. Zajac, JAOCS 54:595 (1977).

    Google Scholar 

  4. Allen, R.R., JAOCS 45:312A (1968).

    Article  Google Scholar 

  5. Lieher, E., and F.L. Morritz, “Advances in Catalysis,” Vol. 5, Edited by W.G. Frankenburg, V.I. Komarewsky, and E.K. Rideal, Academic Press, New York, 1953, p. 417ff.

    Google Scholar 

  6. Mellor, J.W., “Comprehensive Treatise on Inorganic and Theoretical Chemistry,” Vol. XVA, Longmans and Green, London, 1964, p. 816.

    Google Scholar 

  7. Kane, J.G., and S.R. Saitwadekar, Ind. J. Appl. Chem. 28:208 (1965).

    CAS  Google Scholar 

  8. Skoog, D.A., and D.M. West, “Fundamentals of Analytical Chemistry,” 2nd Ed., Holt, Rinehart and Winston, New York, 1969, p. 838.

    Google Scholar 

  9. Vogel, A.I., “A Text Book of Quantitative Inorganic Analysis,” 3rd Ed., Longmans and Green, London, 1966, p. 1216.

    Google Scholar 

  10. “Official and Tentative Methods of the American Oil Chemists’ Society,” 3rd Ed., Method Cc 1-25 and Cd 1-25, AOCS, Champaign, IL, 1972.

  11. “Official Methods of Analysis of the Associaiton of Official Agricultural Chemists,” 11th Ed., Washington, D.C., 1970, p. 1012.

  12. Gravelle, P.C., and S.J. Teichner, in “Advances in Catalysis,” Vol. 20, Edited by D.D. Eley, H. Pines, and P.B. Weisz, Academic Press, New York, 1969, p. 168ff.

    Google Scholar 

  13. Adkins, H., Ind. and Eng. Chem. 32:1189 (1940).

    Article  CAS  Google Scholar 

  14. Kivnick, A., and A.N. Hixon, Chem. Eng. Prog. 48:394 (1952).

    CAS  Google Scholar 

  15. Bailey, A.E., Ind. and Eng. Chem. 44:985 (1952).

    Article  Google Scholar 

  16. Carter, J.L., J.A. Cusumano, and J.H. Sinfelt, J. Phys. Chem. 70:2257 (1966).

    Article  CAS  Google Scholar 

  17. Dafler, J.R., JAOCS 54:17 (1977).

    Article  CAS  Google Scholar 

  18. Salwood, P.W., T.R. Phillips, and S. Adler, J. Am. Chem. Soc. 76:2281 (1955).

    Article  Google Scholar 

  19. Koestler, D., and A. Meisel, Z. Phys. Chem. 231:99 (1966).

    Google Scholar 

  20. Swern, D., in “Bailey’s Industrial Oil and Fat Products,” 3rd Ed., Edited by D. Swern, Interscience Publishers, New York, 1964, p. 97ff.

    Google Scholar 

  21. VanRede, C, and L.V. Cocks, “Laboratory Handbook for Oil and Fat Analysts,” Academic Press, London, 1966, p. 419.

    Google Scholar 

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Massouml1, A., Kajbaf, M.A. Regeneration of used nickel catalyst. J Am Oil Chem Soc 56, 565–568 (1979). https://doi.org/10.1007/BF02660235

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  • DOI: https://doi.org/10.1007/BF02660235

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