In Situ X-Ray Absorption Spectroscopy Studies of Functional Nanomaterials

  • Soma Chattopadhyay
  • Soon Gu Kwon
  • Elena V. Shevchenko
  • Jeffrey T. Miller
  • Steve M. Heald


X-ray absorption spectroscopy (XAS) is a powerful technique to study the unoccupied states and the local structure around an excited species of atoms from an element present in a material. Recently, in situ XAS is being used to study catalytic transformations, synthesis of nanoparticles and thin films, kinetics of potential battery materials, etc. Such studies can explain the mechanisms associated with the formation of chemical species during various types of reactions. In this chapter, we shall describe how XAS has proved to be a powerful characterization tool for nanomaterials with potential applications by determining the variation in interatomic distances, coordination numbers, and the type of neighboring atoms within the first few coordination shells of the atom of interest in nanoparticles.


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Copyright information

© Springer-Verlag GmbH Germany, part of Springer Nature 2018

Authors and Affiliations

  • Soma Chattopadhyay
    • 1
  • Soon Gu Kwon
    • 2
  • Elena V. Shevchenko
    • 3
  • Jeffrey T. Miller
    • 4
  • Steve M. Heald
    • 5
  1. 1.Elgin Community CollegeElginUSA
  2. 2.Center for Nanoparticle ResearchInstitute for Basic Science and Seoul National UniversitySeoulRepublic of Korea
  3. 3.Nanoscience and Technology divisionArgonne National LaboratoryArgonneUSA
  4. 4.School of Chemical EngineeringPurdue UniversityWest LafayetteUSA
  5. 5.Advanced Photon SourceArgonne National LaboratoryArgonneUSA

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