Abstract
Nanoscience and nanotechnology primarily deal with the synthesis characterization exploration and exploitation of nanostructural materials. Polymer nanocomposite materials have lately received great attention in both academia and industry. Small additions of inorganic usually surface-treated nanoparticles have a very positive effect on the electrical properties of insulating polymers. Biopolymers are polymers produced by living organisms in other words they are polymeric biopolymers. Cyclodextrins are a group of naturally occurring cyclic oligosaccharides, with six, seven, or eight glucose subunits linked by α-(1, 4) glycosidic bonds in a torus shaped structure and are denominated as α-, β-, and γ-CD respectively. In the present study, zincoxide/biopolymer nanocompositie was successfully fabricated by a simple and cost effective method. The possible nanomaterial zincoxide was successfully synthesized by simple precipitation technique and then effectivcly impregenated through the β-cyclodextrin matrix. The morphology of the synthesized nanocompositie was investigated using scanning electron microscopy and transmission electron microscopy. The crystalline nature of the nanocomposite was studied using an X-ray diffractometer. XRD analysis revealed the spherical shape allignment of zincoxide with hexagonal wurtzite structure. UV-Vis, FTIR spectral analysis and AFM studies where also performed for the synthesized nano compositie.
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References
Yong, N.L., et al.: Synthesis and characterization of silver oxide nanoparticles by a novel method. Int. J. Sci. Eng. Res. 4, 155–158 (2013)
Manikandan, S., Karthikeyan, N., Silambarasan, M., Rajan, K.S.: Sub-micron dispersions of sand in water prepared by stirred bead milling and ultrasonication: a potential coolant. Appl. Therm. Eng. 44, 1–10 (2012)
Silambarasan, M., Manikandan, S., Rajan, K.S.: Viscosity and thermal conductivity of dispersions of sub-micron TiO2 particles in water prepared by stirred bead milling and ultrasonication. Int. J. Heat Mass Transf. 55, 7991–8003 (2012)
Chitra, K., Annadurai, G.: Antimicrobial activity of wet chemically engineered spherical shaped ZnO nanoparticles on food borne pathogen. Int. Food Res. J. 20(1), 59–64 (2013). [6]. R. Mohamed, I. Mkhalid, E. Baeissa, M. Al-Rayyani
Goh, H.S.: ZnO nanoflake arrays prepared via anodization and their performance in the photodegradation of methyl orange. Turk. J. Chem. 1(35), 375–391 (2011)
Kanade, K.G.: Effect of solvents on the synthesis of nano-size zinc oxide and its properties. Mater. Res. Bull. 41, 590–600 (2006)
Darezereshki, E., et al.: A novel thermal decomposition method for the synthesis of ZnO nanoparticles from low concentration ZnSO4 solutions. Appl Clay Sci. 54, 107–111 (2011)
Kołodziejczak-Radzimska, A., Jesionowski, T.: Zinc oxide-from synthesis to application: a review. Materials 7, 2833–2881 (2014)
Nagaraju, G.: Surfactant free hydrothermally derived ZnO nanowires, nanorods, microrods and their characterization. Mater. Sci. Semicond. Process. 13, 21–28 (2010)
Zareie, M.: A simple method for preparation of micro-sized ZnO flakes. Mater. Lett. 91, 255–257 (2013)
Kale, R.B.: Morphological evolution of hydrothermally derived ZnO nano and microstructures. Opt.-Int. J. Light Electron. Opt. 127, 4621–4624 (2016)
Chen, C.: Synthesis and characterization of nano-sized ZnO powders by direct precipitation method. Chem. Eng. J. 144, 509–513 (2008)
Zhao, D., Zhao, L., Zhu, C.S., Huang, W.Q., Hu, J.L.: Water insoluble ß-cyclodextrin polymer crosslinked by citric acid synthesis and adsorption properties toward phenol and methylene blue. J. Inclus. Phenom. Macrocycl. Chem. 63, 195–201 (2009)
Chen*, C., Liu, P., Lu, C.: Synthesis and characterisation of nano-size ZnO powders by direct precipitation method, July 2008
Lupan, O., Emelchenko, G.A., Ursaki, V.V., Chai, G., Redkin, A.N., Gruzintsev, A.N., Tiginyanu, I.M., Chow, L., Ono, L.K., Roldan Cuenya, B., Heinrich, H., Yakimov, E.E.: Synthesis and characterization of ZnO nanowires for nanosensor applications. Mater. Res. Bull. 45, 1026–1032 (2010)
Dang, D.K., Sundaram, C., Ngo, Y.L.T., Chung, J.S., Kim, E.J., Hur, S.H.: One pot solid-state synthesis of highly fluorescent N and S co-doped carbon dots and its use as fluorescent probe for Ag+ detection in aqueous solution. Sens. Actuators B 255, 3284–3291 (2018)
Zhang, C.L., Liu, J.C., Yang, W.B., Chen, D.L., Jiao, Z.G.: Experimental and molecular docking investigations on the inclusion mechanism of the complex of phloridzin and hydroxypropyl β – cyclodextrin. Food Chem. 215, 124–128 (2017)
Chieng, B.W., Loo, Y.Y.: Synthesis of ZnO nanoparticles by modified polyol method. Mater. Lett. 73, 78–82 (2012)
Zak, A.K., Abrishami, M.E., Majid, W.H.A., Yousef, R., Hosseini, S.M.: Effect of annealing temperature on some structural and optical properties of ZnO nanoparticles prepared by a modified sol-gel combustion method. Ceram. Int. 37, 393–398 (2011)
Sharma, D., Sharma, S., Kaith, B.S., Rajput, J., Kaur, M.: Synthesis of ZnO nanoparticles using surfactant free in-air and microwave method. Appl. Surf. Sci. 257, 9661–9672 (2011)
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Rajalakshmi, T.U., Alagumuthu, G. (2019). A Facile Route for the Fabrication of Nanocompositie by Effective Impregnation Through the Biopolymer Matrix and Its Characterisation. In: Rajan, M., Anand, K., Chuturgoon, A. (eds) Proceedings of the International Conference on Nanomedicine (ICON-2019). ICON 2019. Springer Proceedings in Materials. Springer, Cham. https://doi.org/10.1007/978-3-030-25135-2_14
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DOI: https://doi.org/10.1007/978-3-030-25135-2_14
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