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In Situ and Postmortem Measures of Damage in Polymers at High Strain-Rates

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Dynamic Behavior of Materials, Volume 1

Abstract

Significant progress has been made in the in situ and postmortem observations of the dynamic tensile failure and damage evolution of a range of polymers employing Taylor anvil and Dynamic-Tensile-Extrusion (Dyn-Ten-Ext) loading. The classic Taylor anvil technique involves impacting a right-cylinder against a semi-infinite rigid anvil to access large compressive strains (>1) and high strain-rates (>1,000/s). The Dyn-Ten-Ext technique probes the tensile response of materials at large strains (>1) and high strain-rates (>1,000/s) by firing projectiles through a conical die. Depending on the extrusion ratios and velocities damage varies from bulk deformation with substantial internal damage, to a stable jet with finite particulation, to catastrophic fragmentation. Postmortem sectioning and X-ray computed tomography access mechanisms of internal damage inception and progression. In situ measurements of damage are made with the impact system for ultrafast synchrotron experiments (IMPULSE) using the advanced imaging and X-ray diffraction methods available at the Advanced Photon Source. The time resolved phase-contrast imaging elucidates the evolution of damage features during dynamic loading that is observed in post mortem sectioning and tomography.

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References

  1. Cao F, Cerreta EK, Trujillo CP, Gray GT (2008) Dynamic tensile extrusion response of tantalum. Acta Mater 56(19):5804

    Article  Google Scholar 

  2. Gray GT III, Cerreta E, Yablinsky CA, Addessio LB, Henrie BL, Sencer BH, Burkett M, Maudlin PJ, Maloy SA, Trujillo CP, Lopez MF (2006) Influence of shock prestraining and grain size on the dynamic‐tensile‐extrusion response of copper: experiments and simulation. AIP Conf Proc 845:725

    Article  Google Scholar 

  3. Brown EN, Gray GT III, Trujillo CP (2009) Influence of necking propensity on the Dynamic-Tensile-Extrusion response of fluoropolymers. DYMAT 1:171. doi:10.1051/dymat/2009023

    Google Scholar 

  4. Brown EN, Trujillo CP, Gray GT (2009) Dynamic‐tensile‐extrusion response of fluoropolymers. AIP Conf Proc 1195:1233

    Article  Google Scholar 

  5. Trujillo CP, Brown EN, Gray GT III (2011) Dynamic-Tensile-Extrusion response of polytetrafluoroethylene (PTFE) and polychlorotrifluoroethylene (PCTFE). In: Proulx T (ed) Dynamic behavior of materials, vol 1. Springer, New York, p 73

    Chapter  Google Scholar 

  6. Furmanski J, Trujillo CP, Martinez DT, Gray GT III, Brown EN (2012) Dynamic-Tensile-Extrusion for investigating large strain and high strain rate behavior of polymers. Polym Test 31(8):1031

    Article  Google Scholar 

  7. Furmanski J, Cady CM, Rae PJ, Trujillo CP, Gray GT III, Brown EN (2012) Dynamic-Tensile-Extrusion of polyuria. AIP Conf Proc 1426:1085

    Article  Google Scholar 

  8. Furmanski J, Brown EN, Gray GT III, Trujillo C, Martinez DT, Bilyk S, Becker R (2014) Extreme tensile damage and failure in glassy polymers via Dynamic-Tensile-Extrusion. In: Song B et al (eds) Dynamic behavior of materials, vol 1. Springer, Switzerland, p 107

    Chapter  Google Scholar 

  9. Furmanski J, Brown EN, Clements B, Cady CM, Gray GT (2012) Large-strain time-temperature equivalence in high density polyethylene for prediction of extreme deformation and damage. In: Hiermaier S (ed) DYMAT 2012, vol 26. EPJ Web of Conferences, France, p 01057. doi:10.1051/epjconf/20122601057

    Google Scholar 

  10. Furmanski J, Brown EN, Trujillo CP, Martinez DT, Gray GT III (2013) Incipient and progressive damage in polyethylene under extreme tensile conditions. In: Chalivendra V et al (eds) Dynamic behavior of materials, vol 1. Springer, New York, p 267

    Chapter  Google Scholar 

  11. Jensen BJ, Owens CT, Ramos KJ, Yeager JD, Saavedra RA, Iverson AJ, Luo SN, Fezzaa K, Hooks DE (2013) Impact system for ultrafast synchrotron experiments. Rev Sci Instrum 84:013904

    Article  Google Scholar 

  12. Yeager J, Luo S, Jensen B, Fezzaa K, Montgomery D, Hooks D (2012) High-speed synchrotron X-ray phase contrast imaging for analysis of low-Z composite microstructure. Composites A 43(6):885

    Article  Google Scholar 

  13. Jensen BJ, Luo SN, Hooks DE, Fezzaa K, Ramos KJ, Yeager JD, Kwiatkowski K, Shimada T, Dattelbaum DM (2012) Ultrafast, high resolution, phase contrast imaging of impact response with synchrotron radiation. AIP Advances 2:012170

    Google Scholar 

  14. Luo SN, Jensen BJ, Hooks DE, Fezzaa K, Ramos KJ, Yeager JD, Kwiatkowski K, Shimada T (2012) Gas gun shock experiments with single-pulse X-ray phase contrast imaging and diffraction at the advanced photon source. Rev Sci Instrum 83:073903

    Article  Google Scholar 

  15. Ramos KJ, Jensen BJ, Yeager JD, Bolme CA, Iverson AJ, Carlson CA, Fezzaa K (2014) Investigation of dynamic material cracking with in situ synchrotron-based measurements. In: Song B et al (eds) Dynamic behavior of materials, vol 1. Springer, Switzerland, p 413

    Chapter  Google Scholar 

  16. Brown EN, Willms RB, Gray GT, Rae PJ, Cady CM, Vecchio KS, Flowers J, Martinez MY (2007) Influence of molecular conformation on the constitutive response of polyethylene: a comparison of HDPE, UHMWPE, and PEX. Exp Mech 47(3):381

    Article  Google Scholar 

  17. Brown EN, Trujillo CP, Gray GT (2007) Influence of polyethylene molecular conformation on Taylor impact measurements: a comparison of HDPE, UHMWPE, and PEX. AIP Conf Proc 955:691

    Google Scholar 

  18. Furmanski J, Cady CM, Brown EN (2013) Time–temperature equivalence and adiabatic heating at large strains in high density polyethylene and ultrahigh molecular weight polyethylene. Polymer 54(1):381

    Article  Google Scholar 

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Acknowledgments

This work was performed at Los Alamos National Laboratory and Argonne National Laboratory’s Advanced Photon Source. C.T. Owens of LANL is gratefully acknowledged for his help in target and projectile fabrication, gun setup, and shot execution. J.A. Young and A.H. Curtis of NSTec LLC are gratefully acknowledged for PCI support. This work was supported by LANL’s Science Campaign 2 program and National Security Technologies LLC Shock Wave Physics Related Diagnostics (SWRD) program. LANL is operated by Los Alamos National Security, LLC for the U.S. Department of Energy (DOE) under Contract No. DE-AC52-06NA25396. Use of the Advanced Photon Source, an Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory, was supported by the U.S. DOE under Contract No. DE-AC02-06CH11357.

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Brown, E.N. et al. (2015). In Situ and Postmortem Measures of Damage in Polymers at High Strain-Rates. In: Song, B., Casem, D., Kimberley, J. (eds) Dynamic Behavior of Materials, Volume 1. Conference Proceedings of the Society for Experimental Mechanics Series. Springer, Cham. https://doi.org/10.1007/978-3-319-06995-1_10

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  • DOI: https://doi.org/10.1007/978-3-319-06995-1_10

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