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Sol-gel Preparation and Characterization of ZnCaAl2O4 Composite Nanoparticles

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Recent Advances in Manufacturing Processes

Abstract

Microwave dielectric materials are well-recognized for their broad application in communication from satellite to ground. The advantages of dielectric materials lie scaling down the device and the controlled dielectric permittivity. However, the growing world of communication is expanding its operating frequency for the global position satellite (GPS). Presently, the trend of miniaturization of patch antenna has been demanded to fulfill the requirement of the GPS system. In this perspective, dielectric ceramic materials have got recognized due to the tunability of dielectric permittivity and quality factor to a great extent. In this work, we report the synthesis and characterization of calcium zinc aluminate (ZnCaAl2O4) composite nanoparticles. XRD investigation endorsed the mixed phases of ZnCaAl2O4, and ZnA2O4 in the prepared sample. FTIR study demonstrated the various compositional transmittance peaks correspond to the compound nanoceramic material ZnCaAl2O4. SEM analysis showed the agglomeration of nanoparticles with their average diameter of 50 nm whereas the presence of Zn, Ca, Al, and O are confirmed by the EDS investigation.

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References

  1. Nasarudin W, Jalal W, Abdullah H, Zulfakar MS, Tariqual IM, Bais B, Sahbuddin S (2014) GPS patch antenna performance by modification of Zn(1-x)CaxAl2O4 based microwave dielectric ceramics. https://doi.org/10.1007/s10971-014-3397-2

  2. Zawadzki M, Wrzyszcz J (2000) Hydrothermal synthesis of nanoporous zinc aluminate with high surface area. Mater Res Bull 35(1):109–111. https://doi.org/10.1016/SOO25-5408(00)00185-9

  3. Huang C-L, Chen J-Y and Tseng Y-W (2010) High-dielectric-constant and low-loss microwave dielectric in the Ca(Mg1/3Ta2/3)O3–(Ca0.8Sr0.2)TiO3 solid solution system. Mater Sci Eng B 167:142–146

    Google Scholar 

  4. Zulfaka MS , Abdullah H, Tariqul IM, Nasarudin W, Jalal W, Zainuddin Z, Sahbudin S (2014) Performance effect of ZnAl2O4—SiO2 thin film for wireless patch antenna application. J Nano Res 28:141–150. https://doi.org/10.4028/www.scientific.net/JNanoR.28.141© Trans Tech Publications, Switzerland. Online: 2014-06-06, ISSN: 1661-9897

  5. Abdullah H, Nasarudin W, Jalal W, Zulfakar MS (2013) Miniaturization of GPS patch antennas based on novel dielectric ceramics Zn(1–x)MgxAl2O4 by sol–gel method, journal of sol-gel science and technology. J Sol-Gel Sci Technol 69:429–440. https://doi.org/10.1007/s10971-013-3239-7

    Article  Google Scholar 

  6. Nasarudin W, Jalal W, Abdullah H, Zulfakar MS, (2013) Characterization and dielectric properties of novel dielectric ceramics CaxZn(1-x)Al2O4 for GPS patch antennas. Int J Appl Ceram Technol, 1–11. https://doi.org/10.1111/ijac.12193

  7. Zawadzki M, Staszak W, López-Suárez FE, Illán-Gómez MJ, Bueno-López A (2009) Preparation, characterisation and catalytic performance for soot oxidation of copper-containing ZnAl2O4 spinels. Appl Cataly A General 371(1–2):92–98

    Google Scholar 

  8. Nasarudin W, Jalal W, Abdullah H, Zulfakar MS, Bais B, Sahbudin S, Mohammad Thariqul IM, ZnAl2O4-based microwave dielectric ceramics as GPS patch antenna: a review. Trans Indian Ceramic Soc 72(4):215–224. https://doi.org/10.1080/0371750X.2013.868323

  9. Abdullah H, Zulfakar MS, Nasarudin W, Jalal W, Tariqul IM, Sahbudin S (2014) Synthesis and fabrication of (1-x)ZnAl2O4–xSiO2 thin films to be applied as patch antenna. J Sol-Gel Sci Technol 69:183–192. https://doi.org/10.1007/s10971-013-3202-7

  10. Zulfakar MS, Abdullah H, NasarudinW, Jalal W, Zainuddin Z, Sarada I (2014) Study of (1/2x)ZnAl2O4–xSiO2 spinel structures as microwave dielectric material. Received: 23 Dec 2013/Accepted: 8 May 2014 Springer Science+Business Media New York

    Google Scholar 

  11. Abdullah H, Nasarudin W, Jalal W, Zulfakar MS, Badariah B, Sahbudin S, Tariqul IM, Sarada I (2015) Effects of Mg contents on ZnAl2O4 thin films by sol gel method and its application. In: Ohji T, Singh M, Mathur S (eds) Advanced processing and manufacturing technologies for nanostructured and multifunctional materials. The American Ceramic Society

    Google Scholar 

  12. Abdullah H, Nasarudin W, Jalal W, Zulfakar MS, Tariqul IM, Bais B (2015) Characterization of TixZn(1-x)Al2O4 thin films by sol-gel method for GPS patch antennae. J Korean Phys Soc 66(1): 41–45

    Google Scholar 

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Didde, S., Dubey, R.S., Panda, S.K. (2022). Sol-gel Preparation and Characterization of ZnCaAl2O4 Composite Nanoparticles. In: Kumari, R., Majumdar, J.D., Behera, A. (eds) Recent Advances in Manufacturing Processes. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-16-3686-8_10

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  • DOI: https://doi.org/10.1007/978-981-16-3686-8_10

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  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-16-3685-1

  • Online ISBN: 978-981-16-3686-8

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