Abstract
The paper presents the results of influence of surface pretreatment of Ti6Al4V alloy, used for short-term implants in orthopedics, followed by anodic oxidation and steam sterilization on its physical and chemical properties. The pretreatment was a combination of: grinding, vibration machining, mechanical polishing, sandblasting and electrolytic polishing. Studies of surface topography, wettability, hardness and stress profiles of the substrate after various surface treatments were carried out. Furthermore, studies of pitting and crevice corrosion as well as ion release into a Ringer’s solution after long-term exposure were also performed. The results show that the pretreatment preceding the anodic oxidation and steam sterilization affects the physical and chemical properties of the surface layer of Ti6Al4V alloy implants. Moreover, they indicate that the use of appropriate methods of pretreatment enable formation of a passive layer characterized by good osteoconductive properties.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Frosch, K.H., Sturmer, K.M.: Metallic biomaterials in skeletal repair. Eur. J. Trauma 32, 149–159 (2006)
Anselme, K.: Biomaterials and interface with bone. Osteoporos. Int. 22, 2037–2042 (2011)
Basiaga, M., Jendrus, R., Walke, W., Paszenda, Z., Kaczmarek, M., Popczyk, P.: Influence of surface modification on properties of stainless steel used for implants. Arch. Metall. Mater. 60(4), 2965–2969 (2015)
Kiel, M., Marciniak, J., Basiaga, M., Szewczenko, J.: Numerical analysis of spine stabilizers on lumbar part of spine. ITiB Adv. Intell. Syst. Comput. 69, 447–456 (2010)
Kajzer, W., Kajzer, A., Gzik-Zroska, B., Wolański, W., Janicka, I., Dzielicki, J.: Comparison of numerical and experimental analysis of plates used in treatment of anterior surface deformity of chest. In: Piętka, E., Kawa, J. (eds.) ITIB 2012. LNCS, vol. 7339, pp. 319–330. Springer, Heidelberg (2012). doi:10.1007/978-3-642-31196-3_32
Geetha, M., Singh, A.K., Asokamani, R., Gogia, A.K.: Ti based biomaterials, the ultimate choice for orthopaedic implants a review. Prog. Mater. Sci. 54, 397–425 (2009)
Marciniak, J., Szewczenko, J., Walke, W., Basiaga, M., Kiel, M., Manka, I.: Biomechanical analysis of lumbar spine stabilization by means of transpedicular stabilizer. ITiB Adv. Soft Comput. 47, 529–536 (2008)
Pochrzast, M., Basiaga, M., Marciniak, J., Kaczmarek, M.: Biomechanical analysis of limited-contact plate used for osteosynthesis. Acta. Bioeng. Biomech. 16(1), 99–105 (2014)
Makuch, K., Koczorowski, R.: Biocompatibility of titanium and its alloys used in dentistry. Dent. Med. Probl. 47, 81–88 (2010). (in Polish)
Ziębowicz, A., Bączkowski, B.: Numerical analysis of the implant – abutment system. In: Piętka, E., Kawa, J. (eds.) ITIB 2012. LNCS, vol. 7339, pp. 341–350. Springer, Heidelberg (2012). doi:10.1007/978-3-642-31196-3_34
Rusinek, B., Stobiecka, A., Obtulowicz, K.: Titanium allergy and implants. Alerg. Immunol. 5, 5–7 (2008). (in Polish)
Yamamoto, D., Kawai, I., Kuroda, K., Ichino, R., Okido, M., Seki, A.: Osteoconductivity and hydrophilicity of TiO2 coatings on Ti substrates prepared by different oxidizing processes. Bioinorg Chem Appl, Article ID 495218 (2012)
Park, J.W., Jang, J.H., Lee, C.S., Hanawa, T.: Osteoconductivity of hydrophilic microstructured titanium implants with phosphate ion chemistry. Acta. Biomater. 5, 2311–2321 (2009)
Sobieszczyk, S.: Surface modifications of Ti and its alloys. Nat. Adv. Sci. Inst. Se. 10, 29–42 (2010)
Basiaga, M., Walke, W., Paszenda, Z., Kajzer, A.: The effect of EO and steam sterilization on mechanical and electrochemical properties of titanium grade 4. Mater. Tehnol. 50(1), 153–158 (2016)
Marciniak, J., Szewczenko, J., Kajzer, W.: Surface modification of implants for bone surgery. Arch. Metall. Mater. 60(3B), 2123–2129 (2015)
Szewczenko, J., Pochrzast, M., Walke, W.: Evaluation of electrochemical properties of modified Ti-6Al-4V ELI alloy. Przegl. Elektrotechniczny 87(12b), 177–180 (2011)
Krasicka-Cydzik, E.: Anodic layer formation on titanium and its alloys for biomedical applications, titanium alloys. In: Nurul Amin, A.K.M. (Ed.) Towards Achieving Enhanced Properties for Diversified Applications (2012)
Szewczenko, J., Jaglarz, J., Basiaga, M., Kurzyk, J., Skoczek, E., Paszenda, Z.: Topography and thickness of passive layers on anodically oxidized Ti6Al4V alloys. Przegl. Elektrotechniczny 88(12B), 228–231 (2012)
Diamanti, M.V., Del Curto, B., Pedeferri, M.: Anodic oxidation of titanium: from technical aspects to biomedical applications. J. Appl. Biomater. Biomech. 9, 55–69 (2011)
Fojt, J.: Ti-6Al-4V alloy surface modification for medical applications. Appl. Surf. Sci. 262, 163–167 (2012)
Karambakhsh, A., Afshar, A., Malekinejad, P.: Corrosion resistance and color properties of anodized Ti-6Al-4V. J. Mater. Eng. Perform. 21, 121–127 (2012)
Barranco, V., Onofre, E., Escudero, M.L., Garcia-Alonso, M.C.: Characterization of roughness and pitting corrosion of surfaces modified by blasting and thermal oxidation. Surf. Coat. Tech. 204, 3783–3793 (2010)
Zhang, D., Cheng, H., Wang, Y., Ning, C.: Effect of different acid treatment on surface characteristics of titanium alloy. Mater. Sci. Forum. 694, 490–496 (2011)
Yamamoto, D., Kuroda, K., Ichino, R., Okido, M.: Hydrophilicity and Osteoconductivity of Ti Anodized in Various Aqueous Solutions. Honolulu PRiME, Abstract 2054 (2012)
Yamamoto, D., Iida, T., Arii, K., Kuroda, K., Ichino, R., Okido, M., Seki, A.: Surface hydrophilicity and osteoconductivity of anodized Ti in aqueous solutions with various solute ions. Mater. Trans. 53, 1956–1961 (2012)
Szewczenko, J.: Formation of physical and chemical properties of surface layer on titanium alloys used for implants for traumatology and orthopaedics. Ed. Silesian Technical University, Gliwice (2014)
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2017 Springer International Publishing AG
About this paper
Cite this paper
Szewczenko, J., Basiaga, M., Grygiel-Pradelok, M., Kaczmarek, M. (2017). Characteristics of Surface Layers of Ti6Al4V Implants. In: Gzik, M., Tkacz, E., Paszenda, Z., Piętka, E. (eds) Innovations in Biomedical Engineering. Advances in Intelligent Systems and Computing, vol 526. Springer, Cham. https://doi.org/10.1007/978-3-319-47154-9_10
Download citation
DOI: https://doi.org/10.1007/978-3-319-47154-9_10
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-319-47153-2
Online ISBN: 978-3-319-47154-9
eBook Packages: EngineeringEngineering (R0)