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Experimental Section

  • Zaozao Qiu
Chapter
Part of the Springer Theses book series (Springer Theses)

Abstract

All experiments were performed under an atmosphere of dry dinitrogen with the rigid exclusion of air and moisture using standard Schlenk or cannula techniques, or in a glovebox. All organic solvents (except CH2Cl2) were refluxed over sodium benzophenone ketyl for several days and freshly distilled prior to use. CH2Cl2 was refluxed over CaH2 for several days and distilled immediately prior to use. All chemicals were purchased from either Aldrich or Acros Chemical Co. and used as received unless otherwise noted.

Keywords

Column Chromatography Reaction Vessel Colorless Crystal Yellow Crystal Methyl Acrylate 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Springer-Verlag Berlin Heidelberg 2012

Authors and Affiliations

  1. 1.Department of ChemistryThe Chinese University of Hong KongHong KongPeople’s Republic of China

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