Abstract
The method traditionally used to recover alcohol throughout the ages has been distillation. Its history is lost in antiquity, but there are indications that the art was known to the Chinese as early as 1000 years BC (Rose 1977). It is thought that it was brought to Europe through Spain by the Moors in the 12th century (Ray 1973). The initial use of distillation was in the production of ‘natural medicines’ from naturally fermented wine, aqua vitae or infusions of herbs (Hastie 1949). The enjoyable aspects of aqua vitae were soon realized, and the Annals of Clonmacnoise recorded in 1405 that the ‘Chieftain of Moyntyreolas died at Christmas by taking a surfeit of aqua vitae’ (Ross 1970). The more modern ‘ills’ of government regulation were introduced at an early stage to the industry. Tax on distilled spirit was introduced as early as 1360 in Germany (Daiches 1969), whereas the requirement to possess a licence to operate a still legally was introduced in Ireland in 1556, although peers, gentlemen of property and borough freemen were exempt (Lyons & Rose 1977).
This is a preview of subscription content, log in via an institution.
Buying options
Tax calculation will be finalised at checkout
Purchases are for personal use only
Learn about institutional subscriptionsPreview
Unable to display preview. Download preview PDF.
References
Anonymous 1961. Continuous process freeze-concentrates vinegar. Food Engineering 33 (3), 82–3.
Anonymous 1980a. New ethanol route wears a low-energy label. Chemical Engineering 87 (23), 103.
Anonymous 1980b. Processing twists to further cut grain-derived ethanol costs continue to burgeon. Chemical Engineering 87 (18), 19.
Anonymous 1981. Energy required for distillation of ethanol in biomass-conversion facilities is reduced. Chemical Engineering 88 (3), 17.
Bergeret, J. 1962. Applications du froid en oenologie. Vinification-stabilisation et concentration des vins. Le Vide 101, 43–9.
Black, C. 1980. Distillation modeling of ethanol recovery and dehydration processes for ethanol and gasohol. Chemical Engineering Progress 76 (9), 78–85.
Black, C. and D. E. Ditsler 1972. Dehydration of aqueous ethanol mixtures by extractive distillation. Advances in Chemistry Series 115, 1–15.
Black, C., R. A. Golding and D. E. Ditsler 1972. Azeotropic distillation results from automatic computer calculations. Advances in Chemistry Series 115, 64–92.
Busche, R. M. 1983. Recovering chemical products from dilute fermentation broths. Biotechnology and Bioengineering Symposium No. 13, 597–615.
Carlson, C. S., P. V. Smith, Jr and C. E. Morrell 1954. Separation of oxygenated organic compounds by water extractive distillation. Industrial and Engineering Chemistry 46, 350–5.
Cook, R. A. and W. F. Furter 1968. Extractive distillation employing a dissolved salt as a separating agent. Canadian Journal of Chemical Engineering 46, 119–23.
Court, R. E. and V. H. Bowers 1970. Irish whiskey. Process Biochemistry 5 (10), 17–20.
Cysewski, G. R. and C. R. Wilke 1978. Process design and economic studies of alternative fermentation methods for the production of ethanol. Biotechnology and Bioengineering 20, 1421–44.
Daiches, D. 1969. Scotch whisky. Its past and present. London: Deutsch.
Dick, R. and G. Mavel 1982. R O technology for preconcentrating alcoholic solutions. Proceedings of the 5th International Alcohol Fuel Technology Symposium, Auckland, New Zealand, 13–18 May, Vol. 1, 151–8.
Essien, D. and D. L. Pyle 1983. Energy conservation in ethanol production by fermentation. Process Biochemistry 18 (4), 31–7.
Fanta, G. F., R. C. Burr, W. L. Orton and W. M. Doane 1980. Liquid-phase dehydration of aqueous ethanol-gasoline mixtures. Science 210, 646–7.
Filippi, R. P. de and J. M. Moses 1982. Extraction of organics from aqueous solutions using critical-fluid carbon dioxide. Biotechnology and Bioengineering Symposium No. 12, 205–19.
Floro, M. B. 1945. Steam consumption of pot stills. International Sugar Journal 47, 246–7
Furter, W. F. 1968. Salt effect in distillation: a technical review. The Chemical Engineer 219, CE 173–7.
Furter, W. F. 1972. Extractive distillation by salt effect. Advances in Chemistry Series 115, 35–45.
Furter, W. F. and R. A. Cook 1967. Salt effect in distillation: a literature review. International Journal of Heat and Mass Transfer 10, 23–36.
Geyer, C. R. 1979. Conserving energy in a distillation train. Chemical Engineering Progress 75 (1), 41–5.
Graham, W. O. 1940a. The influence of distillation methods on brandy composition. Australian Brewing and Wine Journal 58 (6), 40–2.
Graham, W. O. 1940b. The influence of distillation methods on brandy composition. Australian Brewing and Wine Journal 58 (7), 31–3.
Graham, W. O. 1940c. The influence of distillation methods on brandy composition. Australian Brewing and Wine Journal 58(8), 26, 29, 31.
Hastie, D. F. S. 1949. The manufacture of Scotch whisky. Journal of the Incorporated Brewers’ Guild 35 (415), 170–89.
Heist, J. A. 1979. Freeze crystallization. Chemical Engineering 86 (10), 72–82.
Herstein, K. M. and M. B. Jacobs 1948. Chemistry and technology of wines and liquors, 2nd edn. New York: Van Nostrand.
Holland, C. D., S. E. Gallun and M. J. Lockett 1981. Modeling azeotropic and extractive distillations. Chemical Engineering 88 (6), 185–200.
Hong, J., M. Voloch, M. R. Ladisch and G. T. Tsao 1982. Adsorption of ethanol-water mixtures by biomass materials. Biotechnology and Bioengineering 24, 725–30.
Hoover, K. C. and S.-T. Hwang 1982. Pervaporation by a continuous membrane column. Journal of Membrane Science 10, 253–71.
I’Anson, J. A. P. 1971. Rum manufacture. Process Biochemistry 6 (7), 35–9.
Irani, C. A. and E. W. Funk 1977. Separations using supercritical gases. In Recent developments in separation science, N. Norman (ed.), Vol. 3, Part A, 171 - 93. Cleveland, Ohio: CRC Press.
Jaques, D. and W. F. Furter 1972. Prediction of vapor composition in isobaric vapor-liquid systems containing salts at saturation. Advances in Chemistry Series 115, 159–68.
Johnson, A. I. and W. F. Furter 1957. Salt effect in vapor-liquid equilibrium Pt 1. Canadian Journal of Technology 34, 413–24.
Johnson, A. I. and W. F. Furter 1960. Salt effect in vapor-liquid equilibrium Pt 2. Canadian Journal of Chemical Engineering 38, 78–87.
Johnson, A. I. and W. F. Furter 1965. Vapor-liquid equilibrium in systems containing dissolved salts. Canadian Journal of Chemical Engineering 43, 356–7.
Ladisch, M. R. and K. Dyck 1979. Dehydration of ethanol: new approach gives positive energy balance. Science 205, 898–900.
Ladisch, M. R., M. Voloch, J. Hong, P. Blenkowski and G. T. Tsao 1984. Cornmeal adsorber for dehydrating ethanol vapors. Industrial Engineering and Chemical Process Design Development 23, 437–43.
Lee, E. K. L., W. C. Babcock and P. A. Bresnahan 1984. Ethanol-water separation by countercurrent reverse osmosis. Polymer Material Science 50, 251–5.
Leeper, S. A. and P. C. Wankat 1982. Gasohol production by extraction of ethanol from water using gasoline as solvent. Industrial Engineering and Chemical Process Design Development 21, 331–4.
Lehtonen, M. and H. Suomalainen 1977. Rum. In Economic microbiology, A. H. Rose (ed.), Vol. 1: Alcoholic beverages, 595–633. New York: Academic Press.
Lyons, T. P. 1974. Irish whiskey. The Brewer 60, 634–7.
Lyons, T. P. and A. H. Rose 1977. Whisky. In Economic microbiology, A. H. Rose (ed.), Vol. 1: Alcoholivc beverages, 635–89. New York: Academic Press
Maiorella, B., C. R. Wilke and H. W. Blanch 1981. Alcohol production and recovery. Advances in Biochemical Engineering 20, 43–92.
Malik, R. K., P. Ghosh and T. K. Ghose 1983. Ethanol separation by adsorption- desorption. Biotechnology and Bio engineering 25, 2277–82.
Marion, L. 1979. In the spotlight: ethanol. Chemical Engineering 86 (5), 78–9.
Mellan, I. 1977. Industrial solvents handbook, 2nd edn. Park Ridge, New Jersey: Noyes Data.
Meranda, D. and W. F. Furter 1966. Vapor-liquid equilibrium data for system: ethanol-water saturated with potassium acetate. Canadian Journal of Chemical Engineering 44, 298–300.
Meranda, D. and W. F. Furter 1971. Vapor-liquid equilibrium in alcohol-water systems containing dissolved acetate salts. American Institute of Chemical Engineers Journal 17, 38–42.
Meranda, D. and W. F. Furter 1972. Vapor-liquid equilibrium in alcohol-water systems containing dissolved halide salts and salt mixtures. American Institute of Chemical Engineers Journal 18, 111–16.
Meranda, D. and W. F. Furter 1974. Salt effects on vapor-liquid equilibrium: some anomalies. American Institute of Chemical Engineers Journal 20, 103–8.
Milestone, N. B. and D. M. Biddy 1981. Concentration of alcohols by adsorption on silicalite. Journal of Chemical Technology and Biotechnology 31, 732–6.
Mix, T. J., J. S. Dweck, M. Weinberg and R. C. Armstrong 1978. Energy conservation in distillation. Chemical Engineering Progress 74 (4), 49–55.
Mulder, M. H. V., J. O. Hendrikman, H. Hegeman and C. A. Smolders 1983. Ethanol-water separation by pervaporation. Journal of Membrane Science 16, 269–84.
Muller, J. G. 1966. Recent developments in crystallization of ice as applied to freeze concentration. Bulletin of the International Institute of Refrigeration Annexe-3, 15–46.
Munson, C. L. and C. J. King 1984. Factors influencing solvent selection for extraction of ethanol from aqueous solutions. Industrial Engineering and Chemical Process Design Development 23, 109–15.
Norman, W. S. 1945. The dehydration of ethanol by azeotropic distillation. Transactions of the American Institute of Chemical Engineers 23, 66–74.
Othmer, D. F. 1936. Vapor re-use process. Separation of mixtures of volatile liquids. Industrial and Engineering Chemistry 28, 1435–8.
Othmer, D. F. 1978. Azeotropic and extractive distillation. In Kirk-Othmer encyclopedia of chemical technology, 3rd edn, Vol. 3, 352–77. New York: Wiley.
Packowski, G. W. 1978. Beverage spirits, distilled. In Kirk Othmer encyclopedia of chemical technology, 3rd edn, Vol. 3, 830–63. New York: Wiley.
Parulekar, S. J., M. M. Sharma, J. B. Joshi and Y. T. Shah 1982. Separation processes for recovery of valuable chemicals from aqueous effluents. Journal of Separation Process Technology 3 (2/3), 2–29.
Paulaitis, M. E. 1982. Separation processes utilizing supercritical fluids. Proceedings of the Scientific Conference of the Corn Refiners Association Inc., Lincolnshire, Illinois, 16–18 June, 168–97.
Perry, R. H. (ed.) 1963. Chemical engineering handbook,4th edn. New York: McGraw- Hill.
Pyke, M. 1965. The manufacture of Scotch grain whisky. Journal of the Institute of Brewing 71, 209–18.
Ray, C. 1973. Cognac. London: Peter Davies.
Roddy, J. W. 1981. Distribution of ethanol-water mixtures to organic liquids. Industrial Engineering and Chemical Process Design Development 20, 104–8.
Rose, A. H. 1977. History and scientific basis of alcoholic beverage production. In Economic microbiology, A. H. Rose (ed.), Vol. 1: Alcoholic beverages, 1–41. New York: Academic Press.
Ross, J. 1970. Whisky. London: Routledge & Kegan Paul.
Scheibel, E. G. 1950. Dehydration of ethyl alcohol by fractional liquid extraction. Industrial and Engineering Chemistry 42, 1497–508.
Schissel, P. and R. A. Orth 1984. Separation of ethanol-water mixtures by pervapor- ation through thin, composite membranes. Journal of Membrane Science 17, 109–20.
Scott, R. W., P. D. Theaker and A. S. Marsh 1981. Use of extracts prepared with liquid carbon dioxide as a substitute for dry hops. Journal of the Institute of Brewing 87, 252–8.
Simpson, A. C. 1968. Manufacture of Scotch malt whisky. Process Biochemistry 3 (1), 9–12.
Simpson, A. C. 1971. Manufacture of brandy. Process Biochemistry 6 (2), 25–7.
Souissi, A. and F. C. Thyrion 1981. Liquid-liquid extraction of ethanol from aqueous solutions. Proceedings of the 2nd World Congress on Chemical Engineering, Montreal, Canada, Vol. 4, 443–6.
Thorne, R. S. W., E. Helm and K. Svendsen 1971. Control of sulphury impurities in beer aroma. Journal of the Institute of Brewing 77, 148–53.
Unger, E. D. and T. R. Coffey 1975. Production of light-bodied rum by an extractive distillation process. Annals of Technology in Agriculture 24, 469–95.
Valaer, P. 1939. Brandy. Industrial and Engineering Chemistry 31, 339–53.
van Pelt, W. H. 1975. Dutch process cuts cost of freeze concentration. Food Engineering 47 (11), 77–9.
Wagner, J. 1983. Improvement in freeze concentration. Food Engineering 55 (2), 98–100.
Watson, D. C. 1983. A laboratory apparatus for distillation research. In Current developments in malting, brewing and distilling, F. G. Priest and I. Campbell (eds), 249–55. London: Institute of Brewing.
Wentworth, T. O. and D. F. Othmer 1940. Absolute alcohol, an economical method for its manufacture. Transactions of the American Institute of Chemical Engineers 36, 785–99.
Wentworth, T. O., D. F. Othmer and G. M. Pohler 1943. Absolute alcohol, an economical method for its manufacture. II Plant data. Transactions of the American Institute of Chemical Engineers 39, 565–78.
Williams, D. F. 1981. Extraction with supercritical gases. Chemical Engineering Science 36, 1769–88.
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1987 D. R. BErry, G. G. Stewart and I. Russell
About this chapter
Cite this chapter
Larsen, V.F. (1987). Alcohol recovery. In: Berry, D.R., Russell, I., Stewart, G.G. (eds) Yeast Biotechnology. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-3119-0_16
Download citation
DOI: https://doi.org/10.1007/978-94-009-3119-0_16
Publisher Name: Springer, Dordrecht
Print ISBN: 978-94-010-7903-7
Online ISBN: 978-94-009-3119-0
eBook Packages: Springer Book Archive