All experiments were performed under an atmosphere of dry dinitrogen with the rigid exclusion of air and moisture using standard Schlenk or cannula techniques, or in a glovebox. All organic solvents (except CH2Cl2) were refluxed over sodium benzophenone ketyl for several days and freshly distilled prior to use. CH2Cl2 was refluxed over CaH2 for several days and distilled immediately prior to use. All chemicals were purchased from either Aldrich or Acros Chemical Co. and used as received unless otherwise noted.
KeywordsColumn Chromatography Reaction Vessel Colorless Crystal Yellow Crystal Methyl Acrylate
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