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Study on Polymeric Nano-Composites by 3D-TEM and Related Techniques

  • Atsushi Kato
  • Yoshinobu Isono
  • Kazuya Nagata
  • Atsushi Asano
  • Yuko IkedaEmail author
Chapter

Abstract

There are strong demands for controlling the morphologies of nanofiller aggregate dispersion and polymer phase separation in order to improve the performance of nanofiller-filled rubber and polymer alloys and to impart new functions to materials. To accomplish these subjects, it is essential to visualize the morphologies three-dimensionally and to have techniques for analyzing and evaluating them. In this chapter, we describe the visualization of the nanofiller network structure and the nanofiller/rubber interaction layer in rubber and the lamella network structure in polyketone/polyamide polymer alloys by using a three-dimensional transmission electron microscopy/electron tomography technique, which is abbreviated as 3D-TEM in this study. The relationship between their morphological parameters and physical properties is also described.

Keywords

Carbon Black Interaction Layer Ethylene Propylene Diene Monomer Volume Resistivity Rubber Matrix 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Notes

Acknowledgments

The authors would like to thank Emeritus Prof. S. Kohjiya of Kyoto University; Dr. S. Hikasa, Dr. H. Iwabuki, and Mr. J. Ootake of the Industrial Technology Center of Okayama Prefecture; Messrs R. Tsushi, Y. Kokubo, and Y. Kasahara of the Kyoto Institute of Technology; Dr. O. Dorozdova of Renishaw K. K.; Mrs. M. Nishioka, and Messrs T. Suda, H. Sawabe, J. Shimanuki, T. Hasegawa, T. Izumi, M. Mukai, and T. Gotou, N. Kojima, M. Hashimoto, Dr. M. Arao, Dr. Y. Takahashi, Misses. M. Gonda, and A. Isoda of NISSAN ARC, LTD. for their valuable cooperation and advice.

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Copyright information

© Springer-Verlag Berlin Heidelberg 2014

Authors and Affiliations

  • Atsushi Kato
    • 1
  • Yoshinobu Isono
    • 2
  • Kazuya Nagata
    • 3
  • Atsushi Asano
    • 4
  • Yuko Ikeda
    • 5
    Email author
  1. 1.Department of Material AnalysisNISSAN ARC, LTDYokosukaJapan
  2. 2.Department of Materials Science and TechnologyNagaoka University of TechnologyNagaokaJapan
  3. 3.Department of Advanced Technology DevelopmentLaboratory of Plastics, Asahikasei Chemicals CorporationKawasaki-ku KawasakiJapan
  4. 4.Department of Applied ChemistryNational Defense AcademyYokosukaJapan
  5. 5.Graduate School of Science and TechnologyKyoto Institute of TechnologyKyotoJapan

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