Skip to main content

Assessment of Individual ASR-Aggregate Particles by XRD

  • Conference paper
  • First Online:
Proceedings of the 10th International Congress for Applied Mineralogy (ICAM)

Abstract

This article describes the direct analysis of polished individual aggregate particles by X-ray diffraction (XRD), as compared to traditional powder samples. These particles are selected from mortar bars and concrete prisms previously exposed to expansion testing as well as virgin aggregate from the PARTNER project [1].The authors performed XRD analyses in solid and powder samples of the same aggregate particle. Comparing the results was concluded that for fine grained rocks without preferred orientation the use of a slab sample is more time efficient than traditional powder specimen, without compromising accuracy. Another advantage of this approach is that the investigated aggregate particles can be selected based on petrographic observations done in concrete thin sections affected by alkali-silica reaction (ASR).

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 259.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 329.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 329.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. Lindgård, J, Nixon, PJ, Borchers, I, Schouenborg, B, Wigum, BJ, Haugen, M, and Åkesson, U (2010): The EU “PARTNER” Project – European standard tests to prevent alkali reactions in aggregates: final results and recommendations. Cement and Concrete Research (40/4): 611–635.

    Google Scholar 

  2. Broekmans, MATM (1999): Classification of the alkali–silica reaction in geochemical terms of silica dissolution. In: Pietersen, H, Larbi, J, and Janssen, H (Editors): Proceedings of the 7th Euroseminar on Microscopy Applied to Building Materials, Delft: 155–170.

    Google Scholar 

  3. Broekmans, MATM (2002): The alkali–silica reaction: mineralogical and geochemical aspects of some Dutch concretes and Norwegian mylonites. PhD-thesis, University of Utrecht, Geologica Ultraiectina (217): pp. 144.

    Google Scholar 

  4. Broekmans, MATM (2004): Structural properties of quartz and their potential role for ASR. Materials Characterization (53): 129–140.

    Article  Google Scholar 

  5. Zhang, X, Blackwell, BQ, and Groves, GW (1990): The microstructures of reactive aggregates. British Ceramic Transaction Journal (89): 89–92.

    Google Scholar 

  6. Broekmans, MATM (2006): Sample representativity: effects of size and preparation on geochemical analysis. In: Fournier, B (editor): Marc-André Bérubé Symposium on alkali-aggregate reactivity in concrete. 8th CANMET/ACI International Conference on Recent Advances in Concrete Technology, May 31 – June 3, 2006, Montréal, Canada: 1–19.

    Google Scholar 

  7. Klug, HP, and Alexander, LE (1974): X-ray Diffraction Procedures for Polycrystalline and Amorphous Materials, 2nd edition. John Wiley & Sons, New York: pp. 966.

    Google Scholar 

  8. Bish, DL, and Reynolds Jr, RC (1989): Sample preparation for X-ray diffraction. In: Bish, DL, and Post, JE (editors): Modern Powder Diffraction. Reviews in Mineralogy (20): 73–99.

    Google Scholar 

  9. Buhrke, VE, Jenkins, R, and Smith, DK (editors) (2001): A Practical Guide for the Preparation of Specimens for X-ray Fluorescence and X-ray Diffraction Analysis. Wiley-VCH, New York: pp. 360.

    Google Scholar 

  10. Cullity, BD, and Stock, SR (2001): Elements of X-ray Diffraction, 3rd edition, Prentice Hall, Upper Saddle River, New Jersey: pp. 664.

    Google Scholar 

  11. RILEM AAR-1 (2003): Detection of potential alkali-reactivity of aggregates – Petrographic method, TC 191-ARP: Alkali-reactivity and prevention – Assessment, specification and diagnosis of alkali-reactivity, prepared by: Sims, I, Nixon, P, Materials and Constructions (36): 480–496.

    Google Scholar 

  12. Humphries, DW (1992): The preparation of thin sections of rocks, minerals and ceramics. Royal Microscopical Society, Oxford Science Publications, Microscopy Handbooks (24): pp. 83.

    Google Scholar 

  13. Varma, A (1991): Handbook of inductively coupled plasma atomic emission spectroscopy. CRC Press, Boca Raton: pp. 380.

    Google Scholar 

Download references

Acknowledgments

The first author kindly acknowledges financial support from Fundação para a Ciência e Tecnologia (FTC/Portugal) through doctoral grant reference SFRH/BD/41810/2007.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Nélia Castro .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2012 Springer-Verlag Berlin Heidelberg

About this paper

Cite this paper

Castro, N., Sorensen, B.E., Broekmans, M.A.T.M. (2012). Assessment of Individual ASR-Aggregate Particles by XRD. In: Broekmans, M. (eds) Proceedings of the 10th International Congress for Applied Mineralogy (ICAM). Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-27682-8_13

Download citation

Publish with us

Policies and ethics