Skip to main content

Solid state NMR spectroscopy of synthetic dyes

  • Chapter
Analytical Chemistry of Synthetic Colorants

Part of the book series: Advances in Color Chemistry Series ((ACCS,volume 2))

  • 184 Accesses

Abstract

High-resolution NMR spectroscopy in liquids has been for many years one of the most frequently used methods in chemical structure determination. Therefore, it is not surprising that this technique has also been successfully applied to the analysis of synthetic dyes. 1H NMR data have been summarized by Foris1 and Fedorov2 has collated some 13C NMR data of azo dyes. In addition, an application of two-dimensional NMR spectroscopy3 and multi-nuclear NMR studies4 of azo dyes has been published recently.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 169.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 219.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 219.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. A. Foris (1977) In The Analytical Chemistry of Synthetic Dyes, ed. K. Venkataraman, Wiley, New York.

    Google Scholar 

  2. L.A. Fedorov (1987) NMR Spectroscopy of Organic and Analytical Reagents and Their Complexes with Metal Ions. Nauka, Moscow (in Russian).

    Google Scholar 

  3. A. Lyčka and J. Jirman (1991) In Color Chemistry, Ch. 10 ed. A.T. Peters and H.S. Freeman. Elsevier, London.

    Google Scholar 

  4. A. Lyčka (1993) Annu. Rep. NMR Spectr., 26 247.

    Article  Google Scholar 

  5. C. Fyfe (1984) Solid State NMR for Chemists. CFC Press, Guelph.

    Google Scholar 

  6. A. Abragam (1961) The Principles of Nuclear Magnetism, Oxford University Press, London.

    Google Scholar 

  7. A.N. Garroway, W.B. Monitz and M.A. Resing (1979) Carbon-13 NMR in Polymer Science, ed. W.H. Pasika. A. C.S. Symposium Series, No. 103 p. 67.

    Chapter  Google Scholar 

  8. L.R. Sarles and R.M. Cotts (1958) Phys. Rev., 111, 853.

    Article  CAS  Google Scholar 

  9. A. Pines, M.G. Gibby and J.S. Waugh (1973) J Chem. Phys., 59, 569.

    Article  CAS  Google Scholar 

  10. S.R. Hartmann and E.L. Hahn (1962) Phys. Rev., 128, 2042.

    Article  CAS  Google Scholar 

  11. M. Goldman (1970) Spin Temperature and Nuclear Magnetic Resonance in Solids. Oxford University Press, London.

    Google Scholar 

  12. M. Mehring (1976) High Resolution NMR Spectroscopy in Solids, Springer-Verlag, Berlin.

    Book  Google Scholar 

  13. B.C. Gerstein and C.R. Dybowski (1985) Transient Techniques in NMR of Solids, Academic Press, Orlando.

    Google Scholar 

  14. J. Schaefer, E.O. Stejskal and R. Buchdahl (1977) Macromolecules, 10, 384.

    Article  CAS  Google Scholar 

  15. D.L. VanderHart, W.L. Earl, and A.N. Garroway (1981) J. Magn. Reson., 10, 361.

    Google Scholar 

  16. R. Voelkel (1988) Angew. Chem., Int. Ed. Engl. 27, 1468.

    Article  Google Scholar 

  17. Y.J. Jiang, R.J. Pugmire and D.H. Grant (1987) J. Magn. Reson., 71, 485.

    CAS  Google Scholar 

  18. L.B. Alemany, D.M. Grant, R.J. Pugmire, T.D. Alger and K.W. Zilm (1983) J. Am. Chem. Soc., 105, 2133.

    Article  CAS  Google Scholar 

  19. P. Granger and R.K. Harris (ed.) (1990) Multinuclear Magnetic Resonance in Liquids and Solids—Chemical Applications. Kluwer Academic, Dordrecht.

    Google Scholar 

  20. J. Straka, B. Schneider, A. Lyčka and J. Jirman (1991) Magn. Reson. Chem., 29, 500.

    Article  CAS  Google Scholar 

  21. A.M. Chippendale, M.A. Mathias, R.K. Harris, K.J. Packer and B.J. Say (1981) J. Chem. Soc., Perkin Tr. II, 1981, 1031.

    Article  Google Scholar 

  22. A. Lyčka, J. Jirman, B. Schneider, and J. Straka (1988) Magn. Reson. Chem., 26 507.

    Article  Google Scholar 

  23. R.E. Wasylishen, W.P. Power, G.H. Penner and R.D. Curtis (1989) Can. J. Chem., 67, 1219.

    Article  CAS  Google Scholar 

  24. A. Lyčka, M. Nečas, J. Jirman, J. Straka and B. Schneider (1990) Collect. Czech. Chem. Commun., 55, 193.

    Article  Google Scholar 

  25. A.C. Olivieri, R.B. Wilson, I.C. Paul, and D.Y. Curtin (1989) J. Am. Chem. Soc., 111, 5525.

    Article  CAS  Google Scholar 

  26. B.R. Hsieh, D. Désuets and P.M. Kazmaier (1990) Dyes Pigm., 14, 165.

    Article  CAS  Google Scholar 

  27. L.A. Fedorov (1991) Izv. Akad. Nauk SSSR, Ser. Khim. 1991, 2302.

    Google Scholar 

  28. R.K. Harris, P. Jonsen, K.J. Packer and C.D. Campbell (1986) Magn. Reson. Chem., 24, 977.

    Article  CAS  Google Scholar 

  29. R.K. Harris, P. Jonsen and K.J. Packer (1984) Org. Magn. Reson., 22, 269.

    Article  CAS  Google Scholar 

  30. L.A. Fedorov, A.I. Rebrov and Shen Lianfang (1992) Dyes Pigm., 18, 207.

    Article  CAS  Google Scholar 

  31. A. Lyčka, J. Jirman, H.S. Freeman, S.A. McIntosh and J. Straka (1994) unpublished data.

    Google Scholar 

  32. S.A. McIntosh, H.S. Freeman and P. Singh (1991) Dyes Pigm., 17, 1.

    Article  CAS  Google Scholar 

  33. S.A. McIntosh, H.S. Freeman and P. Singh (1989) Textile Res. J., 59, 389.

    Article  CAS  Google Scholar 

  34. L.A. Fedorov (1991) Izv. Akad. Nauk SSSR, Ser. Khim. 1991, 2775.

    Google Scholar 

  35. L.A. Fedorov and A.I. Rebrov (1992) Izv. Akad. Nauk SSSR, Ser. Khim. 1992, 113.

    Google Scholar 

  36. A.M. Chippendale, A. Mathias, R.S. Aujla, R.K. Harris, K.J. Packer, and B.J. Say (1983) J. Chem. Soc., Perkin Tr. II, 1983, 1357.

    Article  Google Scholar 

  37. R.K. Harris, P. Jonsen and K.J. Packer (1984) Org. Magn. Reson., 22, 784.

    Article  CAS  Google Scholar 

  38. K.Y. Law, S. Kaplan and I.W. Tarnawskyj (1991) Dyes Pigm., 17, 41.

    Article  CAS  Google Scholar 

  39. R.K. Harris, P. Jonsen and K.J. Packer (1987) J. Chem. Soc. Perkin Tr. II, 1987 1383.

    Article  Google Scholar 

  40. H.H. Limbach and B. Wehrle (1987) Fresenius Z. Anal. Chem., 327 61.

    Article  CAS  Google Scholar 

  41. B. Wehrle, H.-H. Limbach, M. Köcher O. Ermer and E. Vogel (1987) Angew. Chem.,99, 914.

    Article  CAS  Google Scholar 

  42. H.-H. Limbach, J. Hennig, R.D. Kendrick and C.S. Yannoni (1984) J. Am. Chem. Soc., 106, 4059.

    Article  CAS  Google Scholar 

  43. R.D. Kendrick S. Friedrich, B. Wehrle, H.-H. Limbach and C.S. Yannoni (1985) J. Magn. Reson., 65, 159.

    Google Scholar 

Download references

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1995 Springer Science+Business Media New York

About this chapter

Cite this chapter

Lyčka, A., Jirman, J., Straka, J. (1995). Solid state NMR spectroscopy of synthetic dyes. In: Peters, A.T., Freeman, H.S. (eds) Analytical Chemistry of Synthetic Colorants. Advances in Color Chemistry Series, vol 2. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-1358-8_2

Download citation

  • DOI: https://doi.org/10.1007/978-94-011-1358-8_2

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-010-4593-3

  • Online ISBN: 978-94-011-1358-8

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics