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Quantitative 13C and 1H NMR of Crude Oil Petroleum and Coal Liquefaction Products

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Magnetic Resonance

Part of the book series: NATO ASI Series ((ASIC,volume 124))

Abstract

Optimum experimental conditions are given for a quantitative analysis of liquid fuels by both 1H CW-NMR and 13C FT-NMR. General procedures are outlined to determine the optimum instrumental parameters (acquisition time, flip angle, pulse delay, solvent and relaxation reagent) to be used in quantitative FT-NMR. Digital corrections of the signal are shown to be necessary to improve the expected accuracy up to ca. 1%.

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Author information

Authors and Affiliations

  1. Laboratoire de Chimie Physique Organique, ERA CNRS 222, Université de Nancy I, France

    J.-J. Delpuech

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  1. J.-J. Delpuech
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Editor information

Editors and Affiliations

  1. Gulf Research and Development Company, University of Pittsburgh, Pittsburgh, Pennsylvania, USA

    Leonidas Petrakis

  2. Université Pierre et Marie Curie, Laboratorie de Chimie des Surfaces, Paris, France

    Jacques P. Fraissard

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© 1984 D. Reidel Publishing Company

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Delpuech, JJ. (1984). Quantitative 13C and 1H NMR of Crude Oil Petroleum and Coal Liquefaction Products. In: Petrakis, L., Fraissard, J.P. (eds) Magnetic Resonance. NATO ASI Series, vol 124. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-6378-8_13

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  • DOI: https://doi.org/10.1007/978-94-009-6378-8_13

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-009-6380-1

  • Online ISBN: 978-94-009-6378-8

  • eBook Packages: Springer Book Archive

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