Abstract
This chapter deals with the importance of analytical chemistry and more particularly the separation techniques in the field of conservation science. High performance liquid chromatography (HPLC) and gas chromatography (GC) are mainly developed. The principles of the methods, some information about the methodology and their evaluation are discussed.
This is a preview of subscription content, log in via an institution.
Buying options
Tax calculation will be finalised at checkout
Purchases are for personal use only
Learn about institutional subscriptionsReferences
Burgot G, Burgot JL (2002) Méthodes Instrumentales d’Analyse Chimique. Tec et Doc, Paris
Poole CF (2003) The essence of chromatography. Elsevier, Bristol
Chavanne M, Beaudoin GJ, Jullien A, Flamand E (1999) Chimie organique expérimentale. Belin, Paris
Defranceschi M (1990) 144 manipulations de chimie générale et minérale. Ellipses, Paris
Douglas A, Skoog F, Holler J, Timothy A, Nieman T (2003) Principes d’Analyse Instrumentales De Boeck. Paris et, Bruxelles
Rouessac F (2004) Analyse chimique (méthodes et techniques instrumentales modernes). Masson, Paris
Arpino P, Prevôt A, Serpinet J, Tranchant J, Vergnol A, Wittier P (1995) Manuel pratique de chromatographie en phase gazeuse. Masson, Paris
Rosset R, Caude M, Jardy A (1991) Chromatographies en phase liquide et supercritique. Masson, Paris
Martin AJP, Synge RLM (1941) A new form of chromatogram employing two liquid phases. 1. A theory of chromatography. 2. Application of the microdetermination of the higher monoaminoacids in proteins. Biochem J 35:1358–1368
Mills JS, White R (1994) The organic chemistry of museum objects. Butterworth Heinemann, London
Shedrinsky AM, Wampler TP, Indictor N, Baer NS (1989) Application of analytical pyrolysis to problems in art and archaeology: a review. J Anal Appl Pyrol 15:393–412
Hovaneissian M, Archier P, Mathe C, Vieillescazes C (2006) Contribution de la chimie analytique à l’étude des exsudats végétaux styrax, storax et benjoin. C R Chim 9(9):1192–1202
Regert M, Rolando C (1996) Archéologie des résidus organiques: De la chimie analytique à l’archéologie : un état de la question. Techné 3:118–128
Mejanelle P, Bleton J, Goursaud S, Tchapla A (1996) Analyse de baumes de momification d’Egypte ancienne par chromatographie gazeuse capillaire: spectrométrie de masse. Analusis Magazine 24(7):16–20
Bleton J, Coupry C, Sansoulet J (1996) Approche d’étude des encres anciennes. Stud Conserv 41:95–108
Connan J, Deschene O (1996) Le bitume à Suse: Collection du Musée du Louvre Réunion des Musées Nationaux et Elf Aquitaine Production. Paris et Pau, Paris
Colinart S (1987) Chapter IV: Matériaux constitutifs. In: Sculptures en cire de l’ancienne Egypte à l’art abstrait, Ministère de la Culture et de la Communication. Editions de la réunion des musées nationaux, Paris PP 29–57
Ploeger R, Scalaron O, Chiantore O (2008) The characterization of commercial artists’ alkyd paints. J Cult Herit 9(4):412–419
Quye A, Wouters J, Boon JJ (1996) A preliminary study of light-ageing effect on the analysis of natural flavanoid-dye wools by photodiode array HPLC and by direct temperature mass spectrometry. In: Commitee for Conservation. ICOM, Edimbourg 2:704–713
Szostek B, Orska-Gawrys J, Surowiec I (1012) Trojanowicz M (2003) Investigation of natural dyes occurring in historical Coptic textiles by high-performance liquid chromatography with UV–Vis and mass spectrometric detection. J Chromatogr 2:179–192
Wallert A (1996) Tannins of the parchment of the Dead Sea scrolls. In: committee for conservation ICOM. Edimbourg, 2:560–564
Richardin P, Copy S, Chahine C, Saltron F, Bonnassies TS (1996) GC and GC/MS characterization of degradation amino acids in naturally and artificially aged leathers. J Am Leather Chem Assoc 91(1):2–17
Pastore P, Magno F, Volpin S, Biscontin G (1991) Chromatographic determination of oxalate ion in patinas covering ancient materials. Ann Chim (Rome) 81(5–6):233–241
Vieillescazes C, Coen S (1993) Charactérisation de quelques résines utilisées en Egypte ancienne. Stud Conserv 38:255–264
Casoli A, Mirti P, Palla G (1995) Characterization of medieval proteinaceous painting media using gas chromatography and gas chromatography- mass spectrometry. Fresenius’ J Anal Chem 352(3–4):372–379
Halpine SM (1992) Amino acid analysis of proteinaceous media from Cosimo Tura’s The Annunciation with Saint Francis and Saint Louis of Toulouse. Stud Conserv 37(1):22–38
Bouchonnet S (2009) La spectrométrie de masse en couplage avec chromatographie en phase gazeuse. Tec and Doc Lavoisier, Paris
Cuoco G, Mathe C, Archier P, Vieillescazes C (2009) A multivariate study of the performance of an ultrasound-assisted madder dyes extraction and characterization by liquid chromatography-photodiode array detection. Ultrason sonochem 16:75–82
Bleton J, Tchapla A (2009) SPME/GC-MS in the caracterisation of terpenic resins. In: Organic mass spectrometry in art and archeology. J Wiley 10:261–302
Colombini MP, Modugno F, Giannarelli S, Fuoco R, Matteini M (2000) GC-MS characterization of paint varnishes. Microchem J 67:385–396
Colombini MP, Andreotti A, Bonaduce I, Modugno F, Ribechini E (2009) Analytical strategies for characterizing organic paint media using gas chromatography/mass spectrometry. Acc Chem Res 43(6):715–727
Gröβl M, Harrison S, Kaml I, Kenndler E (2005) Characterisation of natural polysaccharides (plant gums) used as binding media for artistic and historic works by capillary zone electrophoresis. J Chromatogr 1077:80–89
Kaml I, Vcelakova K, Kenndler E (2004) Characterisation and identification of proteinaceous binding media (animal glues) from their amino acid profile by capillary zone electrophoresis. J Sep Sci 27:161–166
Harrison S, Kaml I, Prokoratova V, Mazanek M, Kenndler E (2005) Animal glues in mixtures of natural binding media used in artistic and historic objects: identification by capillary zone electrophoresis. Anal Bional Chem 382:1520–1526
Findeisen A, Kolivoska V, Kaml I, Baatz W, Kenndler E (2007) Analysis of diterpenoic compounds in natural resins applied as binders in museum objects by capillary electrophoresis. J Chromatogr 1157:454–461
Surowiec I, Kaml I, Kenndler E (2004) Analysis of drying oils used as binding media for objects of art by capillary electrophoresis with indirect UV and conductivity detection. J Chromatogr 1024:245–254
Harrison S, Kaml I, Rainer F, Kenndler E (2005) Identification of drying oils in mixtures of natural binding media used for artistic and historic works by capillary electrophoresis. J Sep Sci 28:1587–1594
Maguregui M, Alonso R, Barandiaran M, Jimenez R, García N (2007) Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work. J Chromatogr 1154:429–436
Puchalska M, Orlinska M, Ackacha M (2003) Identification of anthraquinone coloring matters in natural red dyes by electrspray mass spectrometry coupled to capillary electrophoresis. J Mass Spectrom 38:1252–1258
Kouznetsov DA, Ivanov A, Veletsky P (1994) Detection of alkylated cellulose derivatives in several archaeological linen textile samples by capillary electrophoresis/mass spectrometry. Anal Chem 66:4359–4365
López-Montes A, Blanc R, Espejo T, Huertas-Pérez J, Navalón A, Vilchez JL (2007) Simultaneous identification of natural dyes in the collection of drawings and maps from the Royal Chancellery Archives in Granada (Spain) by CE. Electrophoresis 28:1243–1251
López-Montes A, Blanc R, Espejo T, Navalón A, Vilchez JL (2009) Characterization of sepia ink in ancient graphic documents by capillary electrophoresis. Microchim J 93:121–126
Chankvetadze B (1997) Capillary electrophoresis in chiral analysis. Willey, New York
Dupont A-L, Egasse C, Morin A, Vasseur F (2007) Comprehensive characterisation of cellulose- and lignocellulose- degradation products in agent papers: Capillary zone electrophoresis of low-molar mass organic acids, carbohydrates, and aromatic lignin derivatives. Carbohydr Polym 68:1–16
Doménech-Carbó M (2008) Novel analytical methods for characterising binding media and protective coatings in artworks. Anal Chim Acta 621:109–139
Author information
Authors and Affiliations
Corresponding authors
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2012 Springer-Verlag Berlin Heidelberg
About this chapter
Cite this chapter
Vieillescazes, C., Sierra, I., Morante-Zarcero, S. (2012). Separation Techniques. In: Varella, E. (eds) Conservation Science for the Cultural Heritage. Lecture Notes in Chemistry, vol 79. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-30985-4_2
Download citation
DOI: https://doi.org/10.1007/978-3-642-30985-4_2
Published:
Publisher Name: Springer, Berlin, Heidelberg
Print ISBN: 978-3-642-30984-7
Online ISBN: 978-3-642-30985-4
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)