Abstract
The preparation of industrial ammonium molybdate from molybdenum concentrate was conducted according to the process of roasting—leaching—purification—precipitation—crystallization. The optimum technological conditions were determined: the roasting temperature was 680 °C, the roasting time was 2.5 h; in the leaching process the alkali excess coefficient was 1.2, the reaction temperature was 80 °C, the liquid-solid ratio was 3:1, the leaching time was 3 h; the amount of (NH4)2S added into the solution was 1.1 times of the theoretical amount, the temperature was 80–85 °C, and the terminal pH was 8.5–9 in the purification process; the density of the solution was 1.4–1.6 g/mL, the pH was 1.5–2 in the precipitation process; temperature of dissolution was controlled at 80–90 °C. The recovery of the preparation of ammonium molybdate can reach 85.18%.
References
P. Huiqing, H. Wei, Experimental study and production practice of copper molybdenum separation in a copper mine. Nonferrous Met. (Min. Process. Sect.) 1, 23–26 (2007)
H. Wei, W. Daijun, Improve the selecting of copper recovery of Tongshankou Copper Mine. Min. Metall. 2, 17–19 (2006)
Z. Dechang, Development and application of four ammonium molybdate. Hydrometall. China 1, 9–12 (1994)
L. Guojian, Z. Hong et al., Experimental study on producing ammonium molybdate molybdenum concentrate. Hydrometall. China 3, 19–23 (2005)
X. Tiegen, Extractive Metallurgy of Molybdenum (Central South University Press, Changsha, 2002), pp. 35–127
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2017 The Minerals, Metals & Materials Society
About this paper
Cite this paper
Qin, Q., Liu, Z., Chen, T., Huang, Z., Yang, J., Han, W. (2017). Study for Preparation of Industrial Ammonium Molybdate from Low Grade Molybdenum Concentrate. In: Kim, H., Alam, S., Neelameggham, N., Oosterhof, H., Ouchi, T., Guan, X. (eds) Rare Metal Technology 2017. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-319-51085-9_28
Download citation
DOI: https://doi.org/10.1007/978-3-319-51085-9_28
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-319-51084-2
Online ISBN: 978-3-319-51085-9
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)