Synthesis and Characterization of MOF-Derived Nanomaterials

Chapter
Part of the Springer Theses book series (Springer Theses)

Abstract

1.436 g of Co(NO3)2 and 3.244 g of 2-methylimidazole are dissolved in 100 mL methanol, respectively. The Co(NO3)2 solution is poured into the 2-methylimidazole solution under vigorous stirring. After 12 min the stirring is stopped followed by standing for 20 h. The purple product is centrifuged and washed with methanol for at least 3 times. After vacuum drying at 150 ℃ for 8 h, the final product is obtained.

References

  1. 1.
    Jun S, Joo SH, Ryoo R et al (2000) Synthesis of new, nanoporous carbon with hexagonally ordered mesostructure. J Am Chem Soc 122(43):10712–10713CrossRefGoogle Scholar
  2. 2.
    Kovtyukhova N, Ollivier P, Martin B et al (1999) Layer-by-layer assembly of ultrathin composite films from micron-sized graphite oxide sheets and polycations. Chem Mater 11:771–778CrossRefGoogle Scholar
  3. 3.
    Hummers W, Offeman R (1958) Preparation of graphitic oxide. J Am Chem Soc 80:1339CrossRefGoogle Scholar
  4. 4.
    Xia W, Zhu J, Guo W et al (2014) Well-defined carbon polyhedrons prepared from nano metal–organic frameworks for oxygen reduction. J Mater Chem A 2:11606–11613CrossRefGoogle Scholar
  5. 5.
    Xia W, Mahmood A, Liang Z et al (2016) Earth-abundant nanomaterials for oxygen reduction. Angew Chem Int Ed 55:2650–2676CrossRefGoogle Scholar
  6. 6.
    Gasteiger H, Kocha S, Sompalli B et al (2005) Activity benchmarks and requirements for Pt, Pt-alloy, and non-Pt oxygen reduction catalysts for PEMFCs. Appl Catal B 56(1–2):9–35CrossRefGoogle Scholar
  7. 7.
    Koper M (2013) Theory of the transition from sequential to concerted electrochemical proton–electron transfer. Phys Chem Chem Phys 15:1399–1407CrossRefGoogle Scholar
  8. 8.
    Katsounaros I, Cherevko S, Zeradjanin A et al (2014) Oxygen electrochemistry as a cornerstone for sustainable energy conversion. Angew Chem Int Ed 53:102–121CrossRefGoogle Scholar
  9. 9.
    Koper M (2011) Thermodynamic theory of multi-electron transfer reactions: Implications for electrocatalysis. J Electroanal Chem 660:254–260CrossRefGoogle Scholar

Copyright information

© Springer Nature Singapore Pte Ltd. 2018

Authors and Affiliations

  • Wei Xia
    • 1
  1. 1.Department of Materials Science and Engineering, College of EngineeringPeking UniversityBeijingChina

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