Abstract
The chiroptical techniques optical rotatory dispersion (o. r. d.) and circular dichroism (c. d.) have now been used by organic chemists for about twenty years. During this time the pace of development has been governed largely by the instrumentation available, which has evolved from manually recording instruments and measurements made over a limited spectral range to sophisticated automatic instruments covering the entire visible and near u. v. regions of the spectrum, 800–185 nm. Most papers which include the words o. r. d. or c. d. in the title deal with fundamental aspects of the subject. As well as the theory of optical activity, these include the study of new chromophores, and of the relationship between the observed Cotton effects (CE) and the underlying electronic transitions, also the formulation and testing of empirical and semi-empirical rules which relate the sign and magnitude of the CE to the geometry of the molecule. Detailed references may be found from the main textbooks and monographs on the subject (64, 82, 83, 92, 333) and from the published proceedings of conferences and symposia (51, 74, 256, 297).
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Hanaoka, M., M. Hesse, and H. Schmid: Na-Demethylseredamin, ein neues Alkaloid aus Rauwolfia sumatrana; absolute Konfiguration von Seredamin. Helv. Chim. Acta 53, 1723 (1970).
Hanson, J. R., and E. Premuzic: Applications of chromous chloride II. The reduction of some steroidal nitro compounds. Tetrahedron 23, 4105 (1967).
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Heckendorn, R., and Ch. Tamm: Synthese von 5-Methyl-3-oxa-A-nor-5β-cholestan und 3-Oxa-Δ4-Cholesten-2-on. Helv. Chim. Acta 50, 1499 (1967).
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Herz, W., and J. J. Schmid: Resin Acids XVI. Some transformations of methyl 12α-hydroxy-13β-abiet-8(9)en-l8-oate. J. Organ. Chem. (USA) 34, 2775 (1969).
Heymes, A., M. Dvolaitzky, and J. Jaques: Conformation et réactivité des sites exocycliques. Sur la stéréochimie de la réduction par les hydrures des méthyl-2 acétylcyclohexanes cis et trans. Bull. soc. chim. France 1968, 2898.
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Hiking, H., K. Nomoro, and T. Takemoto: Sengosterone, an insect metamorphosing substance from Cyathula capitata: Structure. Tetrahedron 26, 887 (1970).
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Höhne, E., I. Seidel, G. Adam, K. Schreiber, and J. Tomko: Stereochemie von Veratrum Alkaloiden. Ord und Röntgenstrukturanalytische Beweise für eine C-BBotkonformation in Tetrahydroveralkalminderivaten. Tetrahedron 28, 409 (1972).
Holý, A.: Nucleic acid components and their analogues CXLVII. Preparation of 5-ethoxycarbonyluridine, 5-carboxyuridine and their nucleotidic derivatives. Collect. Czech. Chem. Comm. 37, 1555 (1972).
Holzapfel, C. W., R. D. Hutchinson, and D. C. Wilkins: The isolation and structure of two new indole derivatives from Penicillium Cyclopium Westling. Tetrahedron 26, 5239 (1970).
Hora, J.: On Steroids CXX. Insect chemosterilants derived from 21-hydroxypregnane6,20-dione. Collect. Czech. Chem. Comm. 34, 344 (1969).
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Houghton, E., and J. E. Saxton: Studies in the echinulin series. Preliminary synthetical studies and the absolute configuration of echinulin. Tetrahedron Letters 1968, 5475.
Huber, U. A., and A. S. Dreiding: Synthese von terpenartigen bicyclischen Systemen über die Cycloaddition von Dimethylketen an Methylcyclopentadien. Helv. Chim. Acta 53, 495 (1970).
Huffman, J. W.: Studies on resin acids VII. Isomerisation of 19-norabietatetraenes. J. Organ. Chem. (USA) 37, 17 (1972).
Huffman, J. W.: Attempted duplication of the methyl shift in eremophilane biosynthesis. J. Organ. Chem. (USA) 37, 2736 (1972).
Hutchison, R. D., P. S. Steyn, and D. L. Thompson: The isolation and structure of 4-hydroxyochratoxin-A and 7-carboxy-3,4-dihydro-8-hydroxy-3-methylisocoumarin from Penicillium viridicatum. Tetrahedron Letters 1971, 4033.
Iguchi, M., A. Nishiyama, H. Koyama, S. Yamamura, and Y. Hirata: Isolation and structure of isocalamendiol. Tetrahedron Letters 1969, 3729.
Ilyas, M., J. N. Usmani, S. P. Bhatnagar, M. Ilyas, W. Rahman, and A. Pelter: WB 1 and W11, the first optically active bifiavones. Tetrahedron Letters 1968, 5515.
Inhoffen, H. H., D. Kopp, S. Marić, J. Bekurdts, and R. Selimoglu: Untersuchungen an hochsubstituierten Athylenen und Glykolen X. Zur Stereochemie der Hexoestrole. Tetrahedron Letters 1970, 999.
Isler, O. (Ed.): Carotenoids. Basel: Birkhäuser Verlag. 1971.
Isono, K., and S. Suzuki: The structure of polyoxin-C. Tetrahedron Letters 1968, 203.
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Jacquesy, J. C., J. Levisalles, and J. Wagnon: Stéréochimie XXXV. Stéroides fluorés VI. Réarrangement spinal de l’androstène-5 diol-3β,17β. Bull. soc. chim. France 1970, 670.
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Johnson, C. R., and D. Mccants: Nucleophilic displacement on sulphur. The inversion of sulphoxide configurations. J. Amer. Chem. Soc. 87, 5404 (1965).
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Kakinuma, K., N. Otake, and H. Yonehara: The structure of detoxin-D1. A selective antagonist of blasticidin-S. Tetrahedron Letters 1972, 2509.
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Kametani, T., M. Ihara, K. Fukumoto, and H. Yagi: Studies on the syntheses of heterocyclic compounds. Part CCC. Syntheses of salutaridine, sinoacutine and thebaine. Formal total syntheses of morphine and sinomenine. J. Chem. Soc. (C) (London) 1969, 2030.
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Kametani, T., H. Sugi, and S. Shibuya: The absolute configuration of cryptostylineIII. Studies on the syntheses of heterocyclic compounds. CCCXCVII. Tetrahedron 27, 2409 (1971).
Kametani, T., H. Sugi, H. Yagi, K. Fukumoto, and S. Shibuya: Synthesis and stereochemistry of 1,2,3,4-tertahydro-6-methoxy-2-methyl- 1 -phenyl-isoquinoline and related compounds. J. Chem. Soc. (C) (London) 1970, 2213.
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Klein, E., and W. Rojahn: (−)7β,10α-Selina-4,11-dien und (+)-5β,7β,10α-Selina3,11-dien. Zwei neue Sesquiterpene der Eudesmanreihe. Tetrahedron Letters 1970, 279.
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Koga, T., and M. Tomoeda: Studies on conformation and reactivity-VII. The synthesis and transannular cyclisation of 2α-hydroxy-5ß-cholestane, leading to 2α,9α-epoxy-5β-cholestane; a new functionalisation reaction at 9C in the steroid nucleus. Tetrahedron 26, 1043 (1970).
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Milborrow, B. V., and C. Djerassi: Alkaloid Studies Part LXI. The structure of twelve new alkaloids from Aspidosperma Cylindrocarpon. J. Chem. Soc. (C) (London) 1969, 417.
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Scopes, P.M. (1975). Applications of the Chiroptical Techniques to the Study of Natural Products. In: Zechmeister, L., Herz, W., Grisebach, H., Kirby, G.W. (eds) Fortschritte der Chemie Organischer Naturstoffe / Progress in the Chemistry of Organic Natural Products. Fortschritte der Chemie Organischer Naturstoffe / Progress in the Chemistry of Organic Natural Products, vol 32. Springer, Vienna. https://doi.org/10.1007/978-3-7091-7083-0_4
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