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Ion Cyclotron Resonance Spectrometry pp 97–135Cite as

Pulsed ICR Studies with a One-Region Trapped Ion Analyzer Cell

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Part of the book series: Lecture Notes in Chemistry ((LNC,volume 7))

Abstract

The first mass spectrometer based upon the cyclotron resonance principle was developed in 1949.1,2 At that time the device was called an omegatron mass spectrometer. During the 1950’s a number of groups studied the theory of its operation in the hope of developing it as a compact, light-weight mass spectrometer. It was successfully applied to residual gas analysis in ultrahigh vacuum3–5 and to airborne sampling of the upper atmosphere. But in spite of a number of desireable features, the omegatron was never widely used because of its low mass range and low mass resolution; it was limited to unit resolution of about m/e 50.

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References

  1. J. A. Hippie, H. Sommer, and H. A. Thomas, Phys. Rev. 76, 1877 (1949)

    Article  Google Scholar 

  2. H. Sommer, H. A. Thomas, and J. A. Hippie, Phys. Rev. 82, 697 (1951)

    Article  CAS  Google Scholar 

  3. D. Alpert and R. S. Buritz, J. Appl. Phys. 25, 202 (1954)

    Article  CAS  Google Scholar 

  4. D. Lichtmann, J. Appl. Phys. 31, 1213 (1960)

    Article  Google Scholar 

  5. R. W. Lawson, J. Sci. Instrum. 39, 281 (1962)

    Article  Google Scholar 

  6. H. B. Niemann and B. C. Kennedy, Rev. Sci. Instrum. 37, 722 (1966)

    Article  CAS  Google Scholar 

  7. J. L. Beauchamp, L. R. Anders, and J. D. Baldeschwieler, J. Am. Chem. Soc. 89, 4569 (1967)

    Article  CAS  Google Scholar 

  8. J. D. Baldeschwieler and S. S. Woodgate, Accounts Chem. Res. 4, 114 (1971)

    Article  CAS  Google Scholar 

  9. D. Wobschall, Rev. Sci. Instrum. 36, 466 (1965)

    Article  CAS  Google Scholar 

  10. D. Wobschall, J. R. Graham Jr., and D. Malone, Phys. Rev. 131, 1565 (1963)

    Article  CAS  Google Scholar 

  11. D. Wobschall, J. R. Graham Jr., and D. Malone, J. Chem. Phys. 42, 3955 (1965)

    Article  CAS  Google Scholar 

  12. D. Wobschall, R. A. Fluegge, and J. R. Graham Jr., J. Chem. Phys. 47, 4091 (1967)

    Article  CAS  Google Scholar 

  13. J. L. Beauchamp and J. T. Armstrong, Rev. Sci. Instrum. 40, 123 (1969).

    Article  CAS  Google Scholar 

  14. T. E. Sharp, J. R. Eyler, and E. Li, Int. J. Mass Spectrom. Ion Phys., 9, 421 (1972)

    Article  CAS  Google Scholar 

  15. T. F. Knott and M. Riggin, Can. J. Phys. 52, 427 (1974)

    Google Scholar 

  16. A recent book on this subject is: T. A. Lehman and M. M. Bursey, “Ion Cyclotron Resonance Spectrometry,” Wiley, New York, 1976

    Google Scholar 

  17. R. P. Clow and J. H. Futrell, J. Am. Chem. Soc. 94, 3748 (1972)

    Article  CAS  Google Scholar 

  18. R. P. Clow and J. H. Futrell, Int. J. Mass Spectrom. Ion Phys. 4, 165 (1970)

    Article  CAS  Google Scholar 

  19. R. P. Clow and J. H. Futrell, Int. J. Mass Spectrom. Ion Phys. 8, 119 (1972)

    Article  CAS  Google Scholar 

  20. T. B. McMahon and J. L. Beauchamp, Rev. Sci. Instrum. 42, 1632 (1971)

    Article  CAS  Google Scholar 

  21. M. T. Bowers, D. D. Elleman, and J. L. Beauchamp, J. Phys. Chem. 72, 3599 (1968)

    Article  CAS  Google Scholar 

  22. A. G. Marshall and S. E. Buttrill, Jr., J. Chem. Phys. 52, 2752 (1970)

    Article  CAS  Google Scholar 

  23. M. B. Comisarow, J. Chem. Phys. 55, 205 (1971)

    Article  CAS  Google Scholar 

  24. R. T. Mclver, Jr., Rev. Sci. Instrum. 41, 555 (1970)

    Article  Google Scholar 

  25. R. T. Mclver Jr. and R. C. Dunbar, Int. J. Mass Spectrom. Ion Phys. 7, 471 (1971)

    Article  Google Scholar 

  26. T. E. Sharp, J. R. Eyler, and E. Li, Int. J. Mass Spectrom. Ion Phys. 9, 421 (1972)

    Article  CAS  Google Scholar 

  27. T. B. McMahon and J. L. Beauchamp, Rev. Sci. Instrum. 43, 509 (1972)

    Article  Google Scholar 

  28. M. T. Bowers, D. H. Aue, H. M. Webb, and R. T. Mclver Jr., J. Am. Chem. Soc. 93, 4314 (1971)

    Article  Google Scholar 

  29. R. T. Mclver Jr. and J. R. Eyler, J. Am. Chem. Soc. 93, 6334 (1971)

    Article  Google Scholar 

  30. R. T. Mclver Jr. and J. S. Miller, J. Am. Chem. Soc. 96, 4323 (1974)

    Article  Google Scholar 

  31. R. W. Taft in “Proton Transfer Reactions” (E. F. Caldin and V. Gold, Editors) Chapman and Hall, Ltd., London (1975)

    Google Scholar 

  32. J. I. Brauman, W. N. Olmstead, and C. A. Lieder, J. Am. Chem. Soc. 96, 4030 (1974)

    Article  CAS  Google Scholar 

  33. W. N. Olmstead and J. I. Brauman, J. Am. Chem. Soc. 99, 4219 (1977)

    Article  CAS  Google Scholar 

  34. R. T. Mclver Jr., E.B. Ledford Jr., and J. S. Miller, Anal. Chem. 47, 692 (1975)

    Article  Google Scholar 

  35. E. B. Ledford Jr. and R. T. Mclver Jr., Int. J. Mass Spectrom. Ion Phys. 22, 399 (1976)

    Article  CAS  Google Scholar 

  36. R. L. Hunter and R. T. Mclver, Jr., Chem. Phys., Lett., in press (1977)

    Google Scholar 

  37. M. B. Comisarow and A. G. Marshall, J. Chem. Phys. 64, 110 (1976)

    Article  CAS  Google Scholar 

  38. The prescription used for plating the copper is as follows: high gloss silver plate, .001” per QQ-S-365 followed by .0001” rhodium flash per MIL-R-46085.

    Google Scholar 

  39. J. R. Eyler, Rev. Sci. Instrum. 45, 1154 (1974)

    Article  CAS  Google Scholar 

  40. Corning Glass type 9658 machineable glass ceramic was used for the insulating support rods of the analyzer cell.

    Google Scholar 

  41. H. G. Dehmelt and F. L. Walls, Phys. Rev. Lett. 21, 127 (1968)

    Article  CAS  Google Scholar 

  42. F. L. Walls and G. H. Dunn, Phys. Today 27, 30 (1974)

    Article  CAS  Google Scholar 

  43. R. T. Mclver Jr., Rev. Sci. Instrum. 44, 1071 (1973)

    Article  Google Scholar 

  44. R. T. Mclver Jr. and A. D. Baranyi, Int. J. Mass Spectrom. Ion Phys. 7, 471 (1971)

    Article  Google Scholar 

  45. M. B. Comisarow and A. G. Marshall, J. Chem. Phys. 62, 293 (1975)

    Article  CAS  Google Scholar 

  46. M. B. Comisarow, J. Chem. Phys. 55, 205 (1971)

    Article  CAS  Google Scholar 

  47. F. H. Field, J. L. Franklin, and M. S. B. Munson, J. Am. Chem. Soc. 85, 3575 (1963)

    Article  CAS  Google Scholar 

  48. S. K. Gupta, E. G. Jones, A. G. Harrison, and J. J. Myher, Can. J. Chem. 45, 3107 (1967)

    Article  CAS  Google Scholar 

  49. J. H. Futrell, T. O. Tiernan, F. P. Abramson, and C. D. Miller, Rev. Sci. Instrum. 39, 340 (1968)

    Article  CAS  Google Scholar 

  50. J. E. Bartmess, J. S. Miller, and R. T. Mclver, Jr., in prep.

    Google Scholar 

  51. S. E. Buttrill, Jr., J. Chem. Phys. 50, 4125 (1969)

    Article  CAS  Google Scholar 

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Author information

Authors and Affiliations

  1. Department of Chemistry, University of California, Irvine, California, 92717, USA

    Robert T. McIver Jr.

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  1. Robert T. McIver Jr.
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Editors and Affiliations

  1. Akademie der Wissenschaften und der Literatur zu Mainz, Geschwister-Scholl-Straße 2, D-6500, Mainz, Germany

    Hermann Hartmann

  2. Institut für Physikalische Chemie, Universität Frankfurt, Robert-Mayer-Straße 11, D-6000, Frankfurt am Main 1, Germany

    Karl-Peter Wanczek

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© 1978 Springer-Verlag Berlin Heidelberg

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McIver, R.T. (1978). Pulsed ICR Studies with a One-Region Trapped Ion Analyzer Cell. In: Hartmann, H., Wanczek, KP. (eds) Ion Cyclotron Resonance Spectrometry. Lecture Notes in Chemistry, vol 7. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-93085-0_5

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  • DOI: https://doi.org/10.1007/978-3-642-93085-0_5

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-540-08760-1

  • Online ISBN: 978-3-642-93085-0

  • eBook Packages: Springer Book Archive

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