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Physicochemical Analysis of Wheat Starch

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Part of the book series: Modern Methods of Plant Analysis ((MOLMETHPLANT,volume 14))

Abstract

Starch occurs as water-insoluble granules which are partially crystalline and birefringent when viewed between crossed polars. Wheat grains contain two main populations of granules, the larger A-type granules are formed early in seed development and have a major dimension ranging from 10–35 μm, the smaller B-type granules are formed later in development and range in size from 1–10 μm. The smaller B-granules can contribute up to 30% by weight of the starch (Evers et al. 1974; Dengate and Meredith 1984). The granules contain two macromolecules, amylose and amylopectin.

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References

  • Adkins GK, Greenwood CT (1966) Isolation of cereal starches in the laboratory. Staerke 18: 213–218

    Article  CAS  Google Scholar 

  • Banks W, Greenwood CT (1975) Starch and its components. Edinburgh University Press, Edinburgh

    Google Scholar 

  • Banks W, Greenwood CT, Muir DD (1971) The characterization of starch and its components, part 3. The technique of semi micro, differential, potentiometric, iodine titration and factors affecting it. Staerke 23: 118–124

    Google Scholar 

  • BeMiller JN (1964) Iodometric determination of amylose amperometric titration. In: Whistler RL (ed) Methods in carbohydrate chemistry, vol 4. Starch. Acad Press, New York, pp 165 —167

    Google Scholar 

  • Biliaderis CG, Page CM, Maurice TJ, Juliano BO (1986) Thermal characterization of rice starches: a polymeric approach to phase transitions of granular starch. J Agric Food Chem 34: 6–14

    Article  CAS  Google Scholar 

  • Colonna P, Buleon A, Mercier C (1987) Physically modified starches. In: Galliard T (ed) Starch: properties and potential. Critical reports on applied chemistry, vol 13. John Wiley, Chichester, pp 79–114

    Google Scholar 

  • Dengate H, Meredith P (1984) Variation in size distribution of starch granules from wheat grain. J Cereal Sci 2: 83–90

    Article  Google Scholar 

  • Donovan JW (1979) Phase transitions of the starch-water system. Biopolymers 18: 263–275

    Article  CAS  Google Scholar 

  • Donovan JW, Lorenz K, Kulp K (1983) Differential scanning calorimetry of heat-moisture treated wheat and potato starches. Cereal Chem 30: 381–387

    Google Scholar 

  • Doublier JL (1987) A rheological comparison of wheat, maize, faba bean and smooth pea starches. J Cereal Sci 5: 247–262

    Article  Google Scholar 

  • Dubois M, Gilles KA, Hamilton JK, Rebers PA, Smith F (1956) Calorimetric method for determination of sugars and related substances. Anal Chem 28: 350–356

    Article  CAS  Google Scholar 

  • Eliasson AC (1986) On the effects of surface active agents on the gelatinization of starch — a calorimetric investigation. Carbohydr Polym 6: 463–476

    Article  CAS  Google Scholar 

  • Ellis HS, Ring SG (1985) A study of some factors influencing amylose gelation. Carbohydr Polym 5: 215–222

    Article  Google Scholar 

  • Ellis HS, Ring SG, Whittam MA (1988) Time dependent changes in the size and volume of gelatinized starch granules on storage. Food Hydrocolloids 2: 321–328

    Article  CAS  Google Scholar 

  • Ellis HS, Ring SG, Whittam MA (1989) A comparison of the viscous behaviour of wheat and maize starch pastes. J Cereal Sci 10: 33–44

    Article  Google Scholar 

  • Evans ID, Haisman DR (1979) Rheology of gelatinised starch suspensions. J Texture Stud 10: 347–370

    Article  Google Scholar 

  • Everett W, Foster JF (1959) The subfractionation of amylose and characterization of subfractions by light scattering. J Am Chem Soc 81: 3459–3469

    Article  CAS  Google Scholar 

  • Evers AD, Greenwood CT, Muir DD, Venables C (1974) Studies on the biosynthesis of starch granules, part 8. A comparison of the properties of the small and the large granules in mature cereal starches. Staerke 26: 42–46

    Google Scholar 

  • Galliard T, Bowler P (1987) Morphology and composition of starch. In: Galliard T (ed) Starch: properties and potential. Critical reports on applied chemistry, vol 13. John Wiley, New York, pp 55–78

    Google Scholar 

  • Gilbert GA, Spragg SP (1964) Iodometric determination of amylose iodine sorption: “blue value”. In: Whistler RL (ed) Methods in carbohydrate chemistry, vol 4. Starch. Acad Press, New York, pp 168–169

    Google Scholar 

  • Gough BM, Greenwell P, Russell PL (1985) On the interaction of sodium dodecyl sulphate with starch granules. In: Hill RD, Munck L (eds) New approaches to research on cereal carbohydrates. Elsevier, Amsterdam, pp 99–108

    Google Scholar 

  • Hizukuri S, Maehara Y (1990) Fine structure of wheat amylopectin: the mode of A to B chain binding. Carbohydr Res 206: 145–159

    Article  CAS  Google Scholar 

  • Hizukuri S, Takagi T (1984) Estimation of the distribution of molecular weight for amylose by the low-angle laser-light scattering technique combined with high performance gel chromatography. Carbohydr Res 134: 1–10

    Article  CAS  Google Scholar 

  • Hizukuri S, Takeda Y, Yasuda M, Suzuki A (1981) Multi-branched nature of amylose and the action of debranching enzymes. Carbohydr Res 94: 205–213

    Article  CAS  Google Scholar 

  • Karkalas J, Raphaelides S (1986) Quantitative aspects of amylose-lipid interactions. Carbohydr Res 157: 215–234

    Article  CAS  Google Scholar 

  • Kugimiya M, Donovan JW (1981) Calorimetric determination of the amylose content of starches based on formation and melting of the amylose-lysolecithin complex. J Food Sci 46: 765–770

    Article  CAS  Google Scholar 

  • Lowy GDA, Sargeant JG, Schofield JD (1981) Wheat starch granule protein: the isolation land characterization of a salt-extractable protein from starch granules. J Sci Food Agric 32:371–377

    Google Scholar 

  • Matheson NK (1971) Amylose changes in the starch of developing wheat grains. Phytochemistry 10: 3213–3219

    Article  CAS  Google Scholar 

  • Mciver RG, Axford DWE, Colwell KH, Elton GAH (1968) Kinetic study of the retrogradation of gelatinised starch. J Sci Food Agric 19: 560–563

    Article  CAS  Google Scholar 

  • Miles MJ, Morris VJ, Orford PD, Ring SG (1985) The roles of amylose and amylopectin in the gelation and retrogradation of starch. Carbohydr Res 135: 271–281

    Article  CAS  Google Scholar 

  • Morrison WR (1988) Lipids in cereal starches: a review. J Cereal Sci 8: 1–15

    Article  CAS  Google Scholar 

  • Morrison WR, Gadan H (1987) The amylose and lipid contents of starch granules in developing wheat endosperm. J Cereal Sci 5: 263–275

    Article  CAS  Google Scholar 

  • Morrison WR, Laignelet B (1983) An improved colorimetric procedure for determining apparent and total amylose in cereal and other starches. J Cereal Sci 1: 9–20

    Article  CAS  Google Scholar 

  • Privalov PL, Gill SJ (1988) Stability of protein structure and hydrophobic interaction. Adv Protein Chem 39: 191–234

    Article  PubMed  CAS  Google Scholar 

  • Ring SG, I’Anson KJ, Morris VJ (1985) Static and dynamic light scattering studies of amylose solutions. Macromolecules 18: 182–188

    Article  CAS  Google Scholar 

  • Russell PL (1987) Gelatinization of starches of different amylose/amylopectin content. A study by differential scanning calorimetry. J Cereal Sci 6: 133–145

    Article  CAS  Google Scholar 

  • Russell PL, Oliver G (1989) The effect of pH and NaC1 content on starch gel ageing. A study by differential scanning calorimetry and rheology. J Cereal Sci 10: 123–138

    Google Scholar 

  • Schoch TJ (1964a) Iodometric determination of amylose potentiometric titration: standard method. In: Whistler RL (ed) Methods in carbohydrate chemistry, vol 4. Starch. Acad Press, New York, pp 157–160

    Google Scholar 

  • Schoch TJ (1964b) Swelling power and solubility of granular starches. In: Whistler RL (ed) Methods in carbohydrate chemistry, vol 4. Starch. Acad Press, New York, pp 106–108

    Google Scholar 

  • Slade L, Levine H (1988) Non-equilibrium melting of native granular starch, part 1. Temperature location of the glass transition associated with gelatinization of A-type cereal starches. Carbohydr Polym 8: 183–188

    Google Scholar 

  • South JB, Morrison WR (1990) Isolation and analysis of starch from single kernels of wheat and barley. J Cereal Sci 12: 43–51

    Article  CAS  Google Scholar 

  • Spies RD, Hoseney RC (1982) Effect of sugars on starch gelatinization. Cereal Chem 59: 128–131

    Google Scholar 

  • Takeda Y, Shirasaka K, Hizukuri S (1984) Examination of the purity and structure of amylose by gel-permeation chromatography. Carbohydr Res 132: 83–92

    Article  CAS  Google Scholar 

  • Takeda Y, Hizukuri S, Takeda C, Suzuki A (1987) Structures of branched molecules of amyloses of various origins, and molar fractions of branched and unbranched molecules. Carbohydr Res 165: 139–145

    Article  CAS  Google Scholar 

  • Watson SA (1964) Determination of starch gelatinization temperature. In: Whistler RL (ed) Methods in carbohydrate chemistry, vol 4. Starch. Acad Press, New York, pp 240–241

    Google Scholar 

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© 1992 Springer-Verlag Berlin Heidelberg

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Noel, T.R., Ring, S.G., Whittam, M.A. (1992). Physicochemical Analysis of Wheat Starch. In: Linskens, H.F., Jackson, J.F. (eds) Seed Analysis. Modern Methods of Plant Analysis, vol 14. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-01639-8_17

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  • DOI: https://doi.org/10.1007/978-3-662-01639-8_17

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-662-01641-1

  • Online ISBN: 978-3-662-01639-8

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