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Reference Materials in Measurement and Technology

RMMT 2018: Reference Materials in Measurement and Technology pp 67–76Cite as

Manufacturing and Certification of Reference Materials for the Mass Fraction of Boron in Silumin

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Abstract

In this research, we set out to provide metrological support to methods used for determination of the content of boron in silumin. In particular, we present a technology for the synthesis and characterisation of reference materials for the composition of silumin. To this end, a number of research methods were applied, including X-ray phase analysis, atomic emission spectral analysis with arc excitation, gravimetry and mass spectral analysis. As a result, the developed set of reference materials has been included into the State register and the Federal information fund.

Keywords

  • Set of CRMs for the mass fraction of boron in silumin
  • Synthesis
  • Estimation of metrological characteristics
  • Homogeneity
  • Stability
  • Traceability

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Author Contribution Statement

All authors contributed equally to this work.

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Authors and Affiliations

  1. Ural Federal University (UrFU), Ekaterinburg, Russia

    Dmitry G. Lisienko, Margarita A. Dombrovskaya & Eugeniya D. Kubrina

Authors
  1. Dmitry G. Lisienko
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  2. Margarita A. Dombrovskaya
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  3. Eugeniya D. Kubrina
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Corresponding author

Correspondence to Margarita A. Dombrovskaya .

Editor information

Editors and Affiliations

  1. Ural Scientific Research Institute for Metrology, Ekaterinburg, Russia

    Dr. Sergei V. Medvedevskikh

  2. Ural Scientific Research Institute for Metrology, Ekaterinburg, Russia

    Olga N. Kremleva

  3. A.P. Vinogradov Institute of Geochemistry Siberian Branch, Russian Academy of Sciences, Irkutsk, Russia

    Dr. Irina E. Vasil’eva

  4. Ural Scientific Research Institute for Metrology, Ekaterinburg, Russia

    Dr. Egor P. Sobina

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Lisienko, D.G., Dombrovskaya, M.A., Kubrina, E.D. (2020). Manufacturing and Certification of Reference Materials for the Mass Fraction of Boron in Silumin. In: Medvedevskikh, S., Kremleva, O., Vasil’eva, I., Sobina, E. (eds) Reference Materials in Measurement and Technology. RMMT 2018. Springer, Cham. https://doi.org/10.1007/978-3-030-32534-3_7

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