Experimental Part

  • Corinna Reisinger
Part of the Springer Theses book series (Springer Theses)


All solvents were purified by distillation before use following standard procedures. Absolute solvents were obtained by distillation over appropriate drying agent (vide infra) and then kept under an atmosphere of argon: diethyl ether, tetrahydrofuran, toluene, and n-hexane (sodium, benzophenone as indicator), chloroform, dichloromethane, triethylamine (calcium hydride), ethanol (magnesium). Absolute 1,4-dioxane, TBME, di(n-butyl)ether, DME, NMP, acetonitrile, and DMSO were purchased from Sigma-Aldrich and used as received. Other commercial reagents were obtained from various sources and used without further purification.


Nuclear Magnetic Resonance Crude Product Title Compound Combine Organic Layer Flash Column Chromatography 
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Copyright information

© Springer-Verlag Berlin Heidelberg 2012

Authors and Affiliations

  1. 1.Max-Planck-Institut für KohlenforschungMülheim an der RuhrGermany

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