Abstract
Fine grinding and dispersing, such as grinding in stirred media mills, gains importance in several industrial processes. Solid materials processing is frequently subjected to dynamic changes, effecting the performance of milling. To accurately model milling processes, dynamic flowsheet simulation turns out as a promising approach to gain quick and reliable solutions, describing the milling process over time. The connection of different process units is even closer to the industrial setup. Therefore, the focus of the study is the introduction of a dynamic model for stirred media mills that can be implemented into flowsheet simulation. The modelling approach aims at separating grinding and transport phenomena in the mill. Starting with an investigation of a batch grinding process in a “calibration mill”, the dependency of the breakage rate on machine and material parameters is shown. The stressing conditions in this calibration mill are determined theoretically and via simulations using coupled CFD-DEM simulations. In the study, the prediction of influences such as varying grinding media, stirrer speed and solids concentration on the breakage rate worked out well. In continuous processes, the particle transport and axial grinding media distribution, effecting the dynamics, are simulated as a series of instantly mixed cells, connected by mixing streams. With the dynamic flowsheet simulator Dyssol, the dynamic response of the product to changes in the feed was compared to experimental investigations with limestone in a laboratory stirred media mill. Material parameters for the model were tested in a newly designed breakage tester.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Tavares, L.M., de Carvalho, R.M.: Modeling breakage rates of coarse particles in ball mills. Miner. Eng. 22(7–8), 650–659 (2009)
Capece, M., Bilgili, E., Davé, R.: Insight into first-order breakage kinetics using a particle-scale breakage rate constant. Chem. Eng. Sci. 117, 318–330 (2014)
Theuerkauf, J.: Numerische und experimentelle Untersuchungen von Fluid- und Mahlkörperbewegungen in Rührwerkskugelmühlen, Zugl.: Braunschweig, Techn. Univ., Diss., 2000, 1. Aufl., Cuvillier Göttingen, 2000, ISBN 3897128039
Conway-Baker, J., Barley, R.W., Williams, R.A., et al.: Measurement of the motion of grinding media in a vertically stirred mill using positron emission particle tracking (PEPT). Miner. Eng. 15(1), 53–59 (2002)
Jankovic, A.: Variables affecting the fine grinding of minerals using stirred mills. Min. Eng. 16(4), 337–345 (2003)
Hennart, S.L.A., Wildeboer, W.J., van Hee, P., Meesters, G.M.H.: Identification of the grinding mechanisms and their origin in a stirred ball mill using population balances. Chem. Eng. Sci. 64(19), 4123–4130 (2009)
Beinert, S., Fragnière, G., Schilde, C., et al.: Analysis and modelling of bead contacts in wet-operating stirred media and planetary ball mills with CFD–DEM simulations. Chem. Eng. Sci. 134, 648–662 (2015)
Beinert, S., Fragnière, G., Schilde, C., et al.: Multiscale simulation of fine grinding and dispersing processes: stressing probability, stressing energy and resultant breakage rate. Adv. Powder Technol. 29(3), 573–583 (2018)
Kwade, A., Schwedes, J.: Wet grinding in stirred media mills. In: Handbook of Powder Technology, vol. 12, pp. 251–382. Elsevier Science B.V. (2007)
Beinert, S., Schilde, C., Kwade, A.: Simulation of stress energy and grinding media movement within a wet-operated annular-gap mill using the discrete-element method. Chem. Eng. Technol. 35(11), 1911–1921 (2012)
Kürten, H., Raasch, J., Rumpf, H.: Beschleunigung eines kugelförmigen Feststoffteilchens im Strömungsfeld konstanter Geschwindigkeit. Chem. Ing. Tec. 38(9), 941–948 (1966)
Beinert, S.: Mehrskalige Simulationen zur Partikelbeanspruchung bei der Zerkleinerung und Dispergierung, Zugl.: Braunschweig, Techn. Univ., Diss., 2015, 1. Aufl. IPAT-Schriftenreihe, Sierke Göttingen, ISBN 9783868447231 (2015)
Eskin, D., Zhupanska, O., Hamey, R., et al.: Microhydrodynamics of stirred media milling. Powder Technol. 156(2), 95–102 (2005)
Kwade, A.: Determination of the most important grinding mechanism in stirred media mills by calculating stress intensity and stress number. Powder Technol. 105(1–3), 382–388 (1999)
Radziszewski, P.: Shear based stirred mill power model—An adimensional analysis. Miner. Eng. 73, 16–20 (2015)
Afolabi, A., Akinlabi, O., Bilgili, E.: Impact of process parameters on the breakage kinetics of poorly water-soluble drugs during wet stirred media milling: a microhydrodynamic view. Eur. J. Pharm. Sci. Official J. Eur. Fed. Pharm. Sci. 51, 75–86 (2014)
Jayasundara, C.T., Yang, R.Y., Yu, A.B., et al.: Prediction of the disc wear in a model IsaMill and its effect on the flow of grinding media. Miner. Eng. 24(14), 1586–1594 (2011)
Cleary, P.W., Sinnott, M.D.: Computational prediction of performance for a full scale Isamill: Part—Wet models of charge and slurry transport. Miner. Eng. 79, 239–260 (2015)
Gers, R., Climent, E., Legendre, D., et al.: Numerical modelling of grinding in a stirred media mill: Hydrodynamics and collision characteristics. Chem. Eng. Sci. 65(6), 2052–2064 (2010)
Concas, A., Lai, N., Pisu, M., et al.: Modelling of comminution processes in Spex mixer/mill. Chem. Eng. Sci. 61(11), 3746–3760 (2006)
Tuzcu, E.T., Rajamani, R.K.: Modeling breakage rates in mills with impact energy spectra and ultra fast load cell data. Miner. Eng. 24(3–4), 252–260 (2011)
de Carvalho, R.M., Tavares, L.M.: Predicting the effect of operating and design variables on breakage rates using the mechanistic ball mill model. Miner. Eng. 43–44, 91–101 (2013)
Capece, M., Bilgili, E., Davé, R.N.: Formulation of a physically motivated specific breakage rate parameter for ball milling via the discrete element method. AIChE J. 60(7), 2404–2415 (2014)
Kwade, A., Schwedes, J.: Breaking charakteristics of different materials and their effect on stress intensity and stress number in stirred media mills. Powder Technol. 122, 109–121 (2002)
He, M., Wang, Y., Forssberg, E.: Parameter effects on wet ultrafine grinding of limestone through slurry rheology in a stirred media mill. Powder Technol. 161(1), 10–21 (2006)
Rácz, Á.: Reduction of surface roughness and rounding of limestone particles in a stirred media mill. Chem. Eng. Technol. 37(5), 865–872 (2014)
Fragnière, G., Beinert, S., Overbeck, A., et al.: Predicting effects of operating condition variations on breakage rates in stirred media mills. Chem. Eng. Res. Des. 138, 433–443 (2018)
Kwade, A.: Autogenzerkleinerung von Kalkstein in Rührwerkmühlen, Zugl.: Braunschweig, Techn. Univ., Diss., 1996. Berichte aus der Verfahrenstechnik, Shaker Aachen, ISBN 3-8265-2082-3 (1997)
Kwade, A.: A stressing model for the description and optimization of grinding processes. Chem. Eng. Technol. 26(2), 199–205 (2003)
Stadler, R., Polke, R., Schwedes, J., et al.: Naßmahlung in Rührwerksmühlen. Chem. Ing. Tec. 62(11), 907–915 (1990)
Berthiaux, H., Heitzmann, D., Dodds, J.A.: Validation of a model of a stirred bead mill by comparing results obtained in batch and continuous mode grinding. Int. J. Miner. Process. 44–45, 653–661 (1996)
Kwade, A.: Axialer Transport der Produktsuspension in Rührwerkskugelmühlen. Schüttgut 4(1), 13–18 (1998)
Stehr, N.: Zerkleinerung und Materialtransport in einer Rührwerkskugelmühle, Dissertation (1982)
Kwade, A., Schwedes, J.: Autogenzerkleinerung in Rührwerkmühlen. Chem. Ing. Tec. 68(7), 809–812 (1996)
Schons, D., Kwade, A.: Determination of the axial grinding media distribution in the IsaMill using radiometric densitometry. Miner. Eng. 130, 110–116 (2019)
Skorych, Vasyl, Dosta, Maksym, Hartge, Ernst-Ulrich, et al.: Novel system for dynamic flowsheet simulation of solids processes. Powder Technol 314, 665–679 (2017)
Author information
Authors and Affiliations
Corresponding authors
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2020 Springer Nature Switzerland AG
About this chapter
Cite this chapter
Fragnière, G., Böttcher, AC., Thon, C., Schilde, C., Kwade, A. (2020). Dynamic Process Models for Fine Grinding and Dispersing. In: Heinrich, S. (eds) Dynamic Flowsheet Simulation of Solids Processes. Springer, Cham. https://doi.org/10.1007/978-3-030-45168-4_6
Download citation
DOI: https://doi.org/10.1007/978-3-030-45168-4_6
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-030-45167-7
Online ISBN: 978-3-030-45168-4
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)