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Square-Wave Voltammetry

Part of the book series: Monographs in Electrochemistry ((MOEC))

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Abstract

Electroanalytical application of square-wave voltammetry can be divided into direct and stripping measurements. Some ions and compounds that were analyzed directly, i.e., without accumulation of the reactant or product of the electrode reaction, are listed in Table 3.1. The stripping methods are based either on the accumulation of amalgams and metal deposits, or on the adsorptive accumulation of organic substances and metal complexes. For the trace determination of zinc, cadmium, lead and copper ions, anodic stripping SWV on various types of thin mercury film covered electrodes was applied [35–51]. Mercury film covered carbon fiber [52–56] and iridium [57] microelectrodes were also used. Figure 3.1 displays square-wave stripping voltammograms at a mercury-coated nanoband electrode for solutions of increasing cadmium and lead concentrations following a 2min deposition [46]. The inset shows the linear relationships between peak currents and the metal concentrations. The band electrode was fabricated from ultrathin carbonized polyacrylonitrile films. The volume of electrolyte in the cell was 1 μl. The limit of detection of lead ions was found to be 1×10−9 M.

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(2008). Applications. In: Square-Wave Voltammetry. Monographs in Electrochemistry. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-540-73740-7_3

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