Abstract
Qualitative and quantitative analysis on phthalate plasticizes (DEHP, DIBP and DBP) of 24 kinds of common food paper packaging were carried out. The study determined the plasticizers using four kinds of organic extraction reagent named n-hexane, ethyl acetate, anhydrous ethanol, and acetone by the Ultrasonic extraction and the gas chromatograph-mass spectrometer technology. The best temperature, time and the way of the extraction of these four different reagent were obtained. Through experiments and analysis, the best extraction reagent of the plasticizers remained in the food paper packaging is ethyl acetate and the best way to extract targets is the combination of ultrasonic oscillation 30 min with vortex 3 min. For the extraction using ethyl acetate, the best temperature of the ultrasonic operation is 25 °C, and the time of the optimum ultrasonic extraction is 90 min. The plasticizers were detected in all of the 24 kinds of food paper packaging samples by the method. The content of DEHP, DBP and DIBP were 0.33497–211.02104, 0.34484–519.9099, 0.20224–37.67883 mg/kg respectively. The result shows that the method is comparatively simple, fast and quantitative accuracy. But the safety of the food paper packaging should be concerned deeply.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Yue Q (2011) Study on potential harm and migration of paper packaging material. Environ Prot Energy Save 4(42):61–63
Yang C (2012) Study on printing ink migration with AAS and GC-MS for paper packaging material. Packag Eng 33(11):18–20
Yamaguchi Y, Fujita Y, Kuroda K, Endo G (2004) Chemical analysis and genotoxico logical safety assessment of paper and paper board used for food packaging. Food Chem 42:1323–1337
Gottfried Z (2001) Odorous compounds in paperboard as influenced by recycled material and storage. Packag Technol Sci 14:13l–136
Wang X, Lin X, Ke H et al (2007) Study progress on pollution and alate plasticizers. Environ Health 24(9):736–738
Wang C, Yang Z, Rong X et al (2013) Detection of plasticizers within costing paper with Ultrasonic extraction-gas chromatograph-mass spectrometer. Technol Prog 3:19–21
Liu Z, Huang H, Liu J et al (2010) Detection of Phthalates plasticizers within tipping paper and packaging paper with isopropanol extraction-gas chromatograph. Anal Instrum 2:30–35
Zhang L, Rong H, X Yu et al (2012) Detection of Phthalates plasticizers within plant fibre food packaging material with Gas chromatograph method. China Sanitary Inspection J 22(3):450–452
Wang C, Mai J et al (2013) Detection of Phthalates plasticizers within costing paper with microwave-assisted extraction-gas chromatograph-mass spectrometer/selected ion monitoring (SIM). Fujian Anal Determ 22(4):1–7
Song YS, Park HJ, Komolprasert V (2000) Analytical procedure for quantifying five compounds suspected as possible contaminants in recycled paper/paperboard for food packaging. J Agric Food Chem 48(12):5856–5859
Yang Y, Xie Y, Tian F et al (2013) Migration detection of Phthalate plasticizers within common food and packaging material. Colour Spectr 31(7):674–678
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2018 Springer Nature Singapore Pte Ltd.
About this paper
Cite this paper
Li, X., Huo, L., Liu, C. (2018). Study on Phthalates Plasticizers Detection of Food Paper Packaging. In: Zhao, P., Ouyang, Y., Xu, M., Yang, L., Ren, Y. (eds) Applied Sciences in Graphic Communication and Packaging. Lecture Notes in Electrical Engineering, vol 477. Springer, Singapore. https://doi.org/10.1007/978-981-10-7629-9_73
Download citation
DOI: https://doi.org/10.1007/978-981-10-7629-9_73
Published:
Publisher Name: Springer, Singapore
Print ISBN: 978-981-10-7628-2
Online ISBN: 978-981-10-7629-9
eBook Packages: EngineeringEngineering (R0)