Skip to main content
SpringerLink
Log in

Introduction to DOR NMR

  • Chapter
Nuclear Magnetic Resonance in Modern Technology

Part of the book series: NATO ASI Series ((ASIC,volume 447))

Abstract

From the symmetry properties of spin interactions, one can design sample rotation techniques for averaging in solids. For the second-order quadmpole effect, this leads to double rotation (DOR), rotating the sample simultaneously about a specific pair of axes. Characteristics of DOR, such as spinning sidebands, are discussed, and representative applications are displayed.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution
Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 429.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 549.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 549.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literature References

  1. A.Samoson, E.Lippmaa. Excitation Phenomena and Line Intensities in High-Resolution NMR Powder spectra of Half-Integer Spin Quadrupolar Nuclei. Phys.Rev B28, 6567 (1983)

    Google Scholar 

  2. A.Samoson, E.Lippmaa. 2D NMR Nutation Spectroscopy of Solids. J.Magn.Res. v79, 255 (1988)

    CAS  Google Scholar 

  3. A.Samoson, A.Pines, E.Lippmaa. High Resolution Solid-State NMR. Averaging of Second-Order Effects by Means of a Double Rotor Molecular Physics. v65,1013 (1988)

    CAS  Google Scholar 

  4. A.Samoson, A.Pines. Double Rotor for Solid State NMR. Rev.Sci.Instrum. v60,3239 (1989)

    Article  CAS  Google Scholar 

  5. A.Samoson, E.Lippmaa. Synchronized Double-Rotation NMR Spectroscopy. J.Magn.Res. v84, 410 (1989)

    CAS  Google Scholar 

  6. P.Grobet, A.Samoson, H.Geerts, J.Martens, P.Jacobs. Crystallographic site Discrimination in Aluminophosphate Molecular sieves by Solid-state NMR: Influence of the Field-Dependent Isotropic Second-Order Quadrupolar Shift on High-Resolution 27Al DOR NMR. J.Phys.Chem. v95, 9620 (1991)

    Article  CAS  Google Scholar 

  7. A.Samoson, B.Sun, A.Pines, New Angles in Motional Averaging. Pulsed Magnetic Resonance: NMR, ESR, and Optics, Clarendon, Oxford 1992

    Google Scholar 

  8. G.Engelhardt, H.Koller, P.Sieger, W.Depmeier, A.Samoson. 27Al and 23Na Double-Rotation NMR of Sodalites. Solid State Nuclear Magn. Res. vl, 127 (1992)

    Article  Google Scholar 

  9. A.Samoson, P.Sarv, J.P. van Braam Houckgeest, B.Kraushaar-Czarnetzki. Chemical Shift Anisotropy of 27Al in ALP04-21. Applied Magnetic Resonance, v4, 171 (1993)

    Article  CAS  Google Scholar 

  10. G.J. Ray, A.Samoson. Double Rotation and Variable Field 27Al NMR study of Dealuminated Y Zeolites. Zeolites,v13, 410 (1993).

    Article  CAS  Google Scholar 

  11. A. Samoson. Approximate Approach to DOR Sideband Suppression. Chem.Phys.Lett. v214, 456 (1993).

    Article  CAS  Google Scholar 

  12. B.Q.Sun, J.H. Baltisberger, Y.Wu, A.Samoson and A. Pines, Solid State Nucl. Magn. Reson., v1, 267 (1993).

    Article  Google Scholar 

  13. M.Hunger, G.Engelhardt, H.Roller and J.Weitkamp. Characterization of sodium cations in dehydrated faujasites and zeolite EMT by 23Na DOR, 2D nutation, and MAS NMR.Solid State Nucl. Magn. Reson. v2,111 (1993),

    Article  CAS  Google Scholar 

  14. E.Cochon and J.P.Amoureux. Sideband analysis in DOR NMR spectra.I. Infinite inner-rotor speed.Solid State Nucl. Magn. Reson., v2,205 (1993).

    Article  CAS  Google Scholar 

  15. J.P.Amoureux and E.Cochon. Sideband analysis in DOR NMR spectra.II. Real finite inner-rotor speed.Solid State Nucl. Magn. Reson., v2,223 (1993).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Chemical Physics and Biophysics, Estonian Academy of Sciences, EE0100, Tallinn, Estonia

    Ago Samoson

Authors
  1. Ago Samoson
    View author publications

    You can also search for this author in PubMed Google Scholar

Editor information

Editors and Affiliations

  1. Department of Chemistry, Colorado State University, Fort Collins, Colorado, USA

    Gary E. Maciel

Rights and permissions

Reprints and permissions

Copyright information

© 1994 Springer Science+Business Media Dordrecht

About this chapter

Cite this chapter

Samoson, A. (1994). Introduction to DOR NMR. In: Maciel, G.E. (eds) Nuclear Magnetic Resonance in Modern Technology. NATO ASI Series, vol 447. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-0756-3_17

Download citation

  • DOI: https://doi.org/10.1007/978-94-011-0756-3_17

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-010-4325-0

  • Online ISBN: 978-94-011-0756-3

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics

Search

Navigation